m-Iodobenzylchloride

Product Name: m-Iodobenzylchloride
CAS No.: 60076-09-7
Chemical Name: m-Iodobenzylchloride
Synonyms: 3-iodobenzylchloride;m-Iodobenzylchloride;1-(ChloroMethyl)-3-iodobenzene;Benzene, 1-(chloromethyl)-3-iodo-
CBNumber: CB81454929
Molecular Formula: C7H6ClI
Formula Weight: 252.48
MOL File: 60076-09-7.mol

More

Less

m-Iodobenzylchloride Property

storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TRC

Product number: C587950
Product name: 1-(Chloromethyl)-3-iodobenzene
Packaging: 100mg
Price: $60
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0362310
Product name: 1-(CHLOROMETHYL)-3-IODOBENZENE
Purity: 95.00%
Packaging: 5MG
Price: $504.8
Updated: 2021/12/16

AK Scientific

Product number: 8955AB
Product name: 1-(Chloromethyl)-3-iodobenzene
Packaging: 250mg
Price: $136
Updated: 2021/12/16

AK Scientific

Product number: 8955AB
Product name: 1-(Chloromethyl)-3-iodobenzene
Packaging: 25g
Price: $586
Updated: 2021/12/16

Alichem

Product number: 60076097
Product name: 3-Iodobenzylchloride
Packaging: 500mg
Price: $806.85
Updated: 2021/12/16

More

Less

m-Iodobenzylchloride Chemical Properties,Usage,Production

Synthesis

57455-06-8

60076-09-7

General procedure for the synthesis of 1-(chloromethyl)-3-iodobenzene from 3-iodobenzyl alcohol: 3-iodobenzyl alcohol (600 mg, 2.56 mmol) was dissolved in dichloromethane (DCM, 3 mL), and thionyl chloride (3 mL, 41.3 mmol) was added, and the reaction was stirred for 18 hours at room temperature. Subsequently, thionyl chloride (1 mL, 13.7 mmol) was added and the reaction mixture was heated to reflux for 12 hours. Upon completion of the reaction, the cooled solution was alkalized with 50% sodium hydroxide solution, diluted with water and extracted with dichloromethane. The organic phases were combined, dried with anhydrous magnesium sulfate, filtered and concentrated to give a clarified slurry. After standing, the slurry crystallized to give 3-iodobenzyl chloride as a white solid (650 mg, quantitative yield).

References

[1] Patent: WO2011/86085, 2011, A1. Location in patent: Page/Page column 39-40
[2] Recueil des Travaux Chimiques des Pays-Bas, 1923, vol. 42, p. 522
[3] Patent: EP1386913, 2004, A1. Location in patent: Page 94
[4] Patent: WO2017/72021, 2017, A1. Location in patent: Page/Page column 76

m-Iodobenzylchloride Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

m-Iodobenzylchloride Suppliers

China 26 India 1 United States 2 Global 29

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Beijing Eternalchem Co,. Ltd.

Tel: 010-59484199 18611897322
Email: sales@eternalchem.com
Country: China
ProdList: 4383
Advantage: 60

Cool Pharm, Ltd

Tel: 021-60455363 18019463053
Fax: 50966098
Email: sales@coolpharm.com
Country: China
ProdList: 12346
Advantage: 58

Changzhou Anxuan Chemical, Co., Ltd.

Tel: 13912302692 13912302692;
Fax: 0519-88064678
Email: sales@anxuanchem.com
Country: China
ProdList: 4828
Advantage: 58

SanoChem (Chengdu) Tech. Co., Ltd.

Tel: 28-87999436 02887999436
Fax: QQ:2746983436
Email: sales@sano-chem.com
Country: China
ProdList: 3795
Advantage: 55

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Aikon International Limited

Tel: 025-66061636 18013972705
Fax: (3)02557626880
Email: qqyang@aikonchem.com
Country: China
ProdList: 15814
Advantage: 58

SHANGHAI FDC-CHEMICAL CO.,LTD

Tel: 021-61469567 13482353728
Fax: 021-61161605
Email: sales@fdc-chemical.com
Country: China
ProdList: 9717
Advantage: 58

Allfluoro pharmaceutical co. ltd.

