ChemicalBook > CAS DataBase List > 5-bromo-1-nitro-naphthalene

5-bromo-1-nitro-naphthalene

Product Name
5-bromo-1-nitro-naphthalene
CAS No.
5328-76-7
Chemical Name
5-bromo-1-nitro-naphthalene
Synonyms
5-bromo-1-nitro-naphthalene;Naphthalene, 1-bromo-5-nitro-;1-Bromo-5-nitronaphthalene96%
CBNumber
CB81465626
Molecular Formula
C10H6BrNO2
Formula Weight
252.06
MOL File
5328-76-7.mol
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5-bromo-1-nitro-naphthalene Property

Melting point:
121 °C
Boiling point:
363.8±17.0 °C(Predicted)
Density 
1.662±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
powder
color 
Light brown to brown
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Safety

HS Code 
2904990090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B697998
Product name
1-Bromo-5-nitronaphthalene
Packaging
250mg
Price
$55
Updated
2021/12/16
AK Scientific
Product number
J53153
Product name
1-Bromo-5-nitronaphthalene
Packaging
5g
Price
$60
Updated
2021/12/16
Matrix Scientific
Product number
143405
Product name
1-Bromo-5-nitronaphthalene
Purity
97%
Packaging
1g
Price
$75
Updated
2021/12/16
AK Scientific
Product number
V6445
Product name
1-Bromo-5-nitronaphthalene
Packaging
5g
Price
$81
Updated
2021/12/16
AK Scientific
Product number
V6445
Product name
1-Bromo-5-nitronaphthalene
Packaging
25g
Price
$214
Updated
2021/12/16
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5-bromo-1-nitro-naphthalene Chemical Properties,Usage,Production

Synthesis

86-57-7

5328-76-7

The general procedure for the synthesis of 1-bromo-5-nitronaphthalene from 1-nitronaphthalene is as follows: 77.5 g (0.485 mol) of bromine was added slowly and dropwise to a stirred mixture of 86 g (0.5 mol) of 1-nitronaphthalene and 0.8-1.0 g of reduced iron powder over a period of 30 min, while the reaction temperature was maintained at 80-85°C. The reaction was carried out in the following manner. After about one hour, the reaction mixture crystallized directly when gas escape ceased. Subsequently, one crystallization was carried out with ethanol and two more with Sorit A from acetone. An average of 52.0 g of a fine yellow needle-like product was obtained with a melting point of 121-122°C (41% yield); the literature reports a melting point of 122.5°C.

References

[1] New Journal of Chemistry, 2005, vol. 29, # 4, p. 579 - 586
[2] Chemistry Letters, 2015, vol. 44, # 6, p. 743 - 745
[3] Angewandte Chemie - International Edition, 2008, vol. 47, # 32, p. 6062 - 6064
[4] Journal of Organic Chemistry, 2017, vol. 82, # 7, p. 3873 - 3879
[5] Journal of Organic Chemistry, 1949, vol. 14, p. 111,114

5-bromo-1-nitro-naphthalene Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-bromo-1-nitro-naphthalene manufacturers

Career Henan Chemical Co
Product
5-bromo-1-nitro-naphthalene 5328-76-7
Price
US $2.00/KG
Min. Order
1g
Purity
98%MIN
Supply Ability
ASK
Release date
2020-01-07

5328-76-7, 5-bromo-1-nitro-naphthaleneRelated Search:


  • 5-bromo-1-nitro-naphthalene
  • 1-Bromo-5-nitronaphthalene96%
  • Naphthalene, 1-bromo-5-nitro-
  • 5328-76-7
  • john's