ChemicalBook > CAS DataBase List > 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine

6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine

Product Name: 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine
CAS No.: 18184-75-3
Chemical Name: 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine
Synonyms: NSC 151664;7-dihydro-5;Moxifloxacin IMP;7-dioxopyrrolo[3;Mosisasin Impurity 30;2,3-Pyridinedicarboximide,N-benzyl;N-Benzyl- 2,3-pyridinedicarboximide;6-Benzylpyrrolo[3,4-b]pyridine-5,7-dione;6-Benzyl-6H-pyrrolo[3,4-b]pyridine- 5,7-dione;6-Benzyl-5H-pyrrolo[3,4-b]pyridine-5,7(6H)-dione
CBNumber: CB81121184
Molecular Formula: C14H10N2O2
Formula Weight: 238.24
MOL File: 18184-75-3.mol

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6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine Property

Melting point:: 154-156°C
Boiling point:: 418.9±28.0 °C(Predicted)
Density: 1.368±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,2-8°C
solubility: DMSO (Slightly), Methanol (Slightly)
form: Solid
pka: -0.78±0.20(Predicted)
color: Off-White
InChI: InChI=1S/C14H10N2O2/c17-13-11-7-4-8-15-12(11)14(18)16(13)9-10-5-2-1-3-6-10/h1-8H,9H2
InChIKey: DWUBVULEMQOCPO-UHFFFAOYSA-N
SMILES: C12C(=O)N(CC3=CC=CC=C3)C(=O)C1=CC=CN=2

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B275850
Product name: 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine
Packaging: 2g
Price: $325
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB18368
Product name: 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine
Packaging: 2g
Price: $462.5
Updated: 2021/12/16

Medical Isotopes, Inc.

Product number: 49729
Product name: 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-β]pyridine
Packaging: 1g
Price: $640
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0013018
Product name: 6-BENZYL-5,7-DIHYDRO-5,7-DIOXOPYRROLO[3,4-B]PYRIDINE
Purity: 95.00%
Packaging: 1G
Price: $739.2
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB18368
Product name: 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine
Packaging: 1g
Price: $254.4
Updated: 2021/12/16

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6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine Chemical Properties,Usage,Production

Chemical Properties

Off-White Solid

Synthesis

89-00-9

100-46-9

18184-75-3

6-Benzyl-6H-pyrrolo[3,4-B]pyridine-5,7-dione was synthesized using 2,3-pyridinedicarboxylic acid and benzylamine as raw materials by the same method as described previously, and the reaction conditions were adjusted to react at 150 °C for 18-26 hours. After completion of the reaction, the crude product was purified using a 15 cm x 2.5 cm silica gel column with a hexane solution of 60-80% ethyl acetate as eluent. The yield of the purified product was recorded in Table 3. Special note: Saturated NH4Cl solution was used instead of 1 M HCl in the step of washing pyridine derivatives.

References

[1] Tetrahedron, 2015, vol. 71, # 48, p. 9101 - 9111
[2] Patent: CN105777750, 2016, A. Location in patent: Paragraph 0024; 0025; 0040
[3] Asian Journal of Chemistry, 2013, vol. 25, # 15, p. 8701 - 8707

6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine 18184-75-3
Price: US $1.10/g
Min. Order: 1g
Purity: 99.0% min
Supply Ability: 100 tons min
Release date: 2021-05-12

Career Henan Chemical Co

Product: 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine 18184-75-3
Price: US $6.60/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg-1000kg
Release date: 2019-12-26

18184-75-3, 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridineRelated Search:

N-Methyl Moxifloxacin Moxifloxacin Related Impurity 2 Moxifloxacin Impurity 46 (4aS,7aS)-1-methyloctahydro-1H-pyrrolo[3,4-b]pyridine 6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione 6-BENZYL-6,7-DIHYDRO-5H-PYRROLO[3,4-B]PYRIDINE

6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine

6-(Phenylmethyl)-5H-pyrrolo[3,4-b]pyridine-5,7(6H)-dione

N-Benzyl- 2,3-pyridinedicarboximide

NSC 151664

6-Benzyl-6H-pyrrolo[3,4-b]pyridine- 5,7-dione

6-Benzyl-5H-pyrrolo[3,4-b]pyridine-5,7(6H)-dione

2,3-Pyridinedicarboximide,N-benzyl

6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridin

6-Benzylpyrrolo[3,4-b]pyridine-5,7-dione

6-benzyl-5H,6H,7H-pyrrolo[3,4-b]pyridine-5,7-dione

Moxifloxacin IMP

5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione, 6-(phenylmethyl)-

6-Benzyl-5,7-dihydro-5,7-dioxopyrrolo[3,4-b]pyridine ISO 9001：2015 REACH

7-dihydro-5

7-dioxopyrrolo[3

5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione, 6-(phenylmethyl)- (9CI, ACI)

Mosisasin Impurity 30

18184-75-3

Aromatics

Heterocycles