ChemicalBook > CAS DataBase List > 4-Iodo-N,N-dimethyl-Benzenamine

4-Iodo-N,N-dimethyl-Benzenamine

Product Name
4-Iodo-N,N-dimethyl-Benzenamine
CAS No.
698-70-4
Chemical Name
4-Iodo-N,N-dimethyl-Benzenamine
Synonyms
4-Iodo-N,N-dimethylanilin;1-DIMETHYLAMINO-4-IODOBENZENE;4-Iodo-N,N-dimethyl-Benzenamine;N,N-DIMETHYLAMINO-4-IODOANILINE;4-(N,N-DIMETHYLAMINO)IODOBENZENE;Benzenamine, 4-iodo-N,N-dimethyl-
CBNumber
CB81481947
Molecular Formula
C8H10IN
Formula Weight
247.08
MOL File
698-70-4.mol
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4-Iodo-N,N-dimethyl-Benzenamine Property

Melting point:
79.5 °C
Boiling point:
263.7±23.0 °C(Predicted)
Density 
1.652±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Store in freezer, under -20°C
solubility 
Chloroform (Slightly), Ethyl Acetate (Slightly)
form 
Solid
pka
4.14±0.12(Predicted)
color 
Very Dark Blue to Very Dark Purple
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC
Product number
I719595
Product name
4-Iodo-N,N-dimethylaniline
Packaging
500mg
Price
$200
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0366364
Product name
4-IODO-N,N-DIMETHYLANILINE
Purity
95.00%
Packaging
250MG
Price
$212.1
Updated
2021/12/16
AK Scientific
Product number
J93018
Product name
4-Iodo-N,N-dimethylaniline
Packaging
10g
Price
$450
Updated
2021/12/16
Ambeed
Product number
A489054
Product name
4-Iodo-N,N-dimethylaniline
Purity
98%
Packaging
100mg
Price
$21
Updated
2021/12/16
Ambeed
Product number
A489054
Product name
4-Iodo-N,N-dimethylaniline
Purity
98%
Packaging
250mg
Price
$28
Updated
2021/12/16
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4-Iodo-N,N-dimethyl-Benzenamine Chemical Properties,Usage,Production

Uses

4-Iodo-N,N-dimethylaniline is a useful reactant for organic reactions and the synthesis of various compounds.

Synthesis

121-69-7

698-70-4

General procedure for the synthesis of 4-N,N-dimethylaminoiodobenzene from N,N-dimethylaniline: to a stirred solution of N,N-dimethylaniline (1 mmol) in dichloromethane (CH2Cl2) or 1,2-dichloroethane ((CH2Cl)2) (0.1 M) was added sequentially Ph3PAuNTf2 (0.025 mmol, 19 mg; if using the 2:1 complex of Ph3PAuNTf2 with toluene) and N-iodosuccinimide (NIS, 1.1 mmol, 248 mg). The reaction mixture was stirred at room temperature or reacted under reflux conditions until complete conversion of the feedstock was shown by thin layer chromatography (TLC) monitoring. Upon completion of the reaction, the solvent was evaporated under reduced pressure and the resulting crude product was purified by fast column chromatography using different ratios of hexane and ethyl acetate (EtOAc) as eluents, resulting in pure 4-N,N-dimethylaminoiodobenzene.

References

[1] RSC Advances, 2014, vol. 4, # 12, p. 6267 - 6274
[2] Journal of Organic Chemistry, 1993, vol. 58, # 8, p. 2058 - 2060
[3] Tetrahedron Letters, 2005, vol. 46, # 32, p. 5421 - 5423
[4] Tetrahedron, 2005, vol. 61, # 49, p. 11657 - 11663
[5] Helvetica Chimica Acta, 2007, vol. 90, # 11, p. 2087 - 2095

4-Iodo-N,N-dimethyl-Benzenamine Preparation Products And Raw materials

Raw materials

Preparation Products

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698-70-4, 4-Iodo-N,N-dimethyl-BenzenamineRelated Search:

sodium metrizoate Iohexol Metrizamide 4-Iodo-N,N-dimethyl-Benzenamine 1-(5-IODOINDOLIN-1-YL)ETHANONE N-(4-IODOPHENYL)SUCCINIMIDE 1-(4-IODOPHENYL)-1H-PYRROLE-2,5-DIONE 1-(4-IODOPHENYL)-3-MORPHOLINODIHYDRO-1H-PYRROLE-2,5-DIONE 1-(4-IODOPHENYL)-3-PIPERIDINODIHYDRO-1H-PYRROLE-2,5-DIONE 1-(4-IODOPHENYL)-3-[(4-METHYLPHENYL)SULFANYL]DIHYDRO-1H-PYRROLE-2,5-DIONE N-(2,4-dimethoxybenzyl)-N-(4-iodophenyl)-N'-phenylthiourea 2-(4-iodophenyl)-2,3-dihydro-1H-isoindol-1-imine 1-AMINO-4-(4-IODOPHENYL)PIPERAZINE-2,5-DIONE methylglucamine metrizoate N-(2,4-DIMETHOXYBENZYL)-N-(4-IODOPHENYL)-N'-METHYLTHIOUREA AKOS AUF0217 N'-BENZYL-N-(2,4-DIMETHOXYBENZYL)-N-(4-IODOPHENYL)THIOUREA 3-[(4-chlorophenyl)sulfanyl]-1-(4-iodophenyl)dihydro-1H-pyrrole-2,5-dione

  • 4-Iodo-N,N-dimethyl-Benzenamine
  • 1-DIMETHYLAMINO-4-IODOBENZENE
  • 4-(N,N-DIMETHYLAMINO)IODOBENZENE
  • N,N-DIMETHYLAMINO-4-IODOANILINE
  • Benzenamine, 4-iodo-N,N-dimethyl-
  • 4-Iodo-N,N-dimethylanilin
  • 698-70-4