6-Chloro-N-methylpyridazin-3-amine
- Product Name
- 6-Chloro-N-methylpyridazin-3-amine
- CAS No.
- 14959-32-1
- Chemical Name
- 6-Chloro-N-methylpyridazin-3-amine
- Synonyms
- 6-Chloro-N-methylpyridazin-3-amine;3-Chloro-6-(methylamino)pyridazine;6-chloro-N-methyl-3-pyridazinamine;3-Chloro-6-N-methylaminopyridazine;3-PyridazinaMine, 6-chloro-N-Methyl-;6-Chloro-N-methylpyridazin-3-amine ISO 9001:2015 REACH
- CBNumber
- CB81262748
- Molecular Formula
- C5H6ClN3
- Formula Weight
- 143.57
- MOL File
- 14959-32-1.mol
6-Chloro-N-methylpyridazin-3-amine Property
- Melting point:
- 198-199℃
- Boiling point:
- 357.4±22.0 °C(Predicted)
- Density
- 1.338
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- solid
- pka
- 4.36±0.10(Predicted)
- color
- off white
- InChI
- InChI=1S/C5H6ClN3/c1-7-5-3-2-4(6)8-9-5/h2-3H,1H3,(H,7,9)
- InChIKey
- IHSYIVAZIINDFR-UHFFFAOYSA-N
- SMILES
- C1(NC)=NN=C(Cl)C=C1
Safety
- Hazard Codes
- Xi
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C349780
- Product name
- 3-Chloro-6-methylaminopyridazine
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C349780
- Product name
- 3-Chloro-6-methylaminopyridazine
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- C349780
- Product name
- 3-Chloro-6-methylaminopyridazine
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 3H31-5-Z7
- Product name
- 3-Chloro-6-(methylamino)pyridazine
- Packaging
- 1g
- Price
- $88
- Updated
- 2021/12/16
- Product number
- W3263
- Product name
- 3-Pyridazinamine,6-chloro-N-methyl-
- Packaging
- 5g
- Price
- $91
- Updated
- 2021/12/16
6-Chloro-N-methylpyridazin-3-amine Chemical Properties,Usage,Production
Uses
3-Chloro-6-methylaminopyridazine
Synthesis
141-30-0
74-89-5
14959-32-1
3,6-Dichloropyridazine (107,500 mg, 3.36 mmol) was slowly added to 2.0 M methanol solution of methylamine (MeOH solution of NH2Me, 5 mL, 10 mmol) and stirred at room temperature for 24 hours. Upon completion of the reaction, water was added to the reaction mixture and the organic phase was extracted with ethyl acetate. The collected organic phase was washed with saturated aqueous sodium chloride solution, dried over anhydrous sodium sulfate and concentrated under reduced pressure. Purification by column chromatography afforded 3-chloro-6-methylaminopyridazine (3-(N-monomethylamino)-6-chloropyridazine, 108e, 505 mg, 88% yield) as a white solid.1H NMR (400 MHz, DMSO-d6) δ 2.84 (d, J = 4.4 Hz, 3H), 6.87 (d, J = 9.2 Hz, 1H), 7.06 (br d, J = 4.0 Hz, 1H), 7.33 (d, J = 9.2 Hz, 1H); 13C NMR (100 MHz, DMSO-d6) δ 27.9, 117.9, 128.2, 144.9, 158.6.
References
[1] Patent: US2010/261727, 2010, A1. Location in patent: Page/Page column 32
6-Chloro-N-methylpyridazin-3-amine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-Chloro-N-methylpyridazin-3-amine manufacturers
- Product
- 6-Chloro-N-methylpyridazin-3-amine 14959-32-1
- Price
- US $0.00-0.00/KG
- Min. Order
- 1g
- Purity
- 98%minHPLC
- Supply Ability
- 10kgs/month
- Release date
- 2021-11-05
- Product
- 6-Chloro-N-methylpyridazin-3-amine 14959-32-1
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-11-02
- Product
- 6-Chloro-N-methylpyridazin-3-amine 14959-32-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 90%-99.9%
- Supply Ability
- 500kg
- Release date
- 2019-07-12