1,9-DIBROMONONANE
- Product Name
- 1,9-DIBROMONONANE
- CAS No.
- 4549-33-1
- Chemical Name
- 1,9-DIBROMONONANE
- Synonyms
- 1,9-Dibromnonan;1,9-Dibromonone;1,9-Dibromnonane;1,9-DIBROMONONANE;1,9-dibromo-nonan;Nonane,1,9-dibromo-;Nonamethylendibromid;1,9-Dibromononane>NONAMETHYLENE BROMIDE;1,9-Dibromononane,97%
- CBNumber
- CB8217879
- Molecular Formula
- C9H18Br2
- Formula Weight
- 286.05
- MOL File
- 4549-33-1.mol
1,9-DIBROMONONANE Property
- Melting point:
- -2 °C
- Boiling point:
- 285-288 °C (lit.)
- Density
- 1.407 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.496(lit.)
- Flash point:
- >230 °F
- storage temp.
- Sealed in dry,Room Temperature
- form
- Liquid
- color
- Clear colorless to yellow
- BRN
- 1737598
- InChI
- InChI=1S/C9H18Br2/c10-8-6-4-2-1-3-5-7-9-11/h1-9H2
- InChIKey
- WGAXVZXBFBHLMC-UHFFFAOYSA-N
- SMILES
- C(Br)CCCCCCCCBr
- CAS DataBase Reference
- 4549-33-1(CAS DataBase Reference)
- EPA Substance Registry System
- Nonane, 1,9-dibromo- (4549-33-1)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- D42402
- Product name
- 1,9-Dibromononane
- Purity
- 97%
- Packaging
- 25g
- Price
- $115.07
- Updated
- 2025/07/31
- Product number
- D1746
- Product name
- 1,9-Dibromononane
- Purity
- >97.0%(GC)
- Packaging
- 25g
- Price
- $66
- Updated
- 2025/07/31
- Product number
- FD75328
- Product name
- 1,9-Dibromononane
- Packaging
- 250g
- Price
- $200
- Updated
- 2021/12/16
- Product number
- 075618
- Product name
- 1,9-Dibromononane
- Purity
- 95+%
- Packaging
- 100g
- Price
- $301
- Updated
- 2021/12/16
- Product number
- FD75328
- Product name
- 1,9-Dibromononane
- Packaging
- 500g
- Price
- $350
- Updated
- 2021/12/16
1,9-DIBROMONONANE Chemical Properties,Usage,Production
Chemical Properties
CLEAR COLOURLESS TO SLIGHTLY YELLOW LIQUID
Uses
1,9-Dibromononane is a useful research chemical compound.
Synthesis
3937-56-2
4549-33-1
General procedure: In a dry reaction flask equipped with a stir bar, copper catalyst (2 mg, 0.002 mmol, 0.01 eq.), 1,9-nonanediol (0.20 mmol, 1.0 eq.), carbon tetrabromide (131.6 mg, 0.4 mmol, 2.0 eq.), and sodium bromide (41 mg, 0.40 mmol, 2.0 eq.) were added in sequence. The reaction vial was sealed and after displacing the air with nitrogen, anhydrous DMF (1.5 mL) was added via syringe. The reaction mixture was stirred under the light of a purple LED (394 nm) for 24 hours. Upon completion of the reaction, the mixture was transferred to a partitioning funnel and layered with ether (10 mL) and water (10 mL). The aqueous layer was separated and extracted with ether (2 x 10 mL). The organic layers were combined and washed sequentially with saturated aqueous NaHCO3 solution, Na2S2O3 solution and brine, dried with anhydrous Na2SO4 and concentrated under reduced pressure. The residue was purified by column chromatography (100% hexane as eluent) to afford the target product 1,9-dibromononane.
References
[1] Beilstein Journal of Organic Chemistry, 2018, vol. 14, p. 2730 - 2736
[2] Nippon Kagaku Zasshi, 1957, vol. 78, p. 1504
[3] Chem.Abstr., 1960, p. 1540
[4] Bulletin de la Societe Chimique de France, 1957, p. 1463,1467
[5] Biochemical Journal, 1947, vol. 41, p. 57
1,9-DIBROMONONANE Preparation Products And Raw materials
Raw materials
Preparation Products
1,9-DIBROMONONANE Suppliers
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View Lastest Price from 1,9-DIBROMONONANE manufacturers
- Product
- 1,9-Dibromononane 4549-33-1
- Price
- US $2.20-8.80/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2025-06-24
- Product
- 1,9-DIBROMONONANE 4549-33-1
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-09-26
- Product
- 1,9-DIBROMONONANE 4549-33-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1000KGS
- Release date
- 2019-12-25