ChemicalBook > CAS DataBase List > 3-CHLORO-4-ISOPROPOXY-BENZOIC ACID

3-CHLORO-4-ISOPROPOXY-BENZOIC ACID

Product Name: 3-CHLORO-4-ISOPROPOXY-BENZOIC ACID
CAS No.: 213598-07-3
Chemical Name: 3-CHLORO-4-ISOPROPOXY-BENZOIC ACID
Synonyms: Ozanimod Impurity 51;3-CHLORO-4-ISOPROPOXY-BENZOIC ACID;3-chloro-4-propan-2-yloxybenzoic Acid;3-Chloro-4-(1-methylethoxy)benzoic acid;Benzoic acid, 3-chloro-4-(1-methylethoxy)-
CBNumber: CB7841404
Molecular Formula: C10H11ClO3
Formula Weight: 214.65
MOL File: 213598-07-3.mol

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3-CHLORO-4-ISOPROPOXY-BENZOIC ACID Property

storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: C598313
Product name: 3-Chloro-4-isopropoxybenzoicAcid
Packaging: 100mg
Price: $65
Updated: 2021/12/16

ChemScene

Product number: CS-M0439
Product name: 3-chloro-4-isopropoxybenzoicacid
Packaging: 1g
Price: $70
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC150050
Product name: 3-Chloro-4-isopropoxybenzoicacid
Packaging: 250mg
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC150050
Product name: 3-Chloro-4-isopropoxybenzoicacid
Packaging: 500mg
Price: $100
Updated: 2021/12/16

AK Scientific

Product number: 0859AB
Product name: 3-Chloro-4-isopropoxybenzoicacid
Packaging: 1g
Price: $158
Updated: 2021/12/16

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3-CHLORO-4-ISOPROPOXY-BENZOIC ACID Chemical Properties,Usage,Production

Synthesis

916596-04-8

213598-07-3

Step 2: Synthesis of 3-chloro-4-isopropoxybenzoic acid (34). To a stirred solution of 3-chloro-4-isopropoxybenzonitrile (33, 57 g, 291 mmol) in ethanol (EtOH, 120 mL) was added an aqueous 12% potassium hydroxide (KOH) solution (300 mL), and the reaction mixture was heated to 100 °C and kept for 3 h. The reaction was carried out with the addition of aqueous potassium hydroxide (KOH). Upon completion of the reaction, the mixture was cooled to room temperature and acidified with hydrochloric acid (HCl) to pH 5. A yellow solid precipitated during the acidification process, which was collected by filtration, washed with water and dried. The resulting solid was mixed with hexane, stirred for 5 minutes and decanted to remove the hexane. The process was repeated once, and the solid was resuspended in hexane, filtered, and washed with hexane to give 3-chloro-4-isopropoxybenzoic acid (34) as a white solid (45 g, 72% yield).

References

[1] Patent: WO2017/4609, 2017, A1. Location in patent: Paragraph 0277
[2] Patent: WO2017/4608, 2017, A1. Location in patent: Paragraph 0153

3-CHLORO-4-ISOPROPOXY-BENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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3-CHLORO-4-ISOPROPOXY-BENZOIC ACID Suppliers

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213598-07-3, 3-CHLORO-4-ISOPROPOXY-BENZOIC ACIDRelated Search:

3-CHLORO-4-ISOPROPOXY-5-METHOXYBENZOIC ACID METHYL 3-CHLORO-4-ISOPROPOXYBENZOATE AKOS B029174 3-CHLORO-4-ISOPROPOXY-BENZOIC ACID

3-chloro-4-propan-2-yloxybenzoic Acid

3-CHLORO-4-ISOPROPOXY-BENZOIC ACID

Benzoic acid, 3-chloro-4-(1-methylethoxy)-

3-Chloro-4-(1-methylethoxy)benzoic acid

Ozanimod Impurity 51

213598-07-3