ChemicalBook > CAS DataBase List > 2,3-DIMETHYL-6-NITROANILINE

2,3-DIMETHYL-6-NITROANILINE

Product Name
2,3-DIMETHYL-6-NITROANILINE
CAS No.
59146-96-2
Chemical Name
2,3-DIMETHYL-6-NITROANILINE
Synonyms
TIMTEC-BB SBB006536;6-NITRO-2,3-XYLIDINE;6-Nitro-2,3-xylidine>2,3-DIMETHYL-6-NITROANILINE;2,3-Dimethyl-6-nitroaniline,97%;2,3-DIMETHYL-6-NITROANILINE 98%;(2,3-Dimethyl-6-nitrophenyl)amine;Benzenamine, 2,3-dimethyl-6-nitro-;2,3-Dimethyl-6-nitroaniline,6-Nitro-2,3-xylidine;6-Nitro-2,3-xylidine, 2-Amino-3,4-dimethylnitrobenzene, 3-Amino-4-nitro-o-xylene
CBNumber
CB7334144
Molecular Formula
C8H10N2O2
Formula Weight
166.18
MOL File
59146-96-2.mol
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2,3-DIMETHYL-6-NITROANILINE Property

Melting point:
117-120 °C(lit.)
Boiling point:
314.38°C (rough estimate)
Density 
1.220±0.06 g/cm3 (20 ºC 760 Torr)
refractive index 
1.6273 (estimate)
storage temp. 
2-8°C, protect from light
form 
Crystalline Powder
pka
-0.16±0.25(Predicted)
color 
Dark yellow to orange-brown
CAS DataBase Reference
59146-96-2(CAS DataBase Reference)
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Safety

Hazard Codes 
Xn
Risk Statements 
20/21/22-36/37/38
Safety Statements 
26-36
RIDADR 
2811
WGK Germany 
3
HazardClass 
6.1
PackingGroup 
III
HS Code 
29214200
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H331Toxic if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical
Product number
N0500
Product name
6-Nitro-2,3-xylidine
Purity
>98.0%(GC)
Packaging
25g
Price
$62
Updated
2025/07/31
TCI Chemical
Product number
N0500
Product name
6-Nitro-2,3-xylidine
Purity
>98.0%(GC)
Packaging
500g
Price
$419
Updated
2025/07/31
TRC
Product number
D457030
Product name
2,3-Dimethyl-6-nitroaniline
Packaging
1g
Price
$55
Updated
2021/12/16
TRC
Product number
D457030
Product name
2,3-Dimethyl-6-nitroaniline
Packaging
10g
Price
$105
Updated
2021/12/16
AK Scientific
Product number
X6989
Product name
2,3-dimethyl-6-nitroaniline
Packaging
25g
Price
$146
Updated
2021/12/16
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2,3-DIMETHYL-6-NITROANILINE Chemical Properties,Usage,Production

Chemical Properties

dark yellow to orange-brown crystalline powder

Uses

2,3-Dimethyl-6-nitroaniline is an aromatic compound used in the study of C-H pi interactions and pi-pi stacking. 

Application

2,3-Dimethyl-6-nitroaniline exhibits solubility in water, ethanol, and acetone, making it a versatile reagent for diverse scientific research applications.

Synthesis

114166-32-4

138330-47-9

59146-96-2

80879-86-3

General procedure for the synthesis of 2,3-dimethyl-6-nitroaniline and 2,3-dimethyl-4-nitroaniline from the compounds (CAS:114166-32-4) and N-(2,3-dimethyl-6-nitrophenyl)acetamide: To a solution of N-(2,3-dimethyl-6-nitrophenyl)acetamide (16.0 g, 1.0 equiv.) was added a 60% H2SO4 solution (150 mL). The reaction mixture was heated to reflux temperature, maintained for 1 hour and then cooled to room temperature. The solution was diluted with ice water (100 mL) and neutralized with 2N NaOH solution. The reaction mixture was extracted with EtOAc (3 x 50 mL). The organic phases were combined, washed sequentially with saturated NaHCO3 solution (2 × 50 mL) and saturated NaCl solution (2 × 50 mL), dried over anhydrous Na2SO4 and concentrated under reduced pressure. The residue was purified by column chromatography (10% CH2Cl2/hexane) to afford 2,3-dimethyl-6-nitroaniline (5.5 g, 43%) and 2,3-dimethyl-4-nitroaniline (1.5 g, 12%). 1H NMR data for 2,3-dimethyl-6-nitroaniline (5.5 g, 43%): δ 2.05 (s, 3H), 2.20 (s, 3H), 6.15 (br s, 2H), 6.45 (d, J=8.7 Hz, 1H), 7.63 (d, J=9.0 Hz, 1H) in CDCl3; δ 2.10 (s 3H), 2.30 (s, 3H), 6.50 (d, J=8.7Hz, 1H), 7.15 (br s, 2H), 7.75 (d, J=9.0Hz, 1H). 1H NMR data for 2,3-dimethyl-4-nitroaniline: δ 2.10 (s, 3H), 2.45 (s, 3H), 4.05 (br s, 2H), 6.45 (d, J=9.0 Hz, 1H), 7.65 (d, J=8.7 Hz, 1H) in CDCl3; δ 2.00 (s, 3H), 2.35 (s 3H), 6.12 (br s, 2H), 6.53 (d, J=9.0 Hz, 1H), 7.63 (d, J=9.0 Hz, 1H).

