ChemicalBook > CAS DataBase List > 3-Phenylisothiazol-5-amine
3-Phenylisothiazol-5-amine
- Product Name
- 3-Phenylisothiazol-5-amine
- CAS No.
- 14208-52-7
- Chemical Name
- 3-Phenylisothiazol-5-amine
- Synonyms
- 3-Phenylisothiazol-5-amine;5-Isothiazolamine, 3-phenyl-;3-phenyl-1,2-thiazol-5-aMine;3-Phenyl-isothiazol-5-ylamine
- CBNumber
- CB82515852
- Molecular Formula
- C9H8N2S
- Formula Weight
- 176.24
- MOL File
- 14208-52-7.mol
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3-Phenylisothiazol-5-amine Property
- Melting point:
- 163 °C
- Boiling point:
- 269.8±38.0 °C(Predicted)
- Density
- 1.261±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- pka
- 6.88±0.20(Predicted)
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N-Bromosuccinimide Price
TRC
- Product number
- P321720
- Product name
- 3-phenylisothiazol-5-amine
- Packaging
- 50mg
- Price
- $130
- Updated
- 2021/12/16
AK Scientific
- Product number
- 6929AA
- Product name
- 3-Phenylisothiazol-5-amine
- Packaging
- 5g
- Price
- $2480
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- CHM0376228
- Product name
- 3-PHENYLISOTHIAZOL-5-AMINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.25
- Updated
- 2021/12/16
Ambeed
- Product number
- A131701
- Product name
- 3-Phenylisothiazol-5-amine
- Purity
- 95+%
- Packaging
- 5g
- Price
- $1395
- Updated
- 2021/12/16
Chemenu
- Product number
- CM189858
- Product name
- 3-Phenylisothiazol-5-amine
- Purity
- 95%
- Packaging
- 5g
- Price
- $1683
- Updated
- 2021/12/16
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3-Phenylisothiazol-5-amine Chemical Properties,Usage,Production
Synthesis
17196-74-6
14208-52-7
In a sealed tube, (Z)-3-amino-3-phenylacrylonitrile (95 mg, 0.660 mmol) was dissolved in a solvent mixture of EtOH (1.0 mL) and THF (1.0 mL). H2S gas was bubbled into the solution for 5 min. Subsequently, the reaction mixture was stirred at 90 °C for 20 hours. Upon completion of the reaction, the mixture was concentrated under reduced pressure. The concentrated residue was dissolved in MeOH (2.0 mL) and H2O2 (30%, 0.5 mL) was added. The reaction was terminated by stirring at room temperature for 2 min. The mixture was again concentrated under reduced pressure. Finally, the residue was purified by high performance liquid chromatography (HPLC) to afford the target product 3-phenylisothiazol-5-amine (22 mg).
References
[1] Patent: US2013/131040, 2013, A1. Location in patent: Paragraph 1140
3-Phenylisothiazol-5-amine Preparation Products And Raw materials
Raw materials
Preparation Products
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