1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYL-1,3-PROPANEDIONE
- Product Name
- 1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYL-1,3-PROPANEDIONE
- CAS No.
- 29976-82-7
- Chemical Name
- 1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYL-1,3-PROPANEDIONE
- Synonyms
- 2-(2-Hydroxy-5-methylbenzoyl)acetophenone;1-(2-hydroxy-5-methylphenyl)-3-phenyl-1,3-propane;1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYL-1,3-PROPANEDIONE;1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYLPROPANE-1,3-DIONE;1,3-Propanedione, 1-(2-hydroxy-5-methylphenyl)-3-phenyl-;1-(2-HYDROXY-5-METHYLPHENYL)3-PHENYL-1,3-PROPANEDIONE 97%;1-(2-Hydroxy-5-methylphenyl)-3-phenyl-1,3-propanedione,97%;JRH-02803, 1-(2-Hydroxy-5-methylphenyl)-3-phenylpropane-1,3-dione, 97%
- CBNumber
- CB7438686
- Molecular Formula
- C16H14O3
- Formula Weight
- 254.28
- MOL File
- 29976-82-7.mol
1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYL-1,3-PROPANEDIONE Property
- Melting point:
- 92-94 °C(lit.)
- Boiling point:
- 437.3±35.0 °C(Predicted)
- Density
- 1.201±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 7.97±0.43(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 1388AL
- Product name
- 1-(2-Hydroxy-5-methylphenyl)-3-phenyl-1,3-propanedione
- Packaging
- 250mg
- Price
- $157
- Updated
- 2021/12/16
- Product number
- COR0000701
- Product name
- 1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYLPROPANE-1,3-DIONE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1030.84
- Updated
- 2021/12/16
- Product number
- 1388AL
- Product name
- 1-(2-Hydroxy-5-methylphenyl)-3-phenyl-1,3-propanedione
- Packaging
- 10g
- Price
- $2328
- Updated
- 2021/12/16
- Product number
- COR0000701
- Product name
- 1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYLPROPANE-1,3-DIONE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $4244.63
- Updated
- 2021/12/16
- Product number
- COR0000701
- Product name
- 1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYLPROPANE-1,3-DIONE
- Purity
- 95.00%
- Packaging
- 10G
- Price
- $7882.88
- Updated
- 2021/12/16
1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYL-1,3-PROPANEDIONE Chemical Properties,Usage,Production
Chemical Properties
yellow crystalline powder or needles
Synthesis
4010-19-9
29976-82-7
2-Benzoyloxy-5-methylacetophenone (I) (5 g, 19.6 mmol) was reacted with 15 g of powdered hot KOH in 25 ml of pyridine and heated at 100 °C for 30 min. After completion of the reaction, the reaction mixture was slowly poured into pre-cooled and acidified (6N HCl) ice water. Subsequently, the precipitated yellow precipitate was collected by filtration. The resulting solid residue was dried under vacuum. The crude product 1-(2-hydroxy-5-methylphenyl)-3-phenylpropane-1,3-dione (II) was purified by recrystallization from petroleum ether, resulting in yellow bright plate-like crystals. Yield: 75%; mass of isolated product: 3.73 g; melting point: 95 °C (literature value: 94 °C [34]).
References
[1] Journal of the Indian Chemical Society, 2006, vol. 83, # 8, p. 835 - 837
[2] European Journal of Medicinal Chemistry, 2014, vol. 73, p. 195 - 209
[3] Chemistry Letters, 2007, vol. 36, # 4, p. 522 - 523
[4] Journal of Organic Chemistry, 1991, vol. 56, # 26, p. 7292 - 7297
[5] Journal of the Indian Chemical Society, 1986, vol. 63, p. 851 - 853
1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYL-1,3-PROPANEDIONE Preparation Products And Raw materials
Raw materials
Preparation Products
1-(2-HYDROXY-5-METHYLPHENYL)-3-PHENYL-1,3-PROPANEDIONE Suppliers
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