4,5-Diiodo-1H-imidazole

Product Name: 4,5-Diiodo-1H-imidazole
CAS No.: 15813-09-9
Chemical Name: 4,5-Diiodo-1H-imidazole
Synonyms: 4,5-DIIODOIMIDAZOLE;Diiodo 1h Imidazole?;4,5-DIIODO-1H-IMIDAZOLE;4,5-triiodo-1H-imidazole;1H-Imidazole, 4,5-diiodo-;4,5-Diiodo-1H-imidazole 98%;4,5-Diiodo-1H-imidazole ISO 9001：2015 REACH
CBNumber: CB7380550
Molecular Formula: C3H2I2N2
Formula Weight: 319.87
MOL File: 15813-09-9.mol

More

Less

4,5-Diiodo-1H-imidazole Property

Melting point:: 197-198°C
Boiling point:: 436.9±30.0 °C(Predicted)
Density: 3.042±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 9.31±0.10(Predicted)
form: solid
color: Off-white
InChI: InChI=1S/C3H2I2N2/c4-2-3(5)7-1-6-2/h1H,(H,6,7)
InChIKey: XMWPTVMTXKJONE-UHFFFAOYSA-N
SMILES: C1NC(I)=C(I)N=1
CAS DataBase Reference: 15813-09-9(CAS DataBase Reference)

More

Less

Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
HazardClass: IRRITANT
HS Code: 2933299090

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

More

Less

N-Bromosuccinimide Price

TRC

Product number: B426665
Product name: 4,5-Diiodo-1H-imidazole
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD147395
Product name: 4,5-Diiodo-1H-imidazole
Packaging: 2g
Price: $89
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD147395
Product name: 4,5-Diiodo-1H-imidazole
Packaging: 5G
Price: $178
Updated: 2021/12/16

AK Scientific

Product number: N700
Product name: 4,5-Diiodo-1H-imidazole
Packaging: 1g
Price: $14
Updated: 2021/12/16

Apolloscientific

Product number: OR10450
Product name: 4,5-Diiodo-1H-imidazole
Purity: 98%
Packaging: 1g
Price: $15
Updated: 2021/12/16

More

Less

4,5-Diiodo-1H-imidazole Chemical Properties,Usage,Production

Uses

suzuki reaction

Synthesis

288-32-4

15813-09-9

The general procedure for the synthesis of 4,5-diiodoimidazole from imidazole was as follows: a mixture of potassium iodide (KI, 29.3 g, 176.0 mmol) and iodine (I2, 22.4 g, 88.0 mmol) in water (60 mL) was added to a solution of 1H-imidazole (3.0 g, 44.1 mmol) dissolved in 2M sodium hydroxide (NaOH, 10.6 g, 264.5 mmol) solution. The reaction mixture was stirred at 20 °C for 3 h and subsequently neutralized by adjusting the pH to 7 with 6 M hydrochloric acid (HCl). The resulting solid product was collected by filtration and purified by recrystallization with ethanol to give the final 4,5-diiodoimidazole as an anhydrous solid (14.0 g, 99.0% yield). The melting point was 166-168 °C. 1H NMR (300 MHz, DMSO-d6) δ (ppm): 12.75 (broad peak, 1H), 7.8 (broad peak, 1H). Mass spectrum (EI) m/z: 320.8 [MH]+.

References

[1] European Journal of Medicinal Chemistry, 2017, vol. 140, p. 293 - 304
[2] Patent: CN107501272, 2017, A. Location in patent: Paragraph 0085; 0086; 0087; 0088
[3] Synlett, 2004, # 7, p. 1306 - 1308
[4] Advanced Synthesis and Catalysis, 2013, vol. 355, # 2-3, p. 499 - 507
[5] Advanced Synthesis and Catalysis, 2013, vol. 355, # 16, p. 3231 - 3243

4,5-Diiodo-1H-imidazole Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

4,5-Diiodo-1H-imidazole Suppliers

China 154 France 1 Germany 4 India 1 United Kingdom 5 United States 20 Global 185

Shaanxi Zhong Zhi Biao Pin Pharmaceutical technology Co., LTD

Tel: 029-89239927 18009291534
Email: 18009291534@163.com
Country: China
ProdList: 406
Advantage: 58

Xuchang Fengfei New Materials Technology Co., Ltd

Tel: 19713077352
Email: 1038096457@qq.com
Country: China
ProdList: 2642
Advantage: 58

Nanjing xiangrui technology co. LTD

Tel: 021-021-00000000 15715199582
Email: njrich168@163.com
Country: China
ProdList: 550
Advantage: 58

Beijing Hezhicheng Chemical Products Co., Ltd

Tel: 18311365218 18311365218
Email: sales@toachem.com
Country: China
ProdList: 196
Advantage: 58

Jiujiang Huayao Biotechnology Co., Ltd.

Tel: 0792-13970278 13970278471
Email: 36516506@qq.com
Country: China
ProdList: 60
Advantage: 58

Shanghai Boyle Chemical Co., Ltd.

Tel
Fax: 86-21-57758967
Email: sales@boylechem.com
Country: China
ProdList: 2922
Advantage: 55

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

Energy Chemical

Tel: 021-021-58432009 400-005-6266
Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
ProdList: 44801
Advantage: 61

Wuhan Chemwish Technology Co., Ltd

Tel: 86-027-67849912
Fax: 86-027-87531808
Email: sales@chemwish.com
Country: China
ProdList: 35896
Advantage: 56

Adamas Reagent, Ltd.

Tel: 400-6009262 16621234537
Fax: 021-64823266
Email: chenyj@titansci.com
Country: China
ProdList: 14101
Advantage: 59

More

Less

View Lastest Price from 4,5-Diiodo-1H-imidazole manufacturers

Chongqing Soarwin Technology Co., Ltd

Product: 4,5-Diiodo-1H-imidazole 15813-09-9
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 20 tons
Release date: 2025-05-12

Hebei Ganmiao New material Technology Co., LTD

Product: 4,5-Diiodo-1H-imidazole 15813-09-9
Price: US $15.00-9.00/kg
Min. Order: 1kg
Purity: 99.9%
Supply Ability: 50ton
Release date: 2024-06-11

Hubei Chuyan Biopharmaceutical Co., Ltd

Product: 4,5-Diiodo-1H-imidazole 15813-09-9
Price: US $50.00/kg
Min. Order: 1kg
Purity: 99.5%
Supply Ability: 20 tons
Release date: 2024-03-29

15813-09-9, 4,5-Diiodo-1H-imidazoleRelated Search:

Levamisole hydrochloride Levamisole Mizolastine Mebendazole 1,1'-Carbonyldiimidazole Imidazole Midazolam 2,4,5-Triiodoimidazole 1-Methyl-4,5-diiodo-1h-imidazole N,N-Dimethyl 4,5-Diiodo-1H-imidazole-1-sulphonamide,N,N-DIMETHYL 4,5-DIIODO-1H-IMIDAZOLE-1-SULFONAMIDE 4,5-Diiodo-2-methyl-1H-imidazole 4,5-Dibromo-1H-imidazole 2,4-DIIODO-1H-IMIDAZOLE 4,5-Diiodo-1H-imidazole 1-[(benzyloxy)methyl]-4,5-diiodo-1H-imidazole 2,5-DIIODO-1H-IMIDAZOLE 2-CYCLOHEXYL-4,5-DIIODO-1H-IMIDAZOLE 1-(3-FLUOROBENZYL)-4,5-DIIODO-2-METHYL-1H-IMIDAZOLE

4,5-DIIODO-1H-IMIDAZOLE

4,5-DIIODOIMIDAZOLE

4,5-Diiodo-1H-imidazole 98%

1H-Imidazole, 4,5-diiodo-

Diiodo 1h Imidazole?

4,5-Diiodo-1H-imidazole ISO 9001：2015 REACH

4,5-triiodo-1H-imidazole

15813-09-9

C3H2I2N2

Halides

Imidazoles & Benzimidazoles

Miscellaneous

Imidazoles & Benzimidazoles

blocks

Imidazoles

Iodides