2,6-DIMETHYL-5-IODO-4(3H)-PYRIMIDONE
- Product Name
- 2,6-DIMETHYL-5-IODO-4(3H)-PYRIMIDONE
- CAS No.
- 83410-37-1
- Chemical Name
- 2,6-DIMETHYL-5-IODO-4(3H)-PYRIMIDONE
- Synonyms
- 2,6-DIMETHYL-5-IODO-4(3H)-PYRIMIDONE;5-iodo-2,6-dimethyl-4(3H)-Pyrimidinone;5-Iodo-2,6-diMethyl-1H-pyriMidin-4-one;5-Iodo-2,6-dimethylpyrimidin-4(3h)-one;4(3H)-Pyrimidinone, 5-iodo-2,6-dimethyl-;5-iodo-2,6-dimethyl-4-pyrimidinol(SALTDATA: FREE)
- CBNumber
- CB7726358
- Molecular Formula
- C6H7IN2O
- Formula Weight
- 250.04
- MOL File
- 83410-37-1.mol
2,6-DIMETHYL-5-IODO-4(3H)-PYRIMIDONE Property
- Melting point:
- 196-199 °C
- Boiling point:
- 254.9±43.0 °C(Predicted)
- Density
- 2.03±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- pka
- 8.33±0.50(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- HCH0261204
- Product name
- 5-IODO-2,6-DIMETHYLPYRIMIDIN-4-OL
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.67
- Updated
- 2021/12/16
- Product number
- BB-4029374
- Product name
- 5-iodo-2,6-dimethyl-4-pyrimidinol
- Purity
- 95%
- Packaging
- 250mg
- Price
- $99
- Updated
- 2021/12/16
- Product number
- 10-1689
- Product name
- 5-Iodo-2,6-dimethyl-pyrimidin-4-ol
- Purity
- >95%
- Packaging
- 1g
- Price
- $175
- Updated
- 2021/12/16
- Product number
- CC00-2031A
- Product name
- 5-Iodo-2,6-dimethyl-1H-pyrimidin-4-one
- Purity
- ＞96%
- Packaging
- 1g
- Price
- $195
- Updated
- 2021/12/16
- Product number
- 10-1689
- Product name
- 5-Iodo-2,6-dimethyl-pyrimidin-4-ol
- Purity
- >95%
- Packaging
- 5g
- Price
- $625
- Updated
- 2021/12/16
2,6-DIMETHYL-5-IODO-4(3H)-PYRIMIDONE Chemical Properties,Usage,Production
Synthesis
6622-92-0
83410-37-1
Step A: 2,6-Dimethylpyrimidin-4-ol (5.0 g, 40 mmol) was dissolved in aqueous sodium hydroxide solution (50 mL, 1 M, 50 mmol). Iodine (10.2 g, 40 mmol) was subsequently added to this solution. The reaction mixture was slowly warmed to 80 °C and stirred continuously for 2 hours. Upon completion of the reaction, the mixture was cooled to room temperature and the pH was adjusted with acetic acid to about 6. At this point, a precipitate appeared in the reaction mixture and the precipitate was collected by filtration. The resulting solid was washed with deionized water and dried to give the target product 5-iodo-2,6-dimethylpyrimidin-4-ol (6.51 g, 65% yield). Mass spectrometry analysis showed m/z 251.2 [M + H]+.
References
[1] Patent: US9617268, 2017, B2. Location in patent: Page/Page column 398
[2] Journal of Medicinal Chemistry, 1998, vol. 41, # 22, p. 4251 - 4260
[3] Tetrahedron, 2007, vol. 63, # 9, p. 1931 - 1936
[4] Patent: US5466692, 1995, A
[5] Patent: US2012/95031, 2012, A1. Location in patent: Page/Page column 160
2,6-DIMETHYL-5-IODO-4(3H)-PYRIMIDONE Preparation Products And Raw materials
Raw materials
Preparation Products
View Lastest Price from 2,6-DIMETHYL-5-IODO-4(3H)-PYRIMIDONE manufacturers
- Product
- 2,6-DIMETHYL-5-IODO-4(3H)-PYRIMIDONE 83410-37-1
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98
- Supply Ability
- 10000KGS
- Release date
- 2025-11-05