ChemicalBook > CAS DataBase List > (2S)-1,4-Dioxan-2-yl-methanol

(2S)-1,4-Dioxan-2-yl-methanol

Product Name: (2S)-1,4-Dioxan-2-yl-methanol
CAS No.: 406913-93-7
Chemical Name: (2S)-1,4-Dioxan-2-yl-methanol
Synonyms: (S)-(1,4-Dioxan-2-yl)Methanol;(2S)-1,4-Dioxane-2-methanol;(2S)-1,4-Dioxan-2-yl-methanol;1,4-Dioxane-2-methanol, (2S)-;(S)-2-(Hydroxymethyl)-1,4-dioxane;(2S)-1,4-Dioxan-2-yl-methanol, (2S)-1;Nantong Advanced Biomedical Technology Co., Ltd
CBNumber: CB82484640
Molecular Formula: C5H10O3
Formula Weight: 118.13
MOL File: 406913-93-7.mol

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(2S)-1,4-Dioxan-2-yl-methanol Property

Boiling point:: 208.2±15.0 °C(Predicted)
Density: 1.102
storage temp.: 2-8°C
pka: 14.24±0.10(Predicted)
Appearance: Colorless to light yellow Liquid
InChI: InChI=1S/C5H10O3/c6-3-5-4-7-1-2-8-5/h5-6H,1-4H2/t5-/m0/s1
InChIKey: CMEPUAROFJSGJN-YFKPBYRVSA-N
SMILES: O1CCOC[C@@H]1CO

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Safety

RIDADR: UN1993

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC

Product number: D486115
Product name: (S)-(1,4-Dioxan-2-yl)methanol
Packaging: 100mg
Price: $220
Updated: 2021/12/16

AK Scientific

Product number: J54798
Product name: (2S)-1,4-Dioxan-2-yl-methanol
Packaging: 1g
Price: $257
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD112027
Product name: (2S)-1,4-Dioxan-2-yl-methanol
Packaging: 250mg
Price: $400
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD112027
Product name: (2S)-1,4-Dioxan-2-yl-methanol
Packaging: 500mg
Price: $600
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD112027
Product name: (2S)-1,4-Dioxan-2-yl-methanol
Packaging: 1g
Price: $800
Updated: 2021/12/16

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(2S)-1,4-Dioxan-2-yl-methanol Chemical Properties,Usage,Production

Synthesis

917882-63-4

406913-93-7

General procedure for the synthesis of (S)-(1,4-dioxan-2-yl)methanol from the compound (CAS: 917882-63-4): palladium carbon (10% w/w, 192 mg) was added to an ethanol solution (20 mL) of intermediate 83 (1.25 g, 4.74 mmol). The reaction mixture was stirred under hydrogen atmosphere for 18 hours. After completion of the reaction, the mixture was filtered through diatomaceous earth and the filter cake was washed with ethyl acetate. The filtrate was concentrated under reduced pressure to give 600 mg of the target product in 89% yield. The product was characterized by 1H NMR (500 MHz, Chloroform-d) with chemical shifts δ (ppm): 3.85-3.67 (m, 5H), 3.66-3.57 (m, 2H), 3.55 (dd, J = 11.7, 5.9 Hz, 1H), 3.46 (dd, J = 11.1, 10.0 Hz, 1H), 1.75 (s, 1H).

References

[1] Patent: WO2016/91776, 2016, A1. Location in patent: Page/Page column 233
[2] Patent: US2006/293358, 2006, A1. Location in patent: Page/Page column 50
[3] Patent: US2009/182002, 2009, A1. Location in patent: Page/Page column 15
[4] Journal of Medicinal Chemistry, 2011, vol. 54, # 12, p. 4092 - 4108

(2S)-1,4-Dioxan-2-yl-methanol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from (2S)-1,4-Dioxan-2-yl-methanol manufacturers

Career Henan Chemical Co

Product: (2S)-1,4-Dioxan-2-yl-methanol 406913-93-7
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-02-16

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Nantong Advanced Biomedical Technology Co., Ltd

406913-93-7