5-FORNYL-3-PYRIDINECARBONITRILE

Product Name: 5-FORNYL-3-PYRIDINECARBONITRILE
CAS No.: 70416-53-4
Chemical Name: 5-FORNYL-3-PYRIDINECARBONITRILE
Synonyms: 3-Cyano-5-formylpyridine;5-ForMyl-nicotinonitrile;5-formylpyridine-3-carbonitril;5-FORMYL-3-PYRIDINECARBONITRILE;5-FORNYL-3-PYRIDINECARBONITRILE;5-formylpyridine-3-carbonitrile;5-Cyanopyridine-3-carboxaldehyde;3-Pyridinecarbonitrile, 5-formyl-
CBNumber: CB7364244
Molecular Formula: C7H4N2O
Formula Weight: 132.12
MOL File: 70416-53-4.mol

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5-FORNYL-3-PYRIDINECARBONITRILE Property

Boiling point:: 229.3±20.0 °C(Predicted)
Density: 1.24±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: -0.01±0.20(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: F701420
Product name: 5-Formyl-3-pyridinecarbonitrile
Packaging: 250mg
Price: $95
Updated: 2021/12/16

TRC

Product number: F701420
Product name: 5-Formyl-3-pyridinecarbonitrile
Packaging: 1g
Price: $305
Updated: 2021/12/16

AK Scientific

Product number: Z5052
Product name: 5-Formylnicotinonitrile
Packaging: 100mg
Price: $74
Updated: 2021/12/16

Apolloscientific

Product number: OR927407
Product name: 5-Formyl-3-pyridinecarbonitrile
Purity: 96%
Packaging: 250mg
Price: $275
Updated: 2021/12/16

Apolloscientific

Product number: OR927407
Product name: 5-Formyl-3-pyridinecarbonitrile
Purity: 96%
Packaging: 1g
Price: $530
Updated: 2021/12/16

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5-FORNYL-3-PYRIDINECARBONITRILE Chemical Properties,Usage,Production

Synthesis

135124-71-9

70416-53-4

General procedure for the synthesis of 5-formyl-3-pyridinecarbonitrile from 5-(hydroxymethyl)nicotinonitrile: (d) 5-(hydroxymethyl)nicotinonitrile (0.070 g, 0.52 mmol), anhydrous dichloromethane (1.04 mL), and manganese oxide (0.181 g, 2.09 mmol) were mixed to form a black suspension, which was heated to reflux and the progress of the reaction was monitored by thin-layer chromatography (TLC). after 8 h, the reaction mixture was cooled to room temperature, and to a reaction flask additional manganese oxide (0.095 g, 1.1 mmol). Subsequently, the reaction mixture was heated to reflux again.After 18 h, the reaction was still incomplete, so manganese oxide (0.097 g, 1.1 mmol) was added again. After continued heating at 60 °C for 72 h, the reaction mixture was cooled to room temperature, diluted with ethyl acetate (50 mL), filtered through diatomaceous earth and washed with additional ethyl acetate (50 mL). The organic filtrates were combined, dried with magnesium sulfate, filtered through sintered glass and concentrated to give 0.064 g (93% yield) of white solid product. Further purification by column chromatography (eluent: ethyl acetate/hexane, 1:3) afforded 0.038 g (55% yield) of 5-formyl-3-pyridinecarbonitrile as a white solid. 1H NMR (CDCl3) data: δ 10.17 (s, 1H), 9.28 (d, J = 1.9 Hz, 1H), 9.11 (d, J = 2.2 Hz, 1H), 8.45 (dd, J = 2.2, 1.9 Hz, 1H).

References

[1] Patent: US2006/104998, 2006, A1. Location in patent: Page/Page column 16

5-FORNYL-3-PYRIDINECARBONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-FORNYL-3-PYRIDINECARBONITRILE Suppliers

China 65 India 2 United Kingdom 1 United States 10 Global 78

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
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Chengdu AstaTech Trading Co., Ltd./AstaTech (Chengdu) Pharma. Co., Ltd.

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Bide Pharmatech Ltd.

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View Lastest Price from 5-FORNYL-3-PYRIDINECARBONITRILE manufacturers

Career Henan Chemical Co

Product: 5-FORNYL-3-PYRIDINECARBONITRILE 70416-53-4
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2020-01-10

Career Henan Chemical Co

Product: 5-FORNYL-3-PYRIDINECARBONITRILE 70416-53-4
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2020-01-10

70416-53-4, 5-FORNYL-3-PYRIDINECARBONITRILERelated Search:

2-AMINO-7-CHLORO-5-OXO-5H-(1)BENZOPYRANO-(2,3-B)-PYRIDINE-3-CARBONITRILE 2-AMINO-5-OXO-5H-(1) BENZOPYRANO-(2,3-B)-PYRIDINE-3-CARBONITRILE 2-AMINO-7-ISOPROPYL-5-OXO-5 H-[1]BENZOPYRANO[2,3-B]PYRIDINE-3-CARBONITRILE ETHYL 2-CHLORO-3-CYANO-6-(TRIFLUOROMETHYL)-PYRIDINE-5-CARBOXYLATE 2-AMINO-7-BROMO-5-OXO-5H-(1)BENZOPYRANO& 5-ACETYL-6-METHYL-2-OXO-1,2-DIHYDROPYRIDINE-3-CARBONITRILE ETHYL 5-CYANO-6-MERCAPTO-2-METHYLNICOTINATE 2,4-DIMETHYL-5-OXO-5H-CHROMENO[3,4-C]PYRIDINE-1-CARBONITRILE 5-ACETYL-2-[(3,4-DICHLOROBENZYL)SULFANYL]-6-METHYLNICOTINONITRILE BUTTPARK 82\12-87 2-AMINO-7 9-DIMETHYL-5-OXO-5H(1)BENZO- METHYL 5-CYANO-2-(DIMETHOXYMETHYL)-6-MERCAPTONICOTINATE ETHYL 5-CYANO-6-MERCAPTO-2-PHENYLNICOTINATE 2-AMINO-7-METHYL-5-OXO-5H-(1)BENZOPYRANO-(2,3-B)PYRIDINE-3-CARBONITRILE, 98 ETHYL 5-CYANO-6-([2-(([(2,6-DICHLORO-4-PYRIDYL)AMINO]CARBONYL)AMINO)PHENYL]THIO)-2-(TRIFLUOROMETHYL)NICOTINATE ETHYL 5-CYANO-6-(METHYLSULFANYL)-2-PHENYLNICOTINATE 5-ACETYL-2-([5-CHLORO-2-NITRO-4-(TRIFLUOROMETHYL)PHENYL]THIO)-4-(4-METHOXYPHENYL)-6-METHYLNICOTINONITRILE AURORA KA-6192

5-FORNYL-3-PYRIDINECARBONITRILE

5-FORMYL-3-PYRIDINECARBONITRILE

5-ForMyl-nicotinonitrile

3-Cyano-5-formylpyridine

5-Cyanopyridine-3-carboxaldehyde

5-formylpyridine-3-carbonitrile

3-Pyridinecarbonitrile, 5-formyl-

5-formylpyridine-3-carbonitril

70416-53-4