2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE

Product Name: 2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE
CAS No.: 15108-18-6
Chemical Name: 2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE
Synonyms: AKOS B003342;AKOS BC-3070;AURORA 23334;ASISCHEM D13394;3-BENZIMIDAZOLE;2-HYDRAZINO-1H-1;AKOS BBS-00004616;IFLAB-BB F0896-0068;CHEMBRDG-BB 4100063;OTAVA-BB BB7211810053
CBNumber: CB8193225
Molecular Formula: C7H8N4
Formula Weight: 148.17
MOL File: 15108-18-6.mol

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2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE Property

Melting point:: 224-225
Boiling point:: 318.2±25.0 °C(Predicted)
Density: 1.49±0.1 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
solubility: DMSO (Slightly, Heated), Methanol (Slightly)
form: Solid
pka: 6.07±0.20(Predicted)
color: Dark Brown
InChI: InChI=1S/C7H8N4/c8-11-7-9-5-3-1-2-4-6(5)10-7/h1-4H,8H2,(H2,9,10,11)
InChIKey: PXUYWNZBZXDJEU-UHFFFAOYSA-N
SMILES: C1(NN)NC2=CC=CC=C2N=1

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Safety

Hazard Codes: Xi
Risk Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39
HazardClass: IRRITANT
HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

Apolloscientific

Product number: OR14212
Product name: 2-Hydrazino-1H-benzimidazole
Packaging: 5g
Price: $66
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H39-1-Y0
Product name: 2-Hydrazino-1H-benzimidazole
Packaging: 5G
Price: $72
Updated: 2021/12/16

Matrix Scientific

Product number: 035802
Product name: 2-Hydrazino-1H-1,3-benzimidazole
Packaging: 5g
Price: $74
Updated: 2021/12/16

Matrix Scientific

Product number: 035802
Product name: 2-Hydrazino-1H-1,3-benzimidazole
Packaging: 500mg
Price: $16
Updated: 2021/12/16

Apolloscientific

Product number: OR14212
Product name: 2-Hydrazino-1H-benzimidazole
Packaging: 1g
Price: $22
Updated: 2021/12/16

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2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE Chemical Properties,Usage,Production

Synthesis

54624-57-6

15108-18-6

The general procedure for the synthesis of 2-hydrazino-1H-1,3-benzimidazole was as follows: firstly, 2-bromobenzimidazole was prepared from 2-mercaptobenzimidazole according to the method reported in literature [13]. Subsequently, 2-bromobenzimidazole (1.97 g, 10 mmol) was dissolved in 20 mL of 80% hydrazine hydrate solution and reacted at reflux to obtain 2-hydrazinylbenzimidazole (1.35 g, 91% yield). Finally, diacetyl monoxime (1.01 g, 10 mmol) was added to a 20 mL methanol solution containing 2-hydrazinylbenzimidazole (1.48 g, 10 mmol) catalyzed by glacial acetic acid (3 drops). The reaction mixture was refluxed for 4 h. After cooling and filtration, the resulting white crystals were washed with cold methanol to afford the target product 2-hydrazino-1H-1,3-benzimidazole (1.6 g, 55% yield, melting point 240 °C).

References

[1] Journal of Molecular Structure, 2017, vol. 1133, p. 546 - 556
[2] Polyhedron, 2017, vol. 127, p. 225 - 237

2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE Suppliers

Austria 1 Canada 1 China 49 Europe 1 Finland 1 Germany 3 India 3 Russia 1 Switzerland 1 Ukraine 4 United Kingdom 3 United States 13 Global 81

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View Lastest Price from 2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE 15108-18-6
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-14

15108-18-6, 2-HYDRAZINO-1H-1,3-BENZIMIDAZOLERelated Search:

HYDRAZINE 2-HYDRAZINO-1-ISOPENTYL-1H-BENZIMIDAZOLE 2H-Benzimidazol-2-one,1,3-dihydro-1-methyl-,hydrazone(9CI) 2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE 5-BROMO-2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE 2-hydrazino-1-methyl-1H-benzimidazole hydrochloride (1-ISOPROPYL-1H-BENZOIMIDAZOL-2-YL)-HYDRAZINE N-4H-1,2,4-TRIAZOL-4-YL-1H-BENZIMIDAZOL-2-AMINE 2-(1H-BENZOIMIDAZOL-2-YL)-4-CHLORO-5-MORPHOLIN-4-YL-2H-PYRIDAZIN-3-ONE 1-METHYL-N-4H-1,2,4-TRIAZOL-4-YL-1H-BENZIMIDAZOL-2-AMINE (4E)-2-(1H-BENZIMIDAZOL-2-YL)-4-{[(3,5-DIMETHOXYPHENYL)AMINO]METHYLENE}-5-METHYL-2,4-DIHYDRO-3H-PYRAZOL-3-ONE 1-(1H-BENZOIMIDAZOL-2-YL)-6-OXO-1,4,5,6-TETRAHYDRO-PYRIDAZINE-3-CARBOXYLIC ACID RARECHEM AQ NN 0128 (4E)-2-(1H-BENZIMIDAZOL-2-YL)-4-[4-(DIMETHYLAMINO)BENZYLIDENE]-5-METHYL-2,4-DIHYDRO-3H-PYRAZOL-3-ONE RARECHEM AQ NN 0127 2-(1H-BENZOIMIDAZOL-2-YL)-4-CHLORO-5-PIPERIDIN-1-YL-2H-PYRIDAZIN-3-ONE 1-BENZYL-2-HYDRAZINO-1H-BENZIMIDAZOLE 2-(1H-BENZIMIDAZOL-2-YL)-4-CHLORO-5-PIPERAZIN-1-YLPYRIDAZIN-3(2H)-ONE

ASISCHEM D13394

AKOS BBS-00004616

AKOS BC-3070

AKOS B003342

2-HYDRAZINO-1H-1,3-BENZIMIDAZOLE

2-HYDRAZINO-1H-BENZIMIDAZOLE

(1H-BENZOIMIDAZOL-2-YL)-HYDRAZINE

1-(1H-benzo[d]iMidazol-2-yl)hydrazine

2H-Benzimidazol-2-one,1,3-dihydro-,hydrazone(9CI)

2-hydrazinyl-1H-benzo[d]imidazole

2-hydrazino-1H-benzimidazole(SALTDATA: FREE)

(1H-Benzimidazol-2-yl)hydrazine

2H-Benzimidazol-2-one, 1,3-dihydro-, hydrazone

Benzimidazole, 2-hydrazino-

OTAVA-BB BB7211810053

IFLAB-BB F0896-0068

CHEMBRDG-BB 4100063

BENZIMIDAZOL-2-YL-HYDRAZINE

AURORA 23334

2-hydrazino-1H-1,3-benzimidazole 97%

2-Hydrazono-2,3-dihydro-1H-benzo[d]imidazole

2-Hydrazinobenzimidazole

1H-Benzimidazole, 2-hydrazinyl-

2-HYDRAZINO-1H-1

3-BENZIMIDAZOLE

15108-18-6

BENZIMIDAZOLE