ChemicalBook > CAS DataBase List > 12H- [1] benzothieno [2,3-a] carbazole
12H- [1] benzothieno [2,3-a] carbazole
- Product Name
- 12H- [1] benzothieno [2,3-a] carbazole
- CAS No.
- 222-21-9
- Chemical Name
- 12H- [1] benzothieno [2,3-a] carbazole
- Synonyms
- A028;Benzothieno[2,3-a]carbazole;12H-benzo[4,5]thieno[2,3-a]carbazole;12H- [1] benzothieno [2,3-a] carbazole;12H - [1] Benzothiopheno [2,3-A] carbazole
- CBNumber
- CB73345932
- Molecular Formula
- C18H11NS
- Formula Weight
- 273.35
- MOL File
- 222-21-9.mol
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12H- [1] benzothieno [2,3-a] carbazole Property
- Boiling point:
- 544.5±23.0 °C(Predicted)
- Density
- 1.411±0.06 g/cm3(Predicted)
- pka
- 16.55±0.30(Predicted)
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12H- [1] benzothieno [2,3-a] carbazole Chemical Properties,Usage,Production
Synthesis
In a 3L flask,104.0 g (0.33 mol) of N-(2-chlorophenyl)dibenzo[b,d]thiophen-4-amine, 7.54 g (33.6 mmol) of palladium acetate, 328.26 g(1.0 mol) cesium carbonate, and 24.7 g (67.17 mol)Tricyclohexylphosphine-tetrafluoroborate were mixed with 1.1 L of N, N-dimethylacetamide. The mixture was heated and refluxed under a stream of nitrogen for 12 hours. When the reaction was over, After volatilizing and removing the solvent. The product was added to 2L of methanol. The crystallized solid was filtered and dissolved in dichlorobenzene. After filtration over silica gel/Celite after removal of the appropriate amount of organic solvent, recrystallization from methanol gave 12H- [1] benzothieno [2,3-a] carbazole (81.0 g, yield 88%).
12H- [1] benzothieno [2,3-a] carbazole Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 12H- [1] benzothieno [2,3-a] carbazole manufacturers
Henan Fengda Chemical Co., Ltd
- Product
- 12H- [1] benzothieno [2,3-a] carbazole 222-21-9
- Price
- US $50.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-22
Zhuozhou Wenxi import and Export Co., Ltd
- Product
- A028 222-21-9
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-11
Zhuozhou Wenxi import and Export Co., Ltd
- Product
- A028 222-21-9
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09