(5-iodo-2-Methylphenyl)Methanol

Product Name: (5-iodo-2-Methylphenyl)Methanol
CAS No.: 1260242-01-0
Chemical Name: (5-iodo-2-Methylphenyl)Methanol
Synonyms: 5-Iodo-2-methylbenzyl Alcohol;5-Iodo-2-methylbenzenemethanol;(5-iodo-2-Methylphenyl)Methanol;Benzenemethanol, 5-iodo-2-methyl-
CBNumber: CB82574257
Molecular Formula: C8H9IO
Formula Weight: 248.06
MOL File: 1260242-01-0.mol

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(5-iodo-2-Methylphenyl)Methanol Property

storage temp.: 2-8°C(protect from light)
Appearance: Brown to reddish brown Solid
InChI: InChI=1S/C8H9IO/c1-6-2-3-8(9)4-7(6)5-10/h2-4,10H,5H2,1H3
InChIKey: CIEQOCDUTRABFK-UHFFFAOYSA-N
SMILES: C1(CO)=CC(I)=CC=C1C

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Safety

HS Code: 2906290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B449575
Product name: (5-iodo-2-methylphenyl)methanol
Packaging: 10mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: 1761DP
Product name: (5-Iodo-2-methylphenyl)methanol
Packaging: 5g
Price: $451
Updated: 2021/12/16

Chemenu

Product number: CM248556
Product name: (5-Iodo-2-methylphenyl)methanol
Purity: 95+%
Packaging: 10g
Price: $468
Updated: 2021/12/16

Alichem

Product number: 1260242010
Product name: 5-Iodo-2-methylbenzylalcohol
Packaging: 250mg
Price: $489.6
Updated: 2021/12/16

Crysdot

Product number: CD12168059
Product name: (5-Iodo-2-methylphenyl)methanol
Purity: 97%
Packaging: 10g
Price: $495
Updated: 2021/12/16

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(5-iodo-2-Methylphenyl)Methanol Chemical Properties,Usage,Production

Synthesis

612833-45-1

1260242-01-0

Step 3: Synthesis of (5-iodo-2-methylphenyl)methanol To a solution of THF (300 mL) containing ester 4 (41.0 g, 141 mmol) was slowly added lithium borohydride (2.0 M solution of THF, 212 mL). The reaction mixture was heated to reflux and stirred overnight. Upon completion of the reaction, the mixture was cooled to 0 °C and water was carefully added to quench the reaction, followed by the addition of saturated NH4Cl solution. The reaction mixture was diluted with water and extracted with EtOAc. The organic layers were combined, washed with brine, dried over anhydrous MgSO4, filtered and concentrated under reduced pressure to afford the title compound (5-iodo-2-methylphenyl)methanol (34.0 g, 97% yield) as a white solid, which could be used in the next reaction without further purification. [M-OH]+ m/z: 231.

References

[1] Patent: WO2011/159067, 2011, A2. Location in patent: Page/Page column 51

(5-iodo-2-Methylphenyl)Methanol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from (5-iodo-2-Methylphenyl)Methanol manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: (5-iodo-2-Methylphenyl)Methanol 1260242-01-0
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-06-27

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1260242-01-0