ChemicalBook > CAS DataBase List > 2-Amino-5-(trifluoromethyl)benzyl alcohol

2-Amino-5-(trifluoromethyl)benzyl alcohol

Product Name: 2-Amino-5-(trifluoromethyl)benzyl alcohol
CAS No.: 220107-65-3
Chemical Name: 2-Amino-5-(trifluoromethyl)benzyl alcohol
Synonyms: 2-Amino-5-(trifluoromethyl)benzyl alcohol;2-Amino-5-(trifluoromethyl)benzenemethanol;Benzenemethanol, 2-amino-5-(trifluoromethyl)-
CBNumber: CB82491475
Molecular Formula: C8H8F3NO
Formula Weight: 191.15
MOL File: 220107-65-3.mol

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2-Amino-5-(trifluoromethyl)benzyl alcohol Property

Boiling point:: 270℃
Density: 1.374
Flash point:: 117℃
storage temp.: 2-8°C(protect from light)
pka: 14.02±0.10(Predicted)
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 8867CZ
Product name: 2-Amino-5-(trifluoromethyl)benzylalcohol
Packaging: 5g
Price: $937
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0103717
Product name: 2-AMINO-5-(TRIFLUOROMETHYL)BENZYL ALCOHOL
Purity: 95.00%
Packaging: 5MG
Price: $495.8
Updated: 2021/12/16

BLDpharm

Product number: BD161184
Product name: (2-Amino-5-(trifluoromethyl)phenyl)methanol
Purity: 97%
Packaging: 5g
Price: $663
Updated: 2021/12/16

Crysdot

Product number: CD12095273
Product name: (2-Amino-5-(trifluoromethyl)phenyl)methanol
Purity: 95+%
Packaging: 5g
Price: $673
Updated: 2021/12/16

Ambeed

Product number: A301949
Product name: (2-Amino-5-(trifluoromethyl)phenyl)methanol
Purity: 97%
Packaging: 5g
Price: $680
Updated: 2021/12/16

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2-Amino-5-(trifluoromethyl)benzyl alcohol Chemical Properties,Usage,Production

Synthesis

83265-53-6

220107-65-3

The general procedure for the synthesis of (2-amino-5-(trifluoromethyl)phenyl)methanol from 2-amino-5-trifluoromethylbenzoic acid was carried out as follows: firstly, compound 24a was prepared from compound 22b according to the literature method, which was followed by the synthesis of the target product 28b. The yield of this step was 84% and the product was a yellow amorphous solid. The main absorption peaks were located at 3389, 2918, 1461, 1274, 1122 cm-1 as detected by infrared spectroscopy (IR, KBr). nuclear magnetic resonance hydrogen spectroscopy (1H NMR, 300 MHz, CDCl3) showed δ-values: 1.26-1.34 (1H, m), 2.09 (1H, dt, J = 5.1, 12.6 Hz), 2.27 ( 1H, dt, J = 2.4, 12.0 Hz), 2.39-2.50 (1H, m), 2.43 (3H, s), 2.89 (1H, d, J = 6.3 Hz), 2.96-2.99 (2H, m), 3.08 (1H, d, J = 17.7 Hz), 3.27 (1H, d, J = 17.7 Hz), 3.49 (1H, d, J = 17.4 Hz), 1H, d, J = 17.7 Hz), 3.49 (1H, d, J = 17.4 Hz), 3.09 (1H, dt, J = 5.1, 12.6 Hz) d, J = 17.4 Hz), 3.69 (1H, d, J = 17.7 Hz), 6.68 (1H, dd, J = 2.1, 8.3 Hz), 7.01 (2H, d, J = 8.3 Hz), 7.04 (1H, d, J = 2.1 Hz), 7.28 (1H, d, J = 8.3 Hz), 7.58 (1H, s), 7.63 ( 1H, s), where two protons (OH) were not observed. The nuclear magnetic resonance carbon spectrum (13C NMR, 75 MHz, CDCl3) showed δ-values: 23.9, 35.8, 36.1, 38.8, 40.3, 42.9, 45.4, 61.5, 69.3, 113.1, 115.2, 123.78 (q, J = 270.5 Hz), 123.79 (q, J = 3.1 Hz), 124.5 (q, J = 4.3 Hz), 125.7, 126.8, 127.0 (q, J = 32.3 Hz), 127.7, 129.0, 129.9, 136.6, 140.4, 145.9, 155.4, 160.0. High-resolution mass spectrometry (HRMS, ESI) showed that the calculated values of [M + H]+ were C25H24F3N2O2, 441.1790; the measured value was 441.1775.

References

[1] Bioorganic and Medicinal Chemistry, 2012, vol. 20, # 19, p. 5810 - 5831
[2] Patent: US6369221, 2002, B1. Location in patent: Page column 37

2-Amino-5-(trifluoromethyl)benzyl alcohol Preparation Products And Raw materials

Raw materials

Preparation Products

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220107-65-3, 2-Amino-5-(trifluoromethyl)benzyl alcoholRelated Search:

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2-Amino-5-(trifluoromethyl)benzenemethanol

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220107-65-3

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