2-PHENYL-ETHANESULFONYL CHLORIDE
- Product Name
- 2-PHENYL-ETHANESULFONYL CHLORIDE
- CAS No.
- 4025-71-2
- Chemical Name
- 2-PHENYL-ETHANESULFONYL CHLORIDE
- Synonyms
- Benzeneethanesulfonyl chloride;2-PHENYL-ETHANESULFONYL CHLORIDE;2-phenylethane-1-sulfonyl chloride;2-Phenyl-ethanesulfonyl chloride ,95%
- CBNumber
- CB7444803
- Molecular Formula
- C8H9ClO2S
- Formula Weight
- 204.67
- MOL File
- 4025-71-2.mol
2-PHENYL-ETHANESULFONYL CHLORIDE Property
- Melting point:
- 32-33 °C
- Boiling point:
- 121-123 °C(Press: 3 Torr)
- Density
- 1.323±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- Appearance
- White to light yellow <32°C Solid,>33°C Liquid
- InChI
- InChI=1S/C8H9ClO2S/c9-12(10,11)7-6-8-4-2-1-3-5-8/h1-5H,6-7H2
- InChIKey
- LKFNLHZZPHHFEC-UHFFFAOYSA-N
- SMILES
- C1(CCS(Cl)(=O)=O)=CC=CC=C1
Safety
- RIDADR
- 1759
- HazardClass
- IRRITANT
- PackingGroup
- Ⅲ
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P321Specific treatment (see … on this label).
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B521345
- Product name
- 2-PhenylethanesulfonylChloride
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B521345
- Product name
- 2-PhenylethanesulfonylChloride
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 034526
- Product name
- 2-Phenyl-ethanesulfonyl chloride
- Packaging
- 500mg
- Price
- $29
- Updated
- 2021/12/16
- Product number
- 034526
- Product name
- 2-Phenyl-ethanesulfonyl chloride
- Packaging
- 1g
- Price
- $44
- Updated
- 2021/12/16
- Product number
- W6072
- Product name
- 2-Phenyl-ethanesulfonylchloride
- Packaging
- 1g
- Price
- $108
- Updated
- 2021/12/16
2-PHENYL-ETHANESULFONYL CHLORIDE Chemical Properties,Usage,Production
Synthesis
4410-99-5
4025-71-2
Example 15 Synthesis of 2-phenylethanesulfonyl chloride: N-chlorosuccinimide (534 mg, 4.00 mmol) was dissolved in a 2M HCl-CH3CN mixed solvent (267.4 μL - 1.34 mL, 3v/w volume relative to N-chlorosuccinimide). To this solution, a CH3CN solution (267.4 μL, 0.5 v/w relative to the volume of N-chlorosuccinimide) of 2-phenylethanethiol (134 μL, 1.00 mmol) was slowly added at 10 °C. After 30 min of reaction, ether was added to the reaction mixture, followed by three extractions with brine. The organic layers were combined, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 2-phenylethanesulfonyl chloride (195.5 mg, 95.4% yield). The product was characterized by 1H NMR (300 MHz, CDCl3): δ 7.43-7.27 (m, 5H), 3.98-3.92 (m, 3H), 3.41-3.35 (m, 1H).
References
[1] Bioorganic and Medicinal Chemistry Letters, 2002, vol. 12, # 8, p. 1181 - 1184
[2] Patent: US2015/329533, 2015, A1. Location in patent: Paragraph 0147; 0148
[3] Advanced Synthesis and Catalysis, 2015, vol. 357, # 18, p. 3825 - 3830
[4] Journal of Medicinal Chemistry, 2016, vol. 59, # 7, p. 3183 - 3203
[5] Journal of the American Chemical Society, 1991, vol. 113, # 6, p. 2259 - 2263
2-PHENYL-ETHANESULFONYL CHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
2-PHENYL-ETHANESULFONYL CHLORIDE Suppliers
- Tel
- 0371-88888888 272369594
- Fax
- QQ:272369594
- 2723695949@qq.com
- Country
- China
- ProdList
- 4960
- Advantage
- 50
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 86-027-67849912
- Fax
- 86-027-87531808
- sales@chemwish.com
- Country
- China
- ProdList
- 35896
- Advantage
- 56
- Tel
- 0573-85285100 18627885956
- Fax
- 0573-85285100
- isenchem@163.com
- Country
- China
- ProdList
- 9310
- Advantage
- 66
- Tel
- 010-59484199 18611897322
- sales@eternalchem.com
- Country
- China
- ProdList
- 4383
- Advantage
- 60
- Tel
- 027-86697669 13986148687
- Fax
- 86-027-86697669
- sales@tcaschem.com
- Country
- China
- ProdList
- 3993
- Advantage
- 55
- Tel
- +86-21-60341587
- Fax
- +86-21-61294319
- sales@topbiochem.com
- Country
- China
- ProdList
- 6175
- Advantage
- 58
- Tel
- +86-28-85122536 85324413
- Fax
- +86-28-85326443
- market@astatech.cn
- Country
- China
- ProdList
- 8026
- Advantage
- 55
- Tel
- 400-164-7117 13681763483
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 42446
- Advantage
- 60
- Tel
- 021-021-56795766
- Fax
- +86-21-56795266
- sales@worldyachem.com
- Country
- China
- ProdList
- 9476
- Advantage
- 58
View Lastest Price from 2-PHENYL-ETHANESULFONYL CHLORIDE manufacturers
- Product
- 2-PHENYL-ETHANESULFONYL CHLORIDE 4025-71-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1000KGS
- Release date
- 2019-12-25