ChemicalBook > CAS DataBase List > 3-BroMo-5-(trifluoroMethyl)anisole
3-BroMo-5-(trifluoroMethyl)anisole
- Product Name
- 3-BroMo-5-(trifluoroMethyl)anisole
- CAS No.
- 627527-23-5
- Chemical Name
- 3-BroMo-5-(trifluoroMethyl)anisole
- Synonyms
- 3-Bromo-5-methoxybenzotrifluoride;3-BroMo-5-(trifluoroMethyl)anisole;1-Bromo-3-methoxy-5-trifluoromethylbenzene;Benzene, 1-bromo-3-methoxy-5-(trifluoromethyl)-
- CBNumber
- CB82502575
- Molecular Formula
- C8H6BrF3O
- Formula Weight
- 255.03
- MOL File
- 627527-23-5.mol
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3-BroMo-5-(trifluoroMethyl)anisole Property
- Boiling point:
- 201℃
- Density
- 1.563
- Flash point:
- 93℃
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Colorless to light yellow Liquid
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Safety
- HS Code
- 2909309090
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
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N-Bromosuccinimide Price
TRC
- Product number
- B700338
- Product name
- 1-Bromo-3-methoxy-5-(trifluoromethyl)benzene
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
Apolloscientific
- Product number
- PC499010
- Product name
- 3-Bromo-5-methoxybenzotrifluoride
- Packaging
- 1g
- Price
- $37
- Updated
- 2021/12/16
Apolloscientific
- Product number
- PC499010
- Product name
- 3-Bromo-5-methoxybenzotrifluoride
- Packaging
- 5g
- Price
- $106
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 2807-B-11
- Product name
- 1-Bromo-3-methoxy-5-(trifluoromethyl)benzene
- Purity
- 96%
- Packaging
- 250mg
- Price
- $251
- Updated
- 2021/12/16
AK Scientific
- Product number
- Z0739
- Product name
- 1-Bromo-3-(trifluoromethyl)-5-methoxybenzene
- Packaging
- 10g
- Price
- $284
- Updated
- 2021/12/16
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3-BroMo-5-(trifluoroMethyl)anisole Chemical Properties,Usage,Production
Chemical Properties
light yellow liquid
Synthesis
349-55-3
627527-23-5
1. 3-Methoxy-5-trifluoromethylaniline (20 g, 104.6 mmol) was added batchwise to a cooled solution of sodium nitrite (7.392 g, 107.1 mmol) in sulfuric acid (74 ml) and acetic acid (88 ml). 2. The mixture was added dropwise to a vigorously stirred solution of cuprous bromide (18 g, 62.8 mmol) in 48% hydrobromic acid (200 ml) at 0°C. 3. The reaction mixture was stirred for 45 minutes at room temperature. 4. The reaction mixture was poured into ice water and the aqueous phase was extracted with dichloromethane. 5. The organic layer was separated. (200 ml) solution. 3. The reaction mixture was stirred at room temperature for 45 min. 4. The reaction mixture was poured into ice water and the aqueous phase was extracted with dichloromethane. 5. The organic layer was separated, dried with anhydrous magnesium sulfate, filtered and the solvent was evaporated at low temperature. 6. The residue was stirred in sodium bicarbonate solution and extracted with diisopropyl ether. 7. The organic layer was separated, dried with anhydrous magnesium sulfate, filtered and the solvent was evaporated to obtain intermediate 3-bromo-5-bromo-5-hydroxybromide. 8. The intermediate 3-bromo-5-trifluoromethyl anisole was obtained (12.7 g, 48% yield).
References
[1] Patent: WO2011/33018, 2011, A1. Location in patent: Page/Page column 38
[2] Patent: US2012/172354, 2012, A1. Location in patent: Page/Page column 17
3-BroMo-5-(trifluoroMethyl)anisole Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-BroMo-5-(trifluoroMethyl)anisole manufacturers
Honest Joy Holdings Limited
- Product
- 1-Bromo-3-methoxy-5-(trifluoromethyl)benzene 627527-23-5
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 97.7%
- Supply Ability
- 100 tons
- Release date
- 2022-01-14
Career Henan Chemical Co
- Product
- 3-BroMo-5-(trifluoroMethyl)anisole 627527-23-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2020-01-11