CHEMBRDG-BB 4004130

Product Name: CHEMBRDG-BB 4004130
CAS No.: 30433-92-2
Chemical Name: CHEMBRDG-BB 4004130
Synonyms: AKOS ISYA01283;RARECHEM AN KA 0153;CHEMBRDG-BB 4004130;UKRORGSYN-BB BBV-182415;2-(5-METHYL-2-THIENYL)ETHANAMINE;2-Thiopheneethanamine, 5-methyl-;2-(5-methylthiophen-2-yl)ethanamine;2-(5-METHYL-THIOPHEN-2-YL)-ETHYLAMINE;2-(5-methyl-2-thienyl)ethanamine(SALTDATA: FREE)
CBNumber: CB7496059
Molecular Formula: C7H11NS
Formula Weight: 141.23
MOL File: 30433-92-2.mol

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CHEMBRDG-BB 4004130 Property

storage temp.: 2-8°C(protect from light)

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Safety

HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M222843
Product name: 2-(5-Methyl-2-thienyl)ethanamine
Packaging: 10mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M222843
Product name: 2-(5-Methyl-2-thienyl)ethanamine
Packaging: 50mg
Price: $90
Updated: 2021/12/16

Matrix Scientific

Product number: 033432
Product name: 2-(5-Methyl-thiophen-2-yl)-ethylamine
Packaging: 500mg
Price: $200
Updated: 2021/12/16

AK Scientific

Product number: 9610AD
Product name: 2-(5-Methyl-thiophen-2-yl)-ethylamine
Packaging: 500mg
Price: $320
Updated: 2021/12/16

Apolloscientific

Product number: OR322779
Product name: 2-(5-Methyl-2-thienyl)ethanamine
Packaging: 500mg
Price: $356
Updated: 2021/12/16

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CHEMBRDG-BB 4004130 Chemical Properties,Usage,Production

Synthesis

117693-20-6

30433-92-2

b) Step 2: Synthesis of 2-(5-methyl-2-thienyl)ethylamine A solution of 6.9 g (175 mmol) of 2-methyl-5-((E)-2-nitrovinyl)-thiophene dissolved in 150 mL of diethyl ether was slowly added dropwise to a suspension of 6.9 g (40.78 mmol) of LiAlH4 in 70 mL of ethyl ether under nitrogen protection, controlling the temperature to 20 to 25 °C. After dropwise addition, the reaction mixture was heated to reflux for 5 hours. After completion of the reaction, the mixture was cooled to 0 °C and the reaction was quenched by sequentially adding 28 mL of water and 7 mL of 5N NaOH solution. The white solid was removed by filtration and the filter cake was washed with ethyl acetate. The filtrates were combined and concentrated under reduced pressure to remove the solvent. The residue was purified by distillation under reduced pressure to give 4.98 g (86% yield) of the target compound 2-(5-methyl-2-thienyl)ethylamine as a colorless liquid.MS (m/e): 142.2 (MH+).

References

[1] Patent: US2008/249125, 2008, A1. Location in patent: Page/Page column 11-12
[2] Journal of Organic Chemistry, 1950, vol. 15, p. 807,810

CHEMBRDG-BB 4004130 Preparation Products And Raw materials

Raw materials

Preparation Products

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CHEMBRDG-BB 4004130 Suppliers

China 18 Germany 1 India 2 United Kingdom 1 United States 6 Global 28

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30433-92-2, CHEMBRDG-BB 4004130Related Search:

2-[5-(1-AZEPANYLMETHYL)-2-THIENYL]ETHANAMINE 2-[5-(4-FLUOROBENZOYL)-2-THIENYL]ACETAMIDE 2-[5-(2,4-DICHLOROBENZOYL)-2-THIENYL]ACETAMIDE 2-[5-(CHLOROACETYL)THIEN-2-YL]ACETAMIDE 2-[5-(1-PYRROLIDINYLMETHYL)-2-THIENYL]ETHANAMINE 2-(5-[(DIETHYLAMINO)METHYL]-2-THIENYL)ETHANAMINE RARECHEM AL BW 1843 2-[5-(2-THIENYLCARBONYL)-2-THIENYL]ACETAMIDE 2-(5-BENZOYL-2-THIENYL)ACETAMIDE 2-[5-(1-PIPERIDINYLMETHYL)-2-THIENYL]ETHYLAMINE 2-CHLORO-1-[5-(2-MORPHOLIN-4-YL-2-OXOETHYL)THIEN-2-YL]ETHANONE 2-[5-(4-MORPHOLINYLMETHYL)-2-THIENYL]ETHYLAMINE 2-[5-(4-CHLOROBENZOYL)-2-THIENYL]ACETAMIDE 2-[5-(2-FLUOROBENZOYL)-2-THIENYL]ACETAMIDE N-([5-(2-AMINOETHYL)-2-THIENYL]METHYL)-N,N-DIMETHYLAMINE 2-amino-3-(5-ethylthien-2-yl)propanoic acid 2-[5-(4-CHLOROBENZOYL)-2-THIENYL]ETHANETHIOAMIDE

CHEMBRDG-BB 4004130

RARECHEM AN KA 0153

2-(5-METHYL-2-THIENYL)ETHANAMINE

2-(5-METHYL-THIOPHEN-2-YL)-ETHYLAMINE

AKOS ISYA01283

UKRORGSYN-BB BBV-182415

2-(5-methyl-2-thienyl)ethanamine(SALTDATA: FREE)

2-(5-methylthiophen-2-yl)ethanamine

2-Thiopheneethanamine, 5-methyl-

30433-92-2