References

[1] Patent: US6353006, 2002, B1. Location in patent: Page column 28-29

2,3-DIMETHYL-6-NITROANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,3-DIMETHYL-6-NITROANILINE Suppliers

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View Lastest Price from 2,3-DIMETHYL-6-NITROANILINE manufacturers

Career Henan Chemical Co
Product
2,3-DIMETHYL-6-NITROANILINE 59146-96-2
Price
US $1.00/KG
Min. Order
1g
Purity
98%
Supply Ability
200kgs
Release date
2020-01-09

59146-96-2, 2,3-DIMETHYL-6-NITROANILINERelated Search:

2,3-DIMETHYL-6-NITROANILINE 3-AMINO-NN-DIMETHYL-4-NITROANILINE 97%,3-AMINO-N,N-DIMETHYL-4-NITROANILINE 4-BROMO-2,3-DIMETHYL-6-NITROANILINE 4,5-DIMETHYL-2-NITROANILINE / 6-NITRO-3,4-XYLIDINE,4,5-DIMETHYL-2-NITROANILINE 4-AMINO-N,N-DIMETHYL-3-NITROANILINE,4-AMINO-NN-DIMETHYL-3-NITROANILINE 97%,4-Amino-N,N-dimethyl-3-nitroaniline, GC 97% 4,6-DIMETHYL-2-NITROANILINE, TECH., 90%,4,6-DIMETHYL-2-NITROANILINE N,N-DIMETHYL-2-NITROANILINE,N,N-DIMETHYL-O-NITROANILINE N,2-DIMETHYL-4-NITROANILINE 4-Fluoro-N,N-dimethyl-2-nitroaniline 2,5-DIMETHYL-4-NITROANILINE N,N-DIMETHYL-M-NITROANILINE,N,N-DIMETHYL-3-NITROANILINE 2-TRIFLUOROMETHYL-N,N-DIMETHYL-4-NITROANILINE 3-TRIFLUOROMETHYL-N,N-DIMETHYL-4-NITROANILINE N,N-Dimethyl-4-nitroaniline, 98+%,N,N-DIMETHYL-P-NITROANILINE,N,N-DIMETHYL-4-NITROANILINE 2-CHLORO-N,N-DIMETHYL-4-NITROANILINE 2 3-DIMETHYL-6-NITROPHENYL ISOCYANATE N-(2,3-DIMETHYL-6-NITROPHENYL)-2,2-DIMETHYLPROPIONAMIDE 2,4-DIMETHYL-5-NITROANILINE

  • TIMTEC-BB SBB006536
  • 6-NITRO-2,3-XYLIDINE
  • 2,3-DIMETHYL-6-NITROANILINE
  • 2,3-Dimethyl-6-nitroaniline,6-Nitro-2,3-xylidine
  • (2,3-Dimethyl-6-nitrophenyl)amine
  • 6-Nitro-2,3-xylidine, 2-Amino-3,4-dimethylnitrobenzene, 3-Amino-4-nitro-o-xylene
  • 2,3-DIMETHYL-6-NITROANILINE 98%
  • 2,3-Dimethyl-6-nitroaniline,97%
  • 6-Nitro-2,3-xylidine&gt
  • Benzenamine, 2,3-dimethyl-6-nitro-
  • 59146-96-2
  • CH32C6H2NO2NH2
  • AMINE
  • Organic Building Blocks
  • Nitrogen Compounds
  • Building Blocks
  • Amines
  • C8