ChemicalBook > CAS DataBase List > 6-broMo-1,2,4-triazin-3-aMine

6-broMo-1,2,4-triazin-3-aMine

Product Name
6-broMo-1,2,4-triazin-3-aMine
CAS No.
69249-22-5
Chemical Name
6-broMo-1,2,4-triazin-3-aMine
Synonyms
3-AMino-6-broMo-1,2,4-triazine;INC280-3;3-Amino-6-bromo-1;Amino-6-bromo-1,2,4-triazine;broMo-1,2,4-triazin-3-a Mine;3-amine-6-bromo-1,2,4-triazin;6-broMo-1,2,4-triazin-3-aMine;3-Amine-6-bromo-1,2,4-triazine;6-BroMo-1,2,4-triazine-3-aMine;1,2,4-Triazin-3-amine, 6-bromo-
CBNumber
CB82599324
Molecular Formula
C3H3BrN4
Formula Weight
174.99
MOL File
69249-22-5.mol
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6-broMo-1,2,4-triazin-3-aMine Property

Boiling point:
373.6±34.0 °C(Predicted)
Density 
1.998±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
2.02±0.63(Predicted)
Appearance
Light yellow to brown Solid
InChI
InChI=1S/C3H3BrN4/c4-2-1-6-3(5)8-7-2/h1H,(H2,5,6,8)
InChIKey
WIBIPFPOGMLYJQ-UHFFFAOYSA-N
SMILES
N1C(Br)=CN=C(N)N=1
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Safety

HS Code 
2933698090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific
Product number
OR930027
Product name
6-Bromo-1,2,4-triazin-3-amine
Purity
95%
Packaging
1g
Price
$30
Updated
2021/12/16
Apolloscientific
Product number
OR930027
Product name
6-Bromo-1,2,4-triazin-3-amine
Purity
95%
Packaging
5g
Price
$89
Updated
2021/12/16
AK Scientific
Product number
6428AJ
Product name
6-Bromo-1,2,4-triazin-3-amine
Packaging
1g
Price
$105
Updated
2021/12/16
SynQuest Laboratories
Product number
3H30-9-0N
Product name
6-Bromo-1,2,4-triazin-3-amine
Purity
97%
Packaging
1g
Price
$125
Updated
2021/12/16
SynQuest Laboratories
Product number
3H30-9-0N
Product name
6-Bromo-1,2,4-triazin-3-amine
Purity
97%
Packaging
5G
Price
$272
Updated
2021/12/16
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6-broMo-1,2,4-triazin-3-aMine Chemical Properties,Usage,Production

Flammability and Explosibility

Flammable

Synthesis

1120-99-6

69249-22-5

General procedure for the synthesis of 3-amino-6-bromo-1,2,4-triazine from 1,2,4-triazin-3-amine: 3-amino-1,2,4-triazine (I) (0.96 g, 10 mmol) was dissolved in 100 mL of N,N-dimethylformamide (DMF) with thorough stirring. A 100 mL DMF solution of N-bromosuccinimide (NBS) (17.8 g, 100 mmol) was added slowly and dropwise under the cooling of an ice bath. The reaction temperature was maintained between 0-30 °C with continuous stirring for 12 hours. After completion of the reaction, sodium hydroxide (12 g, 300 mmol) was added to the reaction mixture for neutralization. The precipitate was collected by filtration and dried to afford the target product 3-amino-6-bromo-1,2,4-triazine (1.43 g, 81.7% yield).

References

[1] Patent: CN108129409, 2018, A. Location in patent: Paragraph 0043; 0044; 0045
[2] Journal of the American Chemical Society, 2015, vol. 137, # 26, p. 8388 - 8391
[3] Patent: US2016/251361, 2016, A1. Location in patent: Paragraph 1004-1006
[4] Russian Chemical Bulletin, 2014, vol. 63, # 6, p. 1359 - 1363
[5] Izv. Akad. Nauk, Ser. Khim., 2014, # 6, p. 1359 - 1363,5

6-broMo-1,2,4-triazin-3-aMine Preparation Products And Raw materials

Raw materials

Preparation Products

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6-broMo-1,2,4-triazin-3-aMine Suppliers

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View Lastest Price from 6-broMo-1,2,4-triazin-3-aMine manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
6-broMo-1,2,4-triazin-3-aMine 69249-22-5
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1Ton
Release date
2022-10-08
Nanjing Fred Technology Co., Ltd
Product
6-Bromo-1,2,4-triazin-3-amine 69249-22-5
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1 ton
Release date
2023-12-21
Henan Fengda Chemical Co., Ltd
Product
6-broMo-1,2,4-triazin-3-aMine 69249-22-5
Price
US $5.00-0.10/KG
Min. Order
1KG
Purity
98%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-04-09

69249-22-5, 6-broMo-1,2,4-triazin-3-aMineRelated Search:

Pyrazole-4-carbonitrile, 3-amino-1-isopropyl- (7CI)

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  • 6-BroMo-1,2,4-triazine-3-aMine
  • 3-AMino-6-broMo-1,2,4-triazine
  • INC280-3
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  • 1,2,4-Triazin-3-amine, 6-bromo-
  • 3-amine-6-bromo-1,2,4-triazin
  • 3-Amino-6-bromo-1
  • broMo-1,2,4-triazin-3-a Mine
  • Amino-6-bromo-1,2,4-triazine
  • 3-Amine-6-bromo-1,2,4-triazine
  • 6-broMo-1,2,4-triazin-3-aMine CAS：
  • 69249-22-5
  • C3H3BrN4
  • Heterocycle-other series