1-Boc-1H-pyrrolo[3,2-c]pyridine
- Product Name
- 1-Boc-1H-pyrrolo[3,2-c]pyridine
- CAS No.
- 148760-75-2
- Chemical Name
- 1-Boc-1H-pyrrolo[3,2-c]pyridine
- Synonyms
- 1-Boc-1H-pyrrolo[3,2-c]pyridine;1-Boc-pyrrolo[3,2-c]pyridine, 95%;1H-Pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester;1H-Pyrrolo[3,2-c]pyridine-1-carboxylic acid, 1,1-diMethylethyl ester
- CBNumber
- CB82533920
- Molecular Formula
- C12H14N2O2
- Formula Weight
- 218.25
- MOL File
- 148760-75-2.mol
1-Boc-1H-pyrrolo[3,2-c]pyridine Property
- Boiling point:
- 339.3±34.0 °C(Predicted)
- Density
- 1.14±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 7.02±0.30(Predicted)
N-Bromosuccinimide Price
- Product number
- B810118
- Product name
- tert-Butyl1H-Pyrrolo[3,2-c]pyridine-1-carboxylate
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B810118
- Product name
- tert-Butyl1H-Pyrrolo[3,2-c]pyridine-1-carboxylate
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 126747
- Product name
- tert-Butyl1H-pyrrolo[3,2-c]pyridine-1-carboxylate
- Purity
- >95%
- Packaging
- 1g
- Price
- $258
- Updated
- 2021/12/16
- Product number
- 126747
- Product name
- tert-Butyl1H-pyrrolo[3,2-c]pyridine-1-carboxylate
- Purity
- >95%
- Packaging
- 5g
- Price
- $892
- Updated
- 2021/12/16
- Product number
- CHM0096878
- Product name
- TERT-BUTYL-1H-PYRROLO[3,2-C]PYRIDINE-1-CARBOXYLATE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $924
- Updated
- 2021/12/16
1-Boc-1H-pyrrolo[3,2-c]pyridine Chemical Properties,Usage,Production
Synthesis
271-34-1
24424-99-5
148760-75-2
Step A: Preparation of tert-butyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate: To a stirred mixture of 5-azaindole (2.3 g, 20 mmol) and 4-dimethylaminopyridine (2.4 g, 20 mmol) in acetonitrile (20 mL) was added di-tert-butyl dicarbonate (3.9 g, 18 mmol). The reaction mixture was stirred at room temperature for 18 hours. Upon completion of the reaction, the mixture was concentrated under reduced pressure and subsequently purified by Biotage Flash 40S column chromatography using 1:1 ethyl acetate/hexane as eluent. The target product 1H-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester was obtained as a colorless oil (4.0 g, 101% yield).
References
[1] Patent: US2007/238726, 2007, A1. Location in patent: Page/Page column 114
[2] Patent: WO2017/23987, 2017, A1. Location in patent: Paragraph 0703; 0704
[3] Patent: WO2017/24003, 2017, A1. Location in patent: Paragraph 0703; 0704
[4] Patent: WO2017/24010, 2017, A1. Location in patent: Paragraph 0650; 0651
[5] Patent: WO2017/23984, 2017, A1. Location in patent: Paragraph 0703
1-Boc-1H-pyrrolo[3,2-c]pyridine Preparation Products And Raw materials
Raw materials
Preparation Products
1-Boc-1H-pyrrolo[3,2-c]pyridine Suppliers
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