6-methoxy-2-methylbenzoxazole

Product Name: 6-methoxy-2-methylbenzoxazole
CAS No.: 23999-64-6
Chemical Name: 6-methoxy-2-methylbenzoxazole
Synonyms: 6-methoxy-2-methylbenzoxazole;6-Methoxy-2-methyl-benzooxazole;Benzoxazole, 6-methoxy-2-methyl-;6-Methoxy-2-Methylbenzo[d]oxazole;6-methoxy-2-methyl-1,3-benzoxazole
CBNumber: CB7894970
Molecular Formula: C9H9NO2
Formula Weight: 163.17
MOL File: 23999-64-6.mol

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6-methoxy-2-methylbenzoxazole Property

Melting point:: 51.5-53 °C(Solv: ligroine (8032-32-4))
Boiling point:: 250.0±13.0 °C(Predicted)
Density: 1.166±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 1.06±0.30(Predicted)
InChI: InChI=1S/C9H9NO2/c1-6-10-8-4-3-7(11-2)5-9(8)12-6/h3-5H,1-2H3
InChIKey: IMRVVUQHPUZLSC-UHFFFAOYSA-N
SMILES: O1C2=CC(OC)=CC=C2N=C1C

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M264453
Product name: 6-Methoxy-2-methylbenzo[D]oxazole
Packaging: 50mg
Price: $265
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: SDY0000304
Product name: 6-METHOXY-2-METHYLBENZOXAZOLE
Purity: 95.00%
Packaging: 5MG
Price: $543
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: SDY0000304
Product name: 6-METHOXY-2-METHYLBENZOXAZOLE
Purity: 95.00%
Packaging: 1G
Price: $1455.3
Updated: 2021/12/16

Chemenu

Product number: CM124643
Product name: 6-methoxy-2-methylbenzo[d]oxazole
Purity: 95%
Packaging: 1g
Price: $837
Updated: 2021/12/16

Alichem

Product number: 23999646
Product name: 6-Methoxy-2-methylbenzo[d]oxazole
Packaging: 5g
Price: $1400.84
Updated: 2021/12/16

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6-methoxy-2-methylbenzoxazole Chemical Properties,Usage,Production

Synthesis

552-41-0

51864-08-5

23999-64-6

GENERAL METHOD: 2-hydroxyacetophenone 4a (1.0 g, 7.4 mmol), acetohydroxamic acid (0.83 g, 11.0 mmol), acetonitrile (3 ml) and concentrated sulfuric acid (0.2 ml) were added to a 10 ml pressure tube. The mixture was heated in a microwave reactor (CEM Discover, 360W, 80°C, 25 psi) for 8 min. After completion of the reaction, the mixture was diluted with ethyl acetate (3 ml) and saturated sodium bicarbonate solution (5 ml) was added dropwise to neutralize it. Subsequently, the mixture was extracted with ethyl acetate (2 x 10 ml). The organic layers were combined, washed with saturated sodium chloride solution and dried with anhydrous sodium sulfate. After concentration under reduced pressure, the mixture was purified by conventional column chromatography (silica gel 60-120 mesh, eluent ethyl acetate/hexane: 1:9) to afford benzoxazole 5a (0.67 g, 70%) as a yellow oil and 2-hydroxyacetophenone oxime 6a (68 mg, 6%, melting point 104-107°C) as a white powder.

References

[1] Tetrahedron Letters, 2011, vol. 52, # 46, p. 6103 - 6107

6-methoxy-2-methylbenzoxazole Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-methoxy-2-methylbenzoxazole manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: Benzoxazole,6-methoxy-2-methyl- 23999-64-6
Price: US $8.80-2.20/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-06-27

Career Henan Chemical Co

Product: 6-methoxy-2-methyl-1,3-benzoxazole 23999-64-6
Price: US $2.00/KG
Min. Order: 1KG
Purity: ≥98%
Supply Ability: 100kg
Release date: 2019-12-20

23999-64-6, 6-methoxy-2-methylbenzoxazoleRelated Search:

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23999-64-6