Benzonitrile, 5-acetyl-2-amino- (9CI)

Product Name: Benzonitrile, 5-acetyl-2-amino- (9CI)
CAS No.: 33720-71-7
Chemical Name: Benzonitrile, 5-acetyl-2-amino- (9CI)
Synonyms: Acetyl-2-aMinobenzonitrile;5-Acetyl-anthranilonitrile;4-aMino-3-cyanoacetophenone;5-Acetyl-2-aMinobenzonitrile;2-Amino-5-acetylbenzonitrile;4'-Amino-3'-cyanoacetophenone;Benzonitrile,5-acetyl-2-amino-;Benzonitrile, 5-acetyl-2-amino- (9CI)
CBNumber: CB81044182
Molecular Formula: C9H8N2O
Formula Weight: 160.17
MOL File: 33720-71-7.mol

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Benzonitrile, 5-acetyl-2-amino- (9CI) Property

Melting point:: 159-161°C
Boiling point:: 375℃
Density: 1.20
Flash point:: 180℃
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: Chloroform (Slightly), Methanol (Slightly, Heated)
form: Solid
pka: -0.62±0.10(Predicted)
color: Light Yellow to Dark Yellow
InChI: InChI=1S/C9H8N2O/c1-6(12)7-2-3-9(11)8(4-7)5-10/h2-4H,11H2,1H3
InChIKey: SJXQSPLLUXAJQJ-UHFFFAOYSA-N
SMILES: C(#N)C1=CC(C(C)=O)=CC=C1N

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Safety

HS Code: 29269090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: A168115
Product name: 5-Acetyl-2-aminobenzonitrile
Packaging: 1g
Price: $190
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA17059
Product name: 5-Acetyl-2-aminobenzonitrile
Packaging: 5G
Price: $250
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA17059
Product name: 5-Acetyl-2-aminobenzonitrile
Packaging: 500mg
Price: $50
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA17059
Product name: 5-Acetyl-2-aminobenzonitrile
Packaging: 1g
Price: $80
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA17059
Product name: 5-Acetyl-2-aminobenzonitrile
Packaging: 2g
Price: $130
Updated: 2021/12/16

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Benzonitrile, 5-acetyl-2-amino- (9CI) Chemical Properties,Usage,Production

Chemical Properties

Yellow Solid

Uses

Cimaterol intermediate.

Synthesis

544-92-3

97776-06-2

33720-71-7

b. Preparation of 3-cyano-4-aminoacetophenone: 3-iodo-4-aminoacetophenone prepared above was dissolved in 95 mL of N,N-dimethylformamide (DMF) and 20.9 g of cuprous cyanide (CuCN) was added. The reaction was stirred under reflux conditions for 6 hours and subsequently cooled to 100 °C. The reaction mixture was slowly poured into 2 L of ice water and continued to cool to room temperature. The precipitate was collected by filtration, air dried and extracted with tetrahydrofuran (THF). The extract was concentrated and the resulting solid was washed with ethanol, filtered again and dried to give a yellow crystalline product in 56.9% yield with a melting point of 150-152 °C.

References

[1] Patent: EP1439164, 2004, A1. Location in patent: Page 5
[2] Arzneimittel-Forschung/Drug Research, 1984, vol. 34, # 11 A, p. 1612 - 1624

Benzonitrile, 5-acetyl-2-amino- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Benzonitrile, 5-acetyl-2-amino- (9CI) Suppliers

Canada 1 China 62 Europe 1 India 2 Switzerland 1 United Kingdom 1 United States 3 Global 71

Zhengzhou Jingjiang Chemical Co. LTD

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J & K SCIENTIFIC LTD.

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View Lastest Price from Benzonitrile, 5-acetyl-2-amino- (9CI) manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: Benzonitrile, 5-acetyl-2-amino- (9CI) 33720-71-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2024-08-15

Career Henan Chemical Co

Product: Benzonitrile, 5-acetyl-2-amino- (9CI) 33720-71-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-02

33720-71-7, Benzonitrile, 5-acetyl-2-amino- (9CI)Related Search:

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Benzonitrile, 5-acetyl-2-amino- (9CI)

Benzonitrile,5-acetyl-2-amino-

5-Acetyl-2-aMinobenzonitrile

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33720-71-7

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