ChemicalBook > CAS DataBase List > 2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTER

2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTER

Product Name: 2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTER
CAS No.: 63243-76-5
Chemical Name: 2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTER
Synonyms: ETHYL 2-AMINO-5-BROMOBENZOATE;2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTER;Benzoic acid, 2-aMino-5-broMo-, ethyl ester
CBNumber: CB8103329
Molecular Formula: C9H10BrNO2
Formula Weight: 244.09
MOL File: 63243-76-5.mol

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2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTER Property

Melting point:: 187 °C(Solv: ethanol (64-17-5))
Boiling point:: 301.2±22.0 °C(Predicted)
Density: 1.503±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 1.77±0.10(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: E899850
Product name: Ethyl2-Amino-5-bromobenzoate
Packaging: 50mg
Price: $60
Updated: 2021/12/16

Oakwood

Product number: 038708
Product name: Ethyl 2-Amino-5-bromobenzoate
Packaging: 1g
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: 3339AL
Product name: Ethyl2-amino-5-bromobenzoate
Packaging: 5g
Price: $151
Updated: 2021/12/16

Oakwood

Product number: 038708
Product name: Ethyl 2-Amino-5-bromobenzoate
Packaging: 5g
Price: $200
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0011065
Product name: 2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTER
Purity: 95.00%
Packaging: 1G
Price: $692.46
Updated: 2021/12/16

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2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTER Chemical Properties,Usage,Production

Synthesis

64-17-5

5794-88-7

63243-76-5

To a 100 mL three-necked round-bottomed flask was added 2-amino-5-bromobenzoic acid (5 g, 23.14 mmol, 1.00 equiv) and anhydrous ethanol (100 mL). Dry hydrogen chloride gas was passed to saturation and the reaction mixture was subsequently heated to reflux for 12 hours. Upon completion of the reaction, saturated sodium bicarbonate solution was slowly added to neutralize the reaction system. The solvent was removed by distillation under reduced pressure to give the crude product. The crude product was purified by fast column chromatography (silica gel, eluent ratio was adjusted according to the TLC results) to give ethyl 2-amino-5-bromobenzoate (2.5 g, 44% yield) as a yellow solid.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2009, vol. 19, # 19, p. 5746 - 5752
[2] Patent: WO2014/182951, 2014, A1. Location in patent: Paragraph 00281
[3] Bioorganic and Medicinal Chemistry Letters, 2007, vol. 17, # 23, p. 6481 - 6488
[4] Patent: EP1180514, 2002, A1. Location in patent: Example 75
[5] Journal of Organic Chemistry, 2018, vol. 83, # 3, p. 1154 - 1159

2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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63243-76-5, 2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTERRelated Search:

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ETHYL 2-AMINO-5-BROMOBENZOATE

2-AMINO-5-BROMO-BENZOIC ACID ETHYL ESTER

Benzoic acid, 2-aMino-5-broMo-, ethyl ester

63243-76-5

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