ChemicalBook > CAS DataBase List > 2-Amino-5-bromonicotinaldehyde

2-Amino-5-bromonicotinaldehyde

Product Name: 2-Amino-5-bromonicotinaldehyde
CAS No.: 206997-15-1
Chemical Name: 2-Amino-5-bromonicotinaldehyde
Synonyms: 2-AMino-5-broMonicotildehyde;2-Amino-5-bromonicotinaldehyde;2-Amino-5-bromonicotinaldehyde 98%;2-aMino-5-broMo-3-pyridinecarbaldehyde;2-AMino-5-broMo-pyridine-3-carbaldehyde;2-AMINO-5-BROMOPYRIDINE-3-CARBOXALDEHYDE;3-Pyridinecarboxaldehyde, 2-aMino-5-broMo-;2-Amino-5-bromopyridine-3-carboxaldehyde, 2-Amino-5-bromo-3-formylpyridine
CBNumber: CB7957776
Molecular Formula: C6H5BrN2O
Formula Weight: 201.02
MOL File: 206997-15-1.mol

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2-Amino-5-bromonicotinaldehyde Property

Melting point:: 167-169
Boiling point:: 300.5±42.0 °C(Predicted)
Density: 1.782±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 2.74±0.49(Predicted)
Appearance: Light yellow to yellow Solid

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Safety

Hazard Codes: Xi
RIDADR: UN 2811 6.1 / PGIII
HazardClass: IRRITANT
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Usbiological

Product number: 415236
Product name: 2-Amino-5-bromonicotinaldehyde
Packaging: 100mg
Price: $305
Updated: 2021/12/16

Matrix Scientific

Product number: 046553
Product name: 2-Amino-5-bromonicotinaldehyde
Purity: >95%
Packaging: 500mg
Price: $143
Updated: 2021/12/16

AK Scientific

Product number: 7045AD
Product name: 2-Amino-5-bromonicotinaldehyde
Packaging: 1g
Price: $184
Updated: 2021/12/16

Matrix Scientific

Product number: 046553
Product name: 2-Amino-5-bromonicotinaldehyde
Purity: >95%
Packaging: 5g
Price: $550
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H30-9-X3
Product name: 2-Amino-5-bromonicotinaldehyde
Packaging: 1g
Price: $199
Updated: 2021/12/16

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2-Amino-5-bromonicotinaldehyde Chemical Properties,Usage,Production

Synthesis

7521-41-7

206997-15-1

General procedure for the synthesis of 2-amino-5-bromonicotinaldehyde from 2-amino-3-pyridinecarboxaldehyde: A. To a solution of 2-aminopyridine-3-carbaldehyde (10.1 g, 81.0 mmol) in acetonitrile (150 mL) was added N-bromosuccinimide (15.1 g, 84.0 mmol). The reaction mixture was stirred under reflux conditions for 2 hours. After completion of the reaction, it was cooled to room temperature and the reaction mixture was filtered. The collected solid was washed with methanol and subsequently dried under vacuum to afford 2-amino-5-bromopyridine-3-carbaldehyde as a brown solid in 79% yield (12.9 g). 1H NMR (400 MHz, CDCl3): δ 9.81 (s, 1H), 8.30 (d, J = 2.4 Hz, 1H), 7.89 (d, J = 2.4 Hz, 1H), 6.78 (br s, 2H).

References

[1] Patent: WO2015/81257, 2015, A2. Location in patent: Page/Page column 61-62
[2] Journal of Polymer Science, Part A: Polymer Chemistry, 2011, vol. 49, # 19, p. 4204 - 4212
[3] Journal of Medicinal Chemistry, 2014, vol. 57, # 21, p. 8777 - 8791
[4] Patent: WO2013/82756, 2013, A1. Location in patent: Page/Page column 21; 30-31
[5] Patent: WO2009/115788, 2009, A1. Location in patent: Page/Page column 54

2-Amino-5-bromonicotinaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Amino-5-bromonicotinaldehyde manufacturers

Career Henan Chemical Co

Product: 2-Amino-5-bromonicotinaldehyde 206997-15-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-11

206997-15-1, 2-Amino-5-bromonicotinaldehydeRelated Search:

2-Amino-5-bromonicotinic acid Methyl 2-amino-5-bromonicotinate 6-BROMOPYRIDO[2,3-D]PYRIMIDIN-4(1H)-ONE tert-Butyl 4-[5-bromo-3-(methoxycarbonyl)pyridin-2-yl]piperazine-1-carboxylate 2-AMINO-5-BROMO-6-METHYL NICOTINAMIDE 6-BROMOPYRIDO[2,3-D]PYRIMIDINE-2,4(1H,3H)-DIONE methyl 5-bromo-2-piperidinonicotinate 2-AMINO-5-BROMO-4-METHYL NICOTINAMIDE 5-bromo-2-piperidinonicotinic acid methyl 5-bromo-2-morpholinonicotinate 2-AMINO-6-BROMOPYRIDO[2,3-D]PYRIMIDIN-4(3H)-ONE 2-AMINO-5-BROMO-4-METHYL NICOTINIC ACID HCL ETHYL 2-AMINO-5-BROMONICOTINATE 2-Amino-5-bromonicotinaldehyde 5-BROMO-6-METHYL-2-METHYLAMINO-NICOTINIC ACID 8-BROMO-2-CHLORO-11-ETHYL-5-METHYL-5H-DIPYRIDO[3,2-B:2',3'-E][1,4]DIAZEPIN-6(11H)-ONE IFLAB-BB F2124-0030 IFLAB-BB F2124-0032

2-Amino-5-bromonicotinaldehyde

2-Amino-5-bromopyridine-3-carboxaldehyde, 2-Amino-5-bromo-3-formylpyridine

2-AMino-5-broMonicotildehyde

2-AMINO-5-BROMOPYRIDINE-3-CARBOXALDEHYDE

2-AMino-5-broMo-pyridine-3-carbaldehyde

3-Pyridinecarboxaldehyde, 2-aMino-5-broMo-

2-aMino-5-broMo-3-pyridinecarbaldehyde

2-Amino-5-bromonicotinaldehyde 98%

206997-15-1