3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid methyl ester

Product Name: 3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid methyl ester
CAS No.: 40361-79-3
Chemical Name: 3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid methyl ester
Synonyms: 3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid;methyl 1-methyl-2-nitro-imidazole-5-carboxylate;Methyl 3-methyl-2-nitro-3H-imidazole-4-carboxylate;3-methyl-2-nitro-4-imidazolecarboxylic acid methyl ester;3-METHYL-2-NITRO-3H-IMIDAZOLE-4-CARBOXYLIC ACID METHYL ESTER;1H-Imidazole-5-carboxylic acid, 1-methyl-2-nitro-, methyl ester
CBNumber: CB7380732
Molecular Formula: C6H7N3O4
Formula Weight: 185.14
MOL File: 40361-79-3.mol

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3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid methyl ester Property

Boiling point:: 374.6±34.0 °C(Predicted)
Density: 1.49±0.1 g/cm3(Predicted)
storage temp.: 2-8°C
pka: -1.69±0.25(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M223753
Product name: Methyl3-Methyl-2-nitro-3H-imidazole-4-carboxylate
Packaging: 50mg
Price: $110
Updated: 2021/12/16

AK Scientific

Product number: 5424AB
Product name: Methyl3-methyl-2-nitro-3H-imidazole-4-carboxylate
Packaging: 250mg
Price: $399
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0087308
Product name: 3-METHYL-2-NITRO-3H-IMIDAZOLE-4-CARBOXYLIC ACID METHYL ESTER
Purity: 95.00%
Packaging: 1G
Price: $1173.94
Updated: 2021/12/16

J&W Pharmlab

Product number: 40R0044
Product name: 3-Methyl-2-nitro-3H-imidazole-4-carboxylicacidmethylester
Purity: 97%
Packaging: 5g
Price: $1390
Updated: 2021/12/16

Chemenu

Product number: CM186759
Product name: 3-Methyl-2-nitro-3H-imidazole-4-carboxylicacidmethylester
Purity: 97%
Packaging: 1g
Price: $439
Updated: 2021/12/16

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3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid methyl ester Chemical Properties,Usage,Production

Synthesis

1-methyl-2-nitro-1H-imidazole-5-carboxylic acid methyl ester 1c (50g, 0.27mol) was dissolve in 500mL tetrahydrofuran, followed by dropwise add methanol (13g, 0.4mol, 1.5eq) at 0 ℃. A solution of lithium hydride in tetrahydrofuran (2M, 202 mL, 1.5 eq) was added, and the reaction was incubated at 0 ℃ for 1 hour. The reaction solution was quenched by adding 500 mL of water, and extracted with ethyl acetate (500 mL × 3). The organic phases were combined, dried over anhydrous sodium sulfate, filtered, and concentrated under reduced pressure. The residue was added with dichloromethane (200 mL) and filtered to obtain 3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid methyl ester(31 g, 0.2 mol, yellow solid), yield: 73%.

3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid methyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid methyl ester Suppliers

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40361-79-3, 3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid methyl esterRelated Search:

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methyl 1-methyl-2-nitro-imidazole-5-carboxylate

3-methyl-2-nitro-4-imidazolecarboxylic acid methyl ester

3-Methyl-2-nitro-3H-imidazole-4-carboxylic acid

40361-79-3