3-CHLORO-2-HYDRAZINO-1,2-DIHYDROPYRAZINE HYDROCHLORIDE
- Product Name
- 3-CHLORO-2-HYDRAZINO-1,2-DIHYDROPYRAZINE HYDROCHLORIDE
- CAS No.
- 63286-28-2
- Chemical Name
- 3-CHLORO-2-HYDRAZINO-1,2-DIHYDROPYRAZINE HYDROCHLORIDE
- Synonyms
- oro-3-hydrazinyL;2-Chloro-3-hydrazinopyrazine;2-CHLORO-3-HYDRAZINYLPYRAZINE;2-chloro-3-hydrazineylpyrazine;(3-Chloropyrazin-2-yl)hydrazine;Pyrazine,2-chloro-3-hydrazinyl-;2-(3-chloropyrazin-2-yl)hydrazine;3-Chloro-2(H)-pyrazinone hydrazone;2-Chloro-3-hydrazinopyrazine, 97%min;2-chloro-3-hydrazinopyrazine(SALTDATA: FREE)
- CBNumber
- CB8221810
- Molecular Formula
- C4H5ClN4
- Formula Weight
- 144.56
- MOL File
- 63286-28-2.mol
3-CHLORO-2-HYDRAZINO-1,2-DIHYDROPYRAZINE HYDROCHLORIDE Property
- Melting point:
- 154-159°C
- Boiling point:
- 271.0±23.0 °C(Predicted)
- Density
- 1.63±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
- solubility
- DMSO (Slightly), Methanol (Slightly)
- form
- Solid
- pka
- 1.27±0.20(Predicted)
- color
- Very Dark Red to Brown
Safety
- Hazard Codes
- Xn
- Risk Statements
- 22-37/38-41
- Safety Statements
- 26-39
- RIDADR
- UN 2811 6.1 / PGIII
- WGK Germany
- 3
- HazardClass
- 6.1
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- 738964
- Product name
- 2-Chloro-3-hydrazinopyrazine
- Purity
- 95%
- Packaging
- 1g
- Price
- $54.28
- Updated
- 2025/07/31
- Product number
- 270062
- Product name
- 3-Chloro-2-Hydrazino-1,2-Dihydropyrazine Hydrochloride
- Packaging
- 250mg
- Price
- $375
- Updated
- 2021/12/16
- Product number
- C367643
- Product name
- 2-Chloro-3-hydrazinylpyrazine
- Packaging
- 1g
- Price
- $80
- Updated
- 2021/12/16
- Product number
- 072452
- Product name
- 2-Chloro-3-hydrazinylpyrazine
- Purity
- 95+%
- Packaging
- 5g
- Price
- $98
- Updated
- 2021/12/16
- Product number
- FC53681
- Product name
- 3-Chloro-2-Hydrazino-1,2-Dihydropyrazine Hydrochloride
- Packaging
- 1g
- Price
- $100
- Updated
- 2021/12/16
3-CHLORO-2-HYDRAZINO-1,2-DIHYDROPYRAZINE HYDROCHLORIDE Chemical Properties,Usage,Production
Synthesis
4858-85-9
63286-28-2
Step 1: 2,3-Dichloropyrazine (150 g, 1.00 mol) was dissolved in ethanol (700 mL) to which hydrazine monohydrate (124.53 g, 2.11 mmol, 85% aqueous solution) was subsequently added. The reaction mixture was heated under reflux conditions overnight. Upon completion of the reaction, the mixture was cooled and the precipitate was collected by filtration. The resulting solid was washed sequentially with water (100 mL, twice) and cold ethanol (150 mL, twice) and finally dried under reduced pressure to give 2-chloro-3-hydrazinopyrazine (140 g, 96% yield).
References
[1] Patent: WO2016/55618, 2016, A1. Location in patent: Page/Page column 64
[2] Patent: US2014/142098, 2014, A1. Location in patent: Paragraph 0233 - 0236
[3] Patent: US2015/133447, 2015, A1. Location in patent: Paragraph 0287; 0288; 0289
[4] Patent: WO2013/39785, 2013, A2. Location in patent: Page/Page column 80; 81
[5] Patent: WO2008/130951, 2008, A1. Location in patent: Page/Page column 60
3-CHLORO-2-HYDRAZINO-1,2-DIHYDROPYRAZINE HYDROCHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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