Tel: +86-400-0216110 +86-15958047586
Fax: 0086-21-33275002
Email: sales@allfluoro.com
Country: China
ProdList: 11385
Advantage: 58

Hefei TNJ Chemical Industry Co.,Ltd.

Tel: +86-0551-65418671 +8618949823763
Fax: 0551-65418697
Email: sales@tnjchem.com
Country: China
ProdList: 34563
Advantage: 58

Win-Win chemical CO., Limited

Tel: +86-0086-577-64498589 +86-15355981851
Fax: 0086-577-56994596
Email: sales@win-winchemical.com
Country: China
ProdList: 14359
Advantage: 58

Shandong WorldSun Biological Technology Co., Ltd.

Tel: 0531-88723173 18596073690
Email: 1047208234@qq.com
Country: China
ProdList: 6779
Advantage: 58

Energy Chemical

Tel: 021-58432009 400-005-6266
Fax: 021-58436166
Email: marketing@energy-chemical.com
Country: China
ProdList: 44918
Advantage: 58

Beijing Jin Ming Biotechnology Co., Ltd.

Tel: 010-60605840 15801484223;
Email: psaitong@jm-bio.com
Country: China
ProdList: 29757
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-6005915
Email: sales@picasso-e.com
Country: China
ProdList: 39653
Advantage: 58

Zhuhai Aobokai Biomedical Technology Co., Ltd.

Tel: 400-0628126 18736790110;
Email: sales-team@aobchem.com.cn
Country: China
ProdList: 50000
Advantage: 58

Baoji Didu Pharmaceutical and Chemical Co., Ltd

Tel: 029-81145305 17791533577
Email: 1021@dideu.com
Country: China
ProdList: 10009
Advantage: 58

DAYANG CHEM (HANGZHOU) CO.,LTD

Tel: +86-88938639 +86-17705817739
Email: info@dycnchem.com
Country: China
ProdList: 53899
Advantage: 58

Changzhou Anxuan Chemical Co., Ltd

Tel: +86-0519-89882563 +86-18961279162
Email: andy@anxuanchem.com
Country: China
ProdList: 4327
Advantage: 58

Aromsyn Co., Ltd.

Tel: +86-0571-85585865 +8613336024896
Email: CB@aromsyn.com
Country: China
ProdList: 19183
Advantage: 58

Changzhou Ansciep Chemical Co., Ltd.

Tel: +86 519 86305871
Fax: +86 519 86305879
Email: sales@ansciepchem.com
Country: CHINA
ProdList: 4241
Advantage: 58

Shanghai Hao Zhun Biological Technology Co., Ltd.

Tel: --
Fax: --
Email: info@zzsrm.com
Country: CHINA
ProdList: 6650
Advantage: 58

Shanghai Wowu Biological Technology Co., Ltd.

Tel: --
Fax: --
Email: shhebio@126.com
Country: CHINA
ProdList: 6137
Advantage: 58

Shanghai Machine Pure Industrial Co., Ltd.

Tel: --
Fax: --
Email: 3245176082@qq.com
Country: CHINA
ProdList: 6800
Advantage: 58

Shanghai Hanhong Chemical Co., Ltd

Tel: --
Fax: --
Email: info@hanhonggroup.com
Country: China
ProdList: 3944
Advantage: 67

Binhai Hanhong Biochemical Co., Ltd

Tel: --
Fax: --
Email: 2355241815@qq.com
Country: China
ProdList: 3448
Advantage: 54

60076-09-7, m-IodobenzylchlorideRelated Search:

m-Iodobenzylchloride

3-iodobenzylchloride

1-(ChloroMethyl)-3-iodobenzene

Benzene, 1-(chloromethyl)-3-iodo-

60076-09-7