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3-BroMo-1-Methyl-pyrrolidine

Application
Product Name
3-BroMo-1-Methyl-pyrrolidine
CAS No.
10603-45-9
Chemical Name
3-BroMo-1-Methyl-pyrrolidine
Synonyms
3-BroMo-1-Methyl-pyrrolidine;Pyrrolidine, 3-bromo-1-methyl-;3-Bromo-1-methylpyrrolidine,97%
CBNumber
CB82580454
Molecular Formula
C5H10BrN
Formula Weight
164.04
MOL File
10603-45-9.mol
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3-BroMo-1-Methyl-pyrrolidine Property

Boiling point:
153-159 °C
Density 
1.361 g/mL at 25 °C
Flash point:
54 °C
refractive index 
1.4910
storage temp. 
2-8°C
form 
Liquid
pka
8.53±0.40(Predicted)
color 
Yellow to brown
Sensitive 
Moisture Sensitive
InChI
InChI=1S/C5H10BrN/c1-7-3-2-5(6)4-7/h5H,2-4H2,1H3
InChIKey
ZHUYTHOKJZSZQJ-UHFFFAOYSA-N
SMILES
N1(C)CCC(Br)C1
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Safety

Hazard Codes 
F,C
Risk Statements 
11-34
Safety Statements 
26-36/37/39-45
RIDADR 
UN 2924 8(3) / PGIII
WGK Germany 
WGK 3
HazardClass 
3
PackingGroup 
Storage Class
3 - Flammable liquids
Hazard Classifications
Eye Irrit. 2
Flam. Liq. 3
Skin Corr. 1B
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H226Flammable liquid and vapour

H314Causes severe skin burns and eye damage

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P233Keep container tightly closed.

P240Ground/bond container and receiving equipment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
721867
Product name
3-Bromo-1-methylpyrrolidine
Purity
97%
Packaging
500MG
Price
$89.5
Updated
2023/06/20
TRC
Product number
B681050
Product name
3-Bromo-1-methylpyrrolidine
Packaging
100mg
Price
$65
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB159636
Product name
3-Bromo-1-methylpyrrolidine
Packaging
10mg
Price
$53
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0364390
Product name
3-BROMO-1-METHYLPYRROLIDINE
Purity
95.00%
Packaging
250MG
Price
$152.25
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB159636
Product name
3-Bromo-1-methylpyrrolidine
Packaging
50mg
Price
$155
Updated
2021/12/16
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3-BroMo-1-Methyl-pyrrolidine Chemical Properties,Usage,Production

Application

3-Bromo-1-methylpyrrolidine is a colorless liquid and an important pharmaceutical intermediate. It can be used to prepare mGluR5 receptor allosteric modulators.

Synthesis

3-Hydroxy-1-methylpyrrolidine (5 g) was added in a 100 ml single-necked flask, n-hexane (50 ml) was cooled in an ice bath for 10 min, phosphorus tribromide (16.9 g) was added under cooling, and the temperature was raised to reflux for 2 h. Cooling was carried out. Neutralized to pH>8 by adding 25% KOH. extracted with ether. Combine the organic phases, add 1N hydrochloric acid 50ml, extract. Retain the aqueous phase, adjust pH>8, ether extract. Air dry. Obtained 3-bromo-1-methylpyrrolidine (1.1g).

3-BroMo-1-Methyl-pyrrolidine Preparation Products And Raw materials

Raw materials

Preparation Products

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3-BroMo-1-Methyl-pyrrolidine Suppliers

Shanghai C&W New Material Co., Ltd.
Tel
021-22062033 15921412618
Email
sales@c-wnewmaterial.com
Country
China
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Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
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42934
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64
Syntechem Co.,Ltd
Tel
Fax
E-Mail Inquiry
Email
info@syntechem.com
Country
China
ProdList
12984
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Amber MolTech LLC
Tel
086-010-62176588
Fax
086-010-62117849
Email
amber@jyamber.com
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China
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10151
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SynAsst Chemical.
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021-60343070
Fax
021-35122006
Country
China
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Chengdu Firster Pharmaceutical Co., Ltd.
Tel
028-87078428 028-87074958
Fax
8772-8116
Email
chengzhenyong@cdfirster.com
Country
China
ProdList
2598
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Shanghai HuanChuan Industry Co.,Ltd.
Tel
021-61478794
Fax
021-61478794
Email
sales@hcshhai.com
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China
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Sigma-Aldrich
Tel
021-61415566 800-8193336
Email
orderCN@merckgroup.com
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China
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TaiChem Taizhou Limited
Tel
052386810091
Email
zcwy9518@yeah.net
Country
China
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Shanghai YuanYe Biotechnology Co., Ltd.
Tel
021-61312847; 18021002903
Fax
QQ:3008007432
Email
3008007409@qq.com
Country
China
ProdList
89689
Advantage
60
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View Lastest Price from 3-BroMo-1-Methyl-pyrrolidine manufacturers

Career Henan Chemical Co
Product
3-BroMo-1-Methyl-pyrrolidine 10603-45-9
Price
US $1.00/KG
Min. Order
1KG
Purity
98%-99.9%
Supply Ability
200kg
Release date
2020-01-10

10603-45-9, 3-BroMo-1-Methyl-pyrrolidineRelated Search:


  • 3-BroMo-1-Methyl-pyrrolidine
  • Pyrrolidine, 3-bromo-1-methyl-
  • 3-Bromo-1-methylpyrrolidine,97%
  • 10603-45-9