4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine

Product Name: 4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine
CAS No.: 1014613-64-9
Chemical Name: 4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine
Synonyms: 4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine;1H-Pyrrolo[2,3-b]pyridine, 4-broMo-2-Methyl-;4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine 95%;(2R,3R,4R,5R)-2-(Acetoxymethyl)-5-(6-amino-9H-purin-9-yl)tetrahydrofuran-3,4-diyl diacetate
CBNumber: CB82487621
Molecular Formula: C8H7BrN2
Formula Weight: 211.06
MOL File: 1014613-64-9.mol

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4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine Property

Density: 1.654±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 13.52±0.40(Predicted)
form: solid
color: Light brown to brown

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H315Causes skin irritation

H318Causes serious eye damage

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P391Collect spillage. Hazardous to the aquatic environment

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B697660
Product name: 4-Bromo-2-methyl-1h-pyrrolo[2,3-b]pyridine
Packaging: 250mg
Price: $160
Updated: 2021/12/16

Apolloscientific

Product number: OR301166
Product name: 4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine
Packaging: 250mg
Price: $82
Updated: 2021/12/16

Matrix Scientific

Product number: 074509
Product name: 4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine
Purity: 95+%
Packaging: 500mg
Price: $245
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-9-52
Product name: 4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine
Purity: 95%
Packaging: 1g
Price: $375
Updated: 2021/12/16

Matrix Scientific

Product number: 074509
Product name: 4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine
Purity: 95+%
Packaging: 1g
Price: $453
Updated: 2021/12/16

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4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine Chemical Properties,Usage,Production

Synthesis

1014613-05-8

1014613-64-9

General procedure for the synthesis of 4-bromo-2-methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridine from 4-bromo-2-methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridine: To 4-bromo-2-methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridine (16 g, 0.045 mol) of 1,4-dioxane ( 320 mL) solution was added to 2M aqueous sodium hydroxide solution (114 mL, 0.228 mol). The reaction mixture was heated to 60°C and kept for 16 hours. After the reaction was completed, the mixture was cooled to room temperature. The organic layer was separated and the aqueous layer was extracted with ethyl acetate. The organic phases were combined, washed with saturated brine, dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure to give 4-bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine as a milky white solid (10.07 g, 104% yield). lC/MS (Method B): m/z 211/213 [M+H]+, retention time 1.04 min.

References

[1] Patent: WO2009/112475, 2009, A1. Location in patent: Page/Page column 62
[2] Bioorganic and Medicinal Chemistry Letters, 2009, vol. 19, # 9, p. 2504 - 2508
[3] Patent: US2010/160647, 2010, A1. Location in patent: Page/Page column 21
[4] Patent: WO2012/170752, 2012, A1. Location in patent: Page/Page column 42
[5] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 15, p. 4344 - 4353

4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine Suppliers

China 58 India 1 United Kingdom 1 United States 7 Global 67

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View Lastest Price from 4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine manufacturers

Career Henan Chemical Co

Product: 4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine 1014613-64-9
Price: US $1.00/g
Min. Order: 1g
Purity: 95--99%
Supply Ability: 1ton
Release date: 2020-01-09

1014613-64-9, 4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridineRelated Search:

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4-Bromo-2-methyl-1H-pyrrolo[2,3-b]pyridine 95%

1014613-64-9

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