4-BROMO-1-FLUORO-2-(PHENYLMETHOXY)BENZENE

Product Name: 4-BROMO-1-FLUORO-2-(PHENYLMETHOXY)BENZENE
CAS No.: 1036724-54-5
Chemical Name: 4-BROMO-1-FLUORO-2-(PHENYLMETHOXY)BENZENE
Synonyms: 2-(Benzyloxy)-4-broMo-1-fluorobenzene;4-BROMO-1-FLUORO-2-(PHENYLMETHOXY)BENZENE;Benzene, 4-bromo-1-fluoro-2-(phenylmethoxy)-
CBNumber: CB82460000
Molecular Formula: C13H10BrFO
Formula Weight: 281.12
MOL File: 1036724-54-5.mol

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4-BROMO-1-FLUORO-2-(PHENYLMETHOXY)BENZENE Property

Boiling point:: 337.8±27.0 °C(Predicted)
Density: 1.445±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B291603
Product name: 2-(Benzyloxy)-4-bromo-1-fluorobenzene
Packaging: 50mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: Y3569
Product name: 4-Bromo-1-fluoro-2-(phenylmethoxy)benzene
Packaging: 1g
Price: $116
Updated: 2021/12/16

Rieke Metals

Product number: B1789
Product name: 2-(benzyloxy)-4-bromo-1-fluorobenzene
Packaging: 1g
Price: $661
Updated: 2021/12/16

Rieke Metals

Product number: B1789
Product name: 2-(benzyloxy)-4-bromo-1-fluorobenzene
Packaging: 5g
Price: $1328
Updated: 2021/12/16

AOBChem

Product number: 16544
Product name: 4-Bromo-1-fluoro-2-(phenylmethoxy)benzene
Purity: 97%
Packaging: 5g
Price: $91
Updated: 2021/12/16

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4-BROMO-1-FLUORO-2-(PHENYLMETHOXY)BENZENE Chemical Properties,Usage,Production

Synthesis

100-39-0

112204-58-7

1036724-54-5

General procedure for the synthesis of 2-(benzyloxy)-4-bromo-1-fluorobenzene from benzyl bromide and 5-bromo-2-fluorophenol: To a solution of acetone (10 ml) containing the product of step a) (0.802 g, 4.20 mmol) and benzyl bromide (0.755 ml, 6.30 mmol) was added potassium carbonate (1.16 g, 8.40 mmol). The mixture was heated at reflux at 60°C for 16 hours. After completion of the reaction, the solid was removed by filtration and washed with acetone. The filtrate was evaporated to give the crude product. The residue was purified by fast chromatography using 0-20% ethyl acetate/isohexane as eluent, resulting in 1.04 g (88% yield) of 2-(benzyloxy)-4-bromo-1-fluorobenzene as an oil, which crystallized on cooling. The NMR hydrogen spectrum (400 MHz, CDCl3) data were as follows: δ 5.08 (2H, s), 6.98 (2H, m), 7.13 (1H, dd, J=7.4,2.2Hz), 7.37 (5H, m).

References

[1] Patent: WO2004/65388, 2004, A1. Location in patent: Page 47
[2] Patent: US2018/311255, 2018, A1. Location in patent: Paragraph 0204-0205

4-BROMO-1-FLUORO-2-(PHENYLMETHOXY)BENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-BROMO-1-FLUORO-2-(PHENYLMETHOXY)BENZENE Suppliers

China 35 India 1 United States 2 Global 38

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1036724-54-5, 4-BROMO-1-FLUORO-2-(PHENYLMETHOXY)BENZENERelated Search:

4-BROMO-1-FLUORO-2-(PHENYLMETHOXY)BENZENE

2-(Benzyloxy)-4-broMo-1-fluorobenzene

Benzene, 4-bromo-1-fluoro-2-(phenylmethoxy)-

1036724-54-5