Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI)
- Product Name
- Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI)
- CAS No.
- 13210-29-2
- Chemical Name
- Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI)
- Synonyms
- 2-Acetyl-3-hydroxypyridine;1-(3-hydroxy-2-pyridyl)ethanone;1-(3-hydroxy-2-pyridinyl)- (9CI);1-(3-hydroxypyridin-2-yl)ethan-1-one;Ethanone, 1-(3-hydroxy-2-pyridinyl)-;Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI);Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI) ISO 9001：2015 REACH
- CBNumber
- CB81072011
- Molecular Formula
- C7H7NO2
- Formula Weight
- 137.14
- MOL File
- 13210-29-2.mol
Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI) Property
- Boiling point:
- 311.5±22.0 °C(Predicted)
- Density
- 1.217
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- 5.76±0.10(Predicted)
- Appearance
- Light yellow to light brown Solid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B433925
- Product name
- 1-(3-Hydroxypyridin-2-yl)ethanone
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- Z4085
- Product name
- 1-(3-Hydroxypyridin-2-yl)ethanone
- Packaging
- 1g
- Price
- $185
- Updated
- 2021/12/16
- Product number
- OR932930
- Product name
- 1-(3-Hydroxypyridin-2-yl)ethanone
- Purity
- 95%
- Packaging
- 5g
- Price
- $665
- Updated
- 2021/12/16
- Product number
- 119448
- Product name
- 1-(3-Hydroxypyridin-2-yl)ethanone
- Purity
- 95+%
- Packaging
- 5g
- Price
- $694
- Updated
- 2021/12/16
- Product number
- Z4085
- Product name
- 1-(3-Hydroxypyridin-2-yl)ethanone
- Packaging
- 10g
- Price
- $698
- Updated
- 2021/12/16
Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI) Chemical Properties,Usage,Production
Synthesis
75-16-1
932-35-4
13210-29-2
General procedure for the synthesis of 1-(3-hydroxypyridin-2-yl)ethanone from methylmagnesium bromide and 2-cyano-3-hydroxypyridine: Referring to the method of Example 58, to a solution of tetrahydrofuran (THF, 50 mL) of 2-cyano-3-hydroxypyridine (3.00 g, 25.0 mmol) was added slowly, under cooling in an ice bath, a THF solution of 3M methylmagnesium bromide ( 25 mL). After addition, the reaction mixture was stirred at room temperature for 30 min. Subsequently, the reaction mixture was neutralized with 6N hydrochloric acid solution and extracted twice with ethyl acetate. The organic layers were combined, washed with saturated sodium chloride solution and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure to afford the title compound 1-(3-hydroxypyridin-2-yl)ethanone (3.43 g, quantitative yield) as a powdered solid. The crude product was used directly in the subsequent reaction without further purification.
References
[1] Patent: EP2123652, 2009, A1. Location in patent: Page/Page column 63
[2] Patent: US2017/145026, 2017, A1. Location in patent: Paragraph 0622; 0623
Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI) manufacturers
- Product
- Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI) 13210-29-2
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-10-19
- Product
- Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI) 13210-29-2
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-09-27
- Product
- Ethanone, 1-(3-hydroxy-2-pyridinyl)- (9CI) 13210-29-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95%-99%
- Supply Ability
- 1000kg
- Release date
- 2019-08-26