ChemicalBook > CAS DataBase List > 4-(METHYLAMINO)-3-NITROPYRIDINE

4-(METHYLAMINO)-3-NITROPYRIDINE

Product Name
4-(METHYLAMINO)-3-NITROPYRIDINE
CAS No.
1633-41-6
Chemical Name
4-(METHYLAMINO)-3-NITROPYRIDINE
Synonyms
UKRORGSYN-BB BBV-213844;N-methyl-3-nitro-4-pyridinamine;4-(METHYLAMINO)-3-NITROPYRIDINE;4-Pyridinamine, N-methyl-3-nitro-;4-(METHYLAMINO)-3-NITROPYRIDINE ISO 9001:2015 REACH
CBNumber
CB82446561
Molecular Formula
C6H7N3O2
Formula Weight
153.14
MOL File
1633-41-6.mol
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4-(METHYLAMINO)-3-NITROPYRIDINE Property

Melting point:
163 °C(Solv: water (7732-18-5); ethanol (64-17-5))
Boiling point:
299.5±25.0 °C(Predicted)
Density 
1.343±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
5.53±0.18(Predicted)
Appearance
Light yellow to yellow Solid
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Apolloscientific
Product number
OR962544
Product name
4-(Methylamino)-3-nitropyridine
Purity
98%
Packaging
1g
Price
$160
Updated
2021/12/16
Matrix Scientific
Product number
072556
Product name
4-(Methylamino)-3-nitropyridine
Purity
95+%
Packaging
250mg
Price
$231
Updated
2021/12/16
Apolloscientific
Product number
OR962544
Product name
4-(Methylamino)-3-nitropyridine
Purity
98%
Packaging
5g
Price
$405
Updated
2021/12/16
Matrix Scientific
Product number
072556
Product name
4-(Methylamino)-3-nitropyridine
Purity
95+%
Packaging
1g
Price
$500
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0077899
Product name
4-(METHYLAMINO)-3-NITROPYRIDINE
Purity
95.00%
Packaging
1G
Price
$721.57
Updated
2021/12/16
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4-(METHYLAMINO)-3-NITROPYRIDINE Chemical Properties,Usage,Production

Synthesis

13091-23-1

74-89-5

1633-41-6

Methylamine (25% aqueous, 10 mL, 63 mmol) was added slowly and dropwise to a dichloromethane (15 mL) suspension of 4-chloro-3-nitropyridine (2 g, 12.6 mmol). The reaction mixture was heated to 40 °C and stirred continuously for 1 hour. Upon completion of the reaction, the mixture was slowly poured into water (20 mL) and the resulting precipitate was collected by filtration and dried under vacuum to afford the target compound 4-methylamino-3-nitropyridine (1.9 g, 98% yield) as a yellow solid. The product was analyzed by LC-MS (ESI) and showed m/z: 154 (M + 1)+.

References

[1] Patent: US2010/35883, 2010, A1. Location in patent: Page/Page column 89
[2] Patent: WO2011/130661, 2011, A1. Location in patent: Page/Page column 173
[3] Patent: WO2005/26164, 2005, A1. Location in patent: Page/Page column 42
[4] Journal of Heterocyclic Chemistry, 1990, vol. 27, # 3, p. 563 - 566
[5] Patent: WO2008/12622, 2008, A2. Location in patent: Page/Page column 55

4-(METHYLAMINO)-3-NITROPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(METHYLAMINO)-3-NITROPYRIDINE Suppliers

Pure Chemistry Scientific Inc.
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View Lastest Price from 4-(METHYLAMINO)-3-NITROPYRIDINE manufacturers

Dideu Industries Group Limited
Product
4-(METHYLAMINO)-3-NITROPYRIDINE 1633-41-6
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-09-22