3-Chloro-4-formylbenzonitrile

Product Name: 3-Chloro-4-formylbenzonitrile
CAS No.: 58588-64-0
Chemical Name: 3-Chloro-4-formylbenzonitrile
Synonyms: 2-Chloro-4-Cyanobenzaldehyd;3-Chloro-4-formylbenzonitrile;Benzonitrile, 3-chloro-4-formyl-
CBNumber: CB73064590
Molecular Formula: C8H4ClNO
Formula Weight: 165.58
MOL File: 58588-64-0.mol

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3-Chloro-4-formylbenzonitrile Property

Melting point:: 117-119 °C(Solv: ethanol (64-17-5))
Boiling point:: 288.8±25.0 °C(Predicted)
Density: 1.32±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Light yellow to yellow Solid
InChI: InChI=1S/C8H4ClNO/c9-8-3-6(4-10)1-2-7(8)5-11/h1-3,5H
InChIKey: UGRNLUNAHZKZTG-UHFFFAOYSA-N
SMILES: C(#N)C1=CC=C(C=O)C(Cl)=C1

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Safety

HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C384563
Product name: 3-Chloro-4-formylbenzonitrile
Packaging: 100mg
Price: $60
Updated: 2021/12/16

ChemScene

Product number: CS-0130923
Product name: 3-Chloro-4-formylbenzonitrile
Purity: 98.61%
Packaging: 1g
Price: $110
Updated: 2021/12/16

ChemScene

Product number: CS-0130923
Product name: 3-Chloro-4-formylbenzonitrile
Purity: 98.61%
Packaging: 5g
Price: $380
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0361106
Product name: 3-CHLORO-4-FORMYLBENZONITRILE
Purity: 95.00%
Packaging: 5MG
Price: $497.01
Updated: 2021/12/16

AK Scientific

Product number: 5563AQ
Product name: 3-chloro-4-formylbenzonitrile
Packaging: 5g
Price: $555.2
Updated: 2021/12/16

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3-Chloro-4-formylbenzonitrile Chemical Properties,Usage,Production

Synthesis

1050477-54-7

58588-64-0

General procedure for the synthesis of 3-chloro-4-formylbenzonitrile using compound (CAS:1050477-54-7) as starting material: the crude product 3-chloro-4-[2-(dimethylamino)vinyl]benzonitrile was dissolved in 500 mL of THF/water (1:1) mixed solvent and 77.6 g (362.9 mmol) of sodium iodide was added. The reaction mixture was stirred at room temperature for 18 h, followed by filtration to remove the precipitate precipitated. The filtrate was mixed with saturated sodium bicarbonate solution and extracted three times with ethyl acetate. The organic phases were combined, dried with sodium sulfate and the solvent was subsequently removed by rotary evaporator. The crude product was purified by silica gel column chromatography with cyclohexane/ethyl acetate (3:7) as mobile phase. 3.0 g of 3-chloro-4-formylbenzonitrile was finally obtained in 15% yield of the theoretical value.

References

[1] Patent: US2010/305052, 2010, A1. Location in patent: Page/Page column 24
[2] Patent: KR101614164, 2016, B1. Location in patent: Paragraph 0363-0365; 0367

3-Chloro-4-formylbenzonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Chloro-4-formylbenzonitrile Suppliers

China 41 India 2 United States 3 Global 46

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58588-64-0, 3-Chloro-4-formylbenzonitrileRelated Search:

3-Chloro-4-formylbenzonitrile

Benzonitrile, 3-chloro-4-formyl-

2-Chloro-4-Cyanobenzaldehyd

58588-64-0