tert-Butyl (1-(Methylsulfonyl)piperidin-4-yl)carbaMate

Product Name: tert-Butyl (1-(Methylsulfonyl)piperidin-4-yl)carbaMate
CAS No.: 287953-38-2
Chemical Name: tert-Butyl (1-(Methylsulfonyl)piperidin-4-yl)carbaMate
Synonyms: tert-butyl N-(1-methylsulfonylpiperidin-4-yl)carbamate;tert-Butyl (1-(Methylsulfonyl)piperidin-4-yl)carbaMate;[1-(Methylsulfonyl)piperidin-4-yl]carbamic acid tert-butyl ester;Carbamic acid, N-[1-(methylsulfonyl)-4-piperidinyl]-, 1,1-dimethylethyl ester
CBNumber: CB82651840
Molecular Formula: C11H22N2O4S
Formula Weight: 278.37
MOL File: 287953-38-2.mol

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tert-Butyl (1-(Methylsulfonyl)piperidin-4-yl)carbaMate Property

Density: 1.21±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 12.12±0.20(Predicted)

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 097346
Product name: tert-Butyl (1-(methylsulfonyl)-piperidin-4-yl)carbamate
Purity: 95+%
Packaging: 250mg
Price: $265
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0393911
Product name: TERT-BUTYL-(1-(METHYLSULFONYL)PIPERIDIN-4-YL)CARBAMATE
Purity: 95.00%
Packaging: 5MG
Price: $502.74
Updated: 2021/12/16

Matrix Scientific

Product number: 097346
Product name: tert-Butyl (1-(methylsulfonyl)-piperidin-4-yl)carbamate
Purity: 95+%
Packaging: 1g
Price: $588
Updated: 2021/12/16

AK Scientific

Product number: 2853AB
Product name: tert-Butyl(1-(methylsulfonyl)piperidin-4-yl)carbamate
Packaging: 5g
Price: $752
Updated: 2021/12/16

Ambeed

Product number: A108129
Product name: tert-Butyl(1-(methylsulfonyl)piperidin-4-yl)carbamate
Purity: 95+%
Packaging: 250mg
Price: $36
Updated: 2021/12/16

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tert-Butyl (1-(Methylsulfonyl)piperidin-4-yl)carbaMate Chemical Properties,Usage,Production

Synthesis

