ChemicalBook > CAS DataBase List > 5-BroMo-6-hydroxypicolinic acid

5-BroMo-6-hydroxypicolinic acid

Product Name: 5-BroMo-6-hydroxypicolinic acid
CAS No.: 1214385-51-9
Chemical Name: 5-BroMo-6-hydroxypicolinic acid
Synonyms: 5-BroMo-6-hydroxypicolinic acid;5-bromo-6-hydroxypyridine-2-carboxylic acid;5-bromo-6-oxo-1H-pyridine-2-carboxylic acid;5-bromo-6-oxo-1,6-dihydropyridine-2-carboxylic acid;2-Pyridinecarboxylic acid, 5-bromo-1,6-dihydro-6-oxo-
CBNumber: CB82619950
Molecular Formula: C6H4BrNO3
Formula Weight: 218
MOL File: 1214385-51-9.mol

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5-BroMo-6-hydroxypicolinic acid Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: B997868
Product name: 5-Bromo-6-hydroxypicolinicAcid
Packaging: 100mg
Price: $65
Updated: 2021/12/16

Matrix Scientific

Product number: 119772
Product name: 5-Bromo-6-hydroxypicolinic acid
Purity: 95+%
Packaging: 250mg
Price: $324
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367047
Product name: 5-BROMO-6-HYDROXYPICOLINIC ACID
Purity: 95.00%
Packaging: 5MG
Price: $502.17
Updated: 2021/12/16

Matrix Scientific

Product number: 119772
Product name: 5-Bromo-6-hydroxypicolinic acid
Purity: 95+%
Packaging: 1g
Price: $810
Updated: 2021/12/16

AK Scientific

Product number: X9492
Product name: 5-Bromo-6-hydroxypicolinicacid
Packaging: 10g
Price: $1399
Updated: 2021/12/16

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5-BroMo-6-hydroxypicolinic acid Chemical Properties,Usage,Production

Synthesis

19621-92-2

1214385-51-9

General procedure for the synthesis of 5-bromo-6-hydroxypyridinecarboxylic acid from 6-hydroxypyridine-2-carboxylic acid: bromine (115 g, 720 mmol) was added dropwise to a suspension of 6-oxo-1,6-dihydropyridine-2-carboxylic acid (25 g, 180 mmol) in acetic acid (400 mL). The reaction mixture was heated to 80 °C and kept for 16 hours. Upon completion of the reaction, the mixture was concentrated to dryness under reduced pressure. The residue was ground with tert-butyl methyl ether (200 mL) and subsequently filtered. The filter cake was washed with tert-butyl methyl ether (3 x 100 mL) to give a gray solid product. Yield: 39.0 g, 179 mmol, 99% yield. The product was characterized by 1H NMR (400 MHz, DMSO-d6): δ 8.03 (d, J = 7.3 Hz, 1H), 6.83 (d, J = 7.3 Hz, 1H).

References

[1] Patent: US2016/222007, 2016, A1. Location in patent: Paragraph 0354; 0355

5-BroMo-6-hydroxypicolinic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-BroMo-6-hydroxypicolinic acid manufacturers

Hong Kong Tiansheng New Material Trading Co., Ltd

Product: 5-Bromo-6-hydroxypicolinic acid 1214385-51-9
Price: US $100.00/Kg/Bag
Min. Order: 1KG
Purity: 99%
Supply Ability: 10kg
Release date: 2021-09-14

Hong Kong Tiansheng New Material Trading Co., Ltd

Product: 5-Bromo-6-hydroxypicolinic acid 1214385-51-9
Price: US $100.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 100KG
Release date: 2021-09-15

Hong Kong Tiansheng New Material Trading Co., Ltd

Product: 5-Bromo-6-hydroxypicolinic acid 1214385-51-9
Price: US $100.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 10KG
Release date: 2021-09-17

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1214385-51-9