Preparation
ChemicalBook > CAS DataBase List > 2-(4-CHLORO-2-NITROPHENYL)ACETIC ACID

2-(4-CHLORO-2-NITROPHENYL)ACETIC ACID

Preparation
Product Name
2-(4-CHLORO-2-NITROPHENYL)ACETIC ACID
CAS No.
37777-71-2
Chemical Name
2-(4-CHLORO-2-NITROPHENYL)ACETIC ACID
Synonyms
Nsc 115143;4-Chloro-2-Nitrobenzeneaceticacid;Benzeneacetic Acid,4-Chloro-2-Nitro-;2-(4-CHLORO-2-NITROPHENYL)ACETIC ACID;(4-CHLORO-2-NITRO-PHENYL)-ACETIC ACID
CBNumber
CB82464604
Molecular Formula
C8H6ClNO4
Formula Weight
215.59
MOL File
37777-71-2.mol
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2-(4-CHLORO-2-NITROPHENYL)ACETIC ACID Property

Melting point:
155 °C
Boiling point:
361.2±27.0 °C(Predicted)
Density 
1.532±0.06 g/cm3(Predicted)
pka
3.81±0.10(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C381960
Product name
2-(4-Chloro-2-nitrophenyl)aceticAcid
Packaging
100mg
Price
$60
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC147748
Product name
2-(4-Chloro-2-nitrophenyl)aceticacid
Packaging
250mg
Price
$82.5
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC147748
Product name
2-(4-Chloro-2-nitrophenyl)aceticacid
Packaging
500mg
Price
$145
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC147748
Product name
2-(4-Chloro-2-nitrophenyl)aceticacid
Packaging
1g
Price
$252
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC147748
Product name
2-(4-Chloro-2-nitrophenyl)aceticacid
Packaging
2g
Price
$439
Updated
2021/12/16
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2-(4-CHLORO-2-NITROPHENYL)ACETIC ACID Chemical Properties,Usage,Production

Preparation

The filtrate of Step A, above, is adjusted to pH 8-9 with 2 N sodium hydroxide and is heated at 35-40 °C. while adding a 3-6% aqueous hydrogen peroxide solu tion until samples no longer turn dark on treatment with 2N sodium hydroxide. The tan precipitate is suspended in 1500 ml. of water, adjusted to pH 8-9 and similarly treated with aqueous hydrogen peroxide. The combined reaction mixtures are then acidified with concentrated hydrochloride acid to obtain a precipitate which are re covered by filtration, washed 3 times with water and dried in vacuo. The crude product (mp 145-150°C) is recrystallized from ether to obtain 4-chloro-2-nitro phenylacetic acid, m.p. 156-159°C.

2-(4-CHLORO-2-NITROPHENYL)ACETIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(4-CHLORO-2-NITROPHENYL)ACETIC ACID Suppliers

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37777-71-2, 2-(4-CHLORO-2-NITROPHENYL)ACETIC ACIDRelated Search:


  • (4-CHLORO-2-NITRO-PHENYL)-ACETIC ACID
  • 2-(4-CHLORO-2-NITROPHENYL)ACETIC ACID
  • 4-Chloro-2-Nitrobenzeneaceticacid
  • Benzeneacetic Acid,4-Chloro-2-Nitro-
  • Nsc 115143
  • 37777-71-2