1-Bromodibenzothiophene
- Product Name
- 1-Bromodibenzothiophene
- CAS No.
- 65642-94-6
- Chemical Name
- 1-Bromodibenzothiophene
- Synonyms
- 1-bromodibenzo[b,d]thiophene;1-Bromodibenzothiophene;Dibenzothiophene, 1-bromo-;1-Bromodibenzothiophene ISO 9001：2015 REACH
- CBNumber
- CB73051910
- Molecular Formula
- C12H7BrS
- Formula Weight
- 263.15
- MOL File
- 65642-94-6.mol
1-Bromodibenzothiophene Property
- Melting point:
- 84 °C
- Boiling point:
- 386.6±15.0 °C(Predicted)
- Density
- 1.611±0.06 g/cm3(Predicted)
- form
- powder to crystal
- color
- White to Orange to Green
Safety
- HS Code
- 2934999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H227Combustible liquid
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P363Wash contaminated clothing before reuse.
P370+P378In case of fire: Use … for extinction.
P403+P235Store in a well-ventilated place. Keep cool.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B5861
- Product name
- 1-Bromodibenzothiophene
- Packaging
- 1G
- Price
- $194
- Updated
- 2024/03/01
- Product number
- 9939CS
- Product name
- 1-Bromodibenzothiophene
- Packaging
- 1g
- Price
- $295
- Updated
- 2021/12/16
- Product number
- 44402
- Product name
- 1-Bromodibenzothiophene,≥98%(GC)
- Purity
- ≥98%(GC)
- Packaging
- 1G
- Price
- $69.34
- Updated
- 2021/12/16
- Product number
- OR31666
- Product name
- 1-Bromodibenzothiophene
- Purity
- 99%
- Packaging
- 1g
- Price
- $157
- Updated
- 2021/12/16
1-Bromodibenzothiophene Chemical Properties,Usage,Production
Uses
1-Bromodibenzothiophene can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development processes and chemical production processes.
Synthesis
Into a 1 L four-necked round bottom flask equipped with a stirrer, a Liebig condenser (not required), a 100 mL dropping funnel and a thermometer, 43.5 g (0.156 mol) of the amine hydrochloride obtained in the above ), 240 mL of acetic acid, 55 mL of concentrated hydrochloric acid and 143 mL of water were placed and cooled to -5 ?? C. or lower in an ice water bath. Next, an aqueous solution of 12.0 g (0.173 mol) of sodium nitrite dissolved in 67 mL of water was added dropwise from the dropping funnel at a temperature not exceeding 5 ?? C., and the mixture was stirred at 5 ?? C. or less for 1 hour.The resulting diazo solution was transferred to a 1 L dropping funnel and set in a 1 L 4-necked round bottom flask equipped with a stirrer, a Liebig condenser (not required) and a thermometer, and then 50 % Hypophosphorous acid and 90 mL of water were added, and the mixture was cooled to -5 ?? C. or lower in an ice water bath. Subsequently, the diazo solution was added dropwise at a temperature not exceeding 5 ?? C., after stirring for 1 hour in an ice water bath, it was returned to room temperature and stirred at room temperature for 48 hours.The obtained reaction solution was extracted twice with 310 mL of ethyl acetate, then washed twice with 310 mL of water, dried with magnesium sulfate, magnesium sulfate was removed by suction filtration, and the solvent was distilled off under reduced pressure. Subsequently, the obtained crude oil was purified on a silica gel column using n-heptane as a developing solution to obtain 33.8 g (yield: 82.5%) of the desired bromide.
1-Bromodibenzothiophene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-Bromodibenzothiophene manufacturers
- Product
- 1-Bromodibenzothiophene 65642-94-6
- Price
- US $35.00-25.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 Ton
- Release date
- 2023-09-01
- Product
- 1-Bromodibenzothiophene 65642-94-6
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 99.9%
- Supply Ability
- 30000 Kg
- Release date
- 2023-10-25