5-Bromo-2-Chloroacetophenone

Product Name: 5-Bromo-2-Chloroacetophenone
CAS No.: 105884-19-3
Chemical Name: 5-Bromo-2-Chloroacetophenone
Synonyms: 1-(5-Bromo-2-chlorophenyl)ethan-1-one;-Bromo-2’-chloroacetophenone;1-(5-Bromo-2-chlorophenyl);5'-Bromo-2'-chloroacetophenone;5'-Bromo-2'-chloroacetophenone 99%;Ethanone, 1-(5-bromo-2-chlorophenyl)-;5′-Bromo-2′-chloroacetophenone, CAS 105884-19-3
CBNumber: CB81032983
Molecular Formula: C8H6BrClO
Formula Weight: 233.49
MOL File: 105884-19-3.mol

More

Less

5-Bromo-2-Chloroacetophenone Property

Boiling point:: 260℃
Density: 1.566
Flash point:: 111℃
storage temp.: Sealed in dry,Room Temperature
form: fused solid
color: Faint yellow

More

Less

Safety

HS Code: 2914790090

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

More

Less

N-Bromosuccinimide Price

TRC

Product number: B683558
Product name: 5''-Bromo-2''-chloroacetophenone
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Apolloscientific

Product number: OR3169
Product name: 5'-Bromo-2'-chloroacetophenone
Purity: 99%
Packaging: 5g
Price: $79
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2617-D-X3
Product name: 5'-Bromo-2'-chloroacetophenone
Packaging: 5G
Price: $93
Updated: 2021/12/16

AK Scientific

Product number: J90994
Product name: 5'-Bromo-2'-chloroacetophenone
Packaging: 1g
Price: $22
Updated: 2021/12/16

Apolloscientific

Product number: OR3169
Product name: 5'-Bromo-2'-chloroacetophenone
Purity: 99%
Packaging: 1g
Price: $26
Updated: 2021/12/16

More

Less

5-Bromo-2-Chloroacetophenone Chemical Properties,Usage,Production

Synthesis

749932-77-2

105884-19-3

General procedure for the synthesis of 1-(5-bromo-2-chlorophenyl)ethanone using 1-(5-bromo-2-chlorophenyl)ethanol as starting material: to a solution of 1-(5-bromo-2-chlorophenyl)ethanol (1.09 g, 4.6 mmol) in dichloromethane (20 mL) was added pyridinium dichromate (2.6 g, 6.94 mmol). The reaction mixture was stirred for 15 hours and then pyridinium dichromate (2.6 g, 6.94 mmol) was added again. After continued stirring for 24 hours, diatomaceous earth was added and the mixture was stirred for 20 minutes. The reaction mixture was filtered through a diatomaceous earth pad and the filter cake was washed with ether. The filtrates were combined and concentrated to give a brown oil. Purification of the crude product by fast silica gel column chromatography (eluent: hexane/ethyl acetate, 0% to 10% ethyl acetate gradient) afforded 1-(5-bromo-2-chlorophenyl)ethanone as a clear oil (0.92 g, 85% yield).1H NMR (400 MHz, CDCl3): δ 2.64 (s, 3H), 7.29 (d, J = 8.6 Hz, 1H) , 7.51 (dd, J = 8.6, 2.3 Hz, 1H), 7.66 (d, J = 2.3 Hz, 1H).

References

[1] Patent: WO2004/74270, 2004, A2. Location in patent: Page 363-364
[2] Patent: US2005/176701, 2005, A1. Location in patent: Page/Page column 177

5-Bromo-2-Chloroacetophenone Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

5-Bromo-2-Chloroacetophenone Suppliers

China 85 India 3 Switzerland 1 United Kingdom 5 United States 5 Global 99

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

Shanghai Harvest Chemical Industrial Co., Ltd.

Tel: 021-31038972,31038973 17321035817
Fax: +86-21-51385350
Email: sales@harvest-chem.com
Country: China
ProdList: 2816
Advantage: 64

Beijing Eternalchem Co,. Ltd.

Tel: 010-59484199 18611897322
Email: sales@eternalchem.com
Country: China
ProdList: 4383
Advantage: 60

Shanghai Topbiochem Technology Co., Ltd

Tel: 021-58170097
Email: info@topbiochem.com
Country: China
ProdList: 9510
Advantage: 58

9ding chemical ( Shanghai) Limited

Tel: 4009209199
Fax: 86-021-52271987
Email: sales@9dingchem.com
Country: China
ProdList: 18209
Advantage: 56

Aloespharm Co., Ltd.

Tel: 021-20960837
Fax: 021-20960837
Email: market@aloespharm.com
Country: China
ProdList: 1302
Advantage: 55

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

Changzhou Tianrui Pharmaceutical Technology Co., Ltd.

Tel: 0519-85386832 13382812559
Fax: 0519-85386832
Email: sales@cztrchem.com
Country: China
ProdList: 1185
Advantage: 56

Changzhou Anxuan Chemical, Co., Ltd.

Tel: 13912302692
Fax: 0519-88064678
Email: sales@anxuanchem.com
Country: China
ProdList: 4828
Advantage: 58

skychemical Co.Ltd

Tel: 021-20960837,QQ1332204249
Fax: 021-20960837
Email: sales@skychemical.com
Country: China
ProdList: 3341
Advantage: 55

More

Less

View Lastest Price from 5-Bromo-2-Chloroacetophenone manufacturers

Career Henan Chemical Co

Product: 5-Bromo-2-Chloroacetophenone 105884-19-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 97%
Supply Ability: 200kg
Release date: 2020-02-01

105884-19-3, 5-Bromo-2-ChloroacetophenoneRelated Search:

Potassium cyanate

1-(5-Bromo-2-chlorophenyl)ethan-1-one

1-(5-Bromo-2-chlorophenyl)

5'-Bromo-2'-chloroacetophenone 99%

Ethanone, 1-(5-bromo-2-chlorophenyl)-

-chloroacetophenone

-Bromo-2&rsquo

5'-Bromo-2'-chloroacetophenone

5′-Bromo-2′-chloroacetophenone, CAS 105884-19-3

105884-19-3

Aromatic Acetophenones & Derivatives (substituted)