(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE

Product Name: (4-CHLORO-3-METHOXYPHENYL)ACETONITRILE
CAS No.: 13726-21-1
Chemical Name: (4-CHLORO-3-METHOXYPHENYL)ACETONITRILE
Synonyms: RARECHEM AL MP 0203;2-(4-Chloro-3-methoxyphenyl);(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE;2-(4-Chloro-3-Methoxyphenyl)acetonitrile;Benzeneacetonitrile, 4-chloro-3-methoxy-;2-(4-Chloro-3-methoxyphenyl)acetonitrilev
CBNumber: CB82452470
Molecular Formula: C9H8ClNO
Formula Weight: 181.62
MOL File: 13726-21-1.mol

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(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE Property

Melting point:: 170-178 °C
Boiling point:: 297.5±25.0 °C(Predicted)
Density: 1.198±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to light yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 6563AA
Product name: 2-(4-Chloro-3-methoxyphenyl)acetonitrile
Packaging: 1g
Price: $447
Updated: 2021/12/16

Matrix Scientific

Product number: 116087
Product name: (4-Chloro-3-methoxyphenyl)acetonitrile
Purity: >97%
Packaging: 500mg
Price: $544
Updated: 2021/12/16

Matrix Scientific

Product number: 116087
Product name: (4-Chloro-3-methoxyphenyl)acetonitrile
Purity: >97%
Packaging: 1g
Price: $730
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0314348
Product name: 4-CHLORO-3-METHOXY-BENZENEACETONITRILE
Purity: 95.00%
Packaging: 1G
Price: $808.5
Updated: 2021/12/16

Ambeed

Product number: A861924
Product name: 2-(4-Chloro-3-methoxyphenyl)acetonitrile
Purity: 98%
Packaging: 100mg
Price: $49
Updated: 2021/12/16

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(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE Chemical Properties,Usage,Production

Synthesis

143-33-9

103347-14-4

13726-21-1

To a 90% ethanol (500 mL) solution of 4-(bromomethyl)-1-chloro-2-methoxybenzene (68.5 g, 0.290 mol) was added sodium cyanide (28.5 g, 0.580 mol). The reaction mixture was stirred at 60 °C overnight. Upon completion of the reaction, the ethanol was removed by evaporation under reduced pressure and the residue was dissolved in water. The aqueous phase was extracted with ethyl acetate (300 mL × 3). The organic layers were combined, washed with saturated saline, and dried over anhydrous sodium sulfate. Purification by silica gel column chromatography (eluent: petroleum ether/ethyl acetate = 30:1) afforded 4-chloro-3-methoxyphenylacetonitrile (25 g, 48% yield).1H NMR (400 MHz, CDCl3) δ 7.36 (d, J = 8 Hz, 1H), 6.88-6.84 (m, 2H), 3.92 (s, 3H), 3.74 (s, 2H ).13C NMR (100 MHz, CDCl3) δ 155.4, 130.8, 129.7, 122.4, 120.7, 117.5, 111.5, 56.2, 23.5.

References

[1] Patent: US2007/244159, 2007, A1. Location in patent: Page/Page column 91
[2] Patent: US2005/239881, 2005, A1. Location in patent: Page/Page column 27
[3] Patent: WO2007/39736, 2007, A1. Location in patent: Page/Page column 28
[4] Patent: US2008/293775, 2008, A1. Location in patent: Page/Page column 22
[5] Patent: US2004/192704, 2004, A1. Location in patent: Page 23

(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE Suppliers

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13726-21-1, (4-CHLORO-3-METHOXYPHENYL)ACETONITRILERelated Search:

Benzeneacetonitrile (3-Methoxyphenyl)acetonitrile [3-(BENZYLOXY)-4-CHLOROPHENYL]ACETONITRILE 4-CHLORO-3-(TRIFLUOROMETHOXY)PHENYLACETONITRILE (4-CHLORO-3-HYDROXYPHENYL)ACETONITRILE (4-CHLORO-3-METHOXYPHENYL)ACETONITRILE

(4-CHLORO-3-METHOXYPHENYL)ACETONITRILE

RARECHEM AL MP 0203

2-(4-Chloro-3-Methoxyphenyl)acetonitrile

2-(4-Chloro-3-methoxyphenyl)

2-(4-Chloro-3-methoxyphenyl)acetonitrilev

Benzeneacetonitrile, 4-chloro-3-methoxy-

13726-21-1