7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE, 1,4-DIHYDRO-
- Product Name
- 7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE, 1,4-DIHYDRO-
- CAS No.
- 13877-55-9
- Chemical Name
- 7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE, 1,4-DIHYDRO-
- Synonyms
- 1,6-dihydro-7H-Pyrazolo[4,3-d]pyrimidin-7-one;7H-Pyrazolo[4,3-d]pyriMidin-7-one, 1,6-dihydro-;Nsc 79301;7-ketopyrazolo(4,3-d)pyrimidine;7H-Pyrazolo[4,3-d]pyrimidin-7-one;7-Hydroxypyrazolo[4,3-d]pyrimidine;1H-Pyrazolo(4,3-D)pyrimidine-7-one;1H-pyrazolo[4,3-d]pyrimidin-7(4H)-one;2H-pyrazolo[4,3-d]pyrimidin-7(6H)-one;7-Hydroxy-1H-pyrazolo[4,3-d]pyrimidine
- CBNumber
- CB8156592
- Molecular Formula
- C5H4N4O
- Formula Weight
- 136.11
- MOL File
- 13877-55-9.mol
7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE, 1,4-DIHYDRO- Property
- Melting point:
- >30 °C(Solv: water (7732-18-5))
- Boiling point:
- 559.8±23.0 °C(Predicted)
- Density
- 1.89±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 10.66±0.20(Predicted)
- Appearance
- Off-white to gray Solid
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
N-Bromosuccinimide Price
- Product number
- H956213
- Product name
- 7-Hydroxypyrazolo[4,3-D]Pyrimidine
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- W3034
- Product name
- 7-Hydroxypyrazolo[4,3-d]pyrimidine
- Packaging
- 250mg
- Price
- $79
- Updated
- 2021/12/16
- Product number
- 4H48-1-JB
- Product name
- 1H,6H,7H-Pyrazolo[4,3-d]pyrimidin-7-one
- Purity
- 97.0%
- Packaging
- 250mg
- Price
- $190
- Updated
- 2021/12/16
- Product number
- 4H48-1-JB
- Product name
- 1H,6H,7H-Pyrazolo[4,3-d]pyrimidin-7-one
- Purity
- 97.0%
- Packaging
- 1g
- Price
- $490
- Updated
- 2021/12/16
- Product number
- 073003
- Product name
- 7-Hydroxypyrazolo[4,3-d]pyrimidine
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $601
- Updated
- 2021/12/16
7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE, 1,4-DIHYDRO- Chemical Properties,Usage,Production
Synthesis
923283-63-0
3473-63-0
13877-55-9
GENERAL STEPS: Formamidine acetate (40.3 mmol, 4.2 g) was added to a mixed solution of Hunig base (40 mL) and n-butanol (n-BuOH, 40 mL) containing 1-tert-butyl 3-methyl 4-amino-1H-pyrazole-1,3-dicarboxylic acid (26, 8.85 g, 36.7 mmol). The reaction mixture was heated with stirring at 110 °C for 1 hour. After completion of the reaction, it was cooled to room temperature and the precipitated solid product was collected. The solid was washed with dichloromethane and then dried under reduced pressure to afford 7-hydroxypyrazolo[4,3-D]pyrimidine (27, 4.46 g, 89% yield). The structure of the product was confirmed by electrospray mass spectrometry (ES(+)MS), m/e = 137.
References
[1] Patent: US2007/27166, 2007, A1. Location in patent: Page/Page column 84-85
7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE, 1,4-DIHYDRO- Preparation Products And Raw materials
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View Lastest Price from 7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE, 1,4-DIHYDRO- manufacturers
- Product
- 7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE, 1,4-DIHYDRO- 13877-55-9
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-12-10
- Product
- 7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE, 1,4-DIHYDRO- 13877-55-9
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10
- Product
- 7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE, 1,4-DIHYDRO- 13877-55-9
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09