ChemicalBook > CAS DataBase List > N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamine

N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamine

Product Name
N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamine
CAS No.
1086111-20-7
Chemical Name
N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamine
Synonyms
diethyl({2-[4-(tetraMethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl]ethyl})aMine;N,N-Diethyl-4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole-1-ethanaMine;N,N-diethyl-2-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrazol-1-yl]ethanamine;1H-Pyrazole-1-ethanamine, N,N-diethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-;N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamine;diethyl({2-[4-(tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl]ethyl})amine - [D16474]
CBNumber
CB82520274
Molecular Formula
C15H28BN3O2
Formula Weight
293.21
MOL File
1086111-20-7.mol
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N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamine Property

Boiling point:
394.6±22.0 °C(Predicted)
Density 
1.02±0.1 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
9.84±0.25(Predicted)
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific
Product number
1712AA
Product name
N,N-Diethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole-1-ethanamine
Packaging
250mg
Price
$176
Updated
2021/12/16
Synthonix
Product number
D16474
Product name
diethyl({2-[4-(tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl]ethyl})amine
Purity
97.0%
Packaging
1g
Price
$280
Updated
2021/12/16
AK Scientific
Product number
1712AA
Product name
N,N-Diethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole-1-ethanamine
Packaging
1g
Price
$350
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
BOR0007320
Product name
N,N-DIETHYL-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-1H-PYRAZOLE-1-ETHANAMINE
Purity
95.00%
Packaging
5MG
Price
$497.08
Updated
2021/12/16
Matrix Scientific
Product number
096378
Product name
N,N-Diethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole-1-ethanamine
Purity
95+%
Packaging
250mg
Price
$545
Updated
2021/12/16
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N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamine Chemical Properties,Usage,Production

Synthesis

269410-08-4

5392-81-4

1086111-20-7

A solution was prepared in tetrahydrofuran at 0°C using 4-pyrazoleboronic acid pinacol ester (250 mg, 1.29 mmol) and sodium hydride (61.8 mg, 2.58 mmol) as starting materials. Subsequently, 2-bromo-N,N-diethylethylamine (558 mg, 2.58 mmol) was added to the solution. The reaction system was slowly warmed up to room temperature and the progress of the reaction was monitored by LCMS.After 90 min, if the reaction did not take place, potassium iodide (1.71 g, 10.3 mmol) was added and the reaction mixture was heated at 50 °C overnight. After completion of the reaction, the reaction mixture was diluted with a large amount of ethyl acetate and water and liquid-liquid partitioning was performed. The organic layer containing the target product was collected, washed with brine and concentrated by vacuum to give a clear thick oily product. It was analyzed by LCMS and confirmed to be pure N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethylamine (340 mg, 90% yield, M + 1 294.2).

References

[1] Patent: US2012/245144, 2012, A1. Location in patent: Page/Page column 118

N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamine Preparation Products And Raw materials

Raw materials

Preparation Products

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N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamine Suppliers

Capot Chemical Co., Ltd
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+86 (0) 571 85 58 67 18
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0086-571-85864795
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China
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ShangHai AmK Pharmaceutical Technology Co., Ltd.
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微信 17321281695 18019252918
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17321281695
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sale@amkchem.com
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Amadis Chemical Company Limited
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Yantai ShengKailun Chemical Technology Co., Ltd.
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Capot Chemical Co.,Ltd.
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Aikon International Limited
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1086111-20-7, N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamineRelated Search:


  • N,N-diethyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl)ethanamine
  • diethyl({2-[4-(tetraMethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl]ethyl})aMine
  • N,N-Diethyl-4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole-1-ethanaMine
  • 1H-Pyrazole-1-ethanamine, N,N-diethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-
  • N,N-diethyl-2-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrazol-1-yl]ethanamine
  • diethyl({2-[4-(tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazol-1-yl]ethyl})amine - [D16474]
  • 1086111-20-7
  • C15H28BN3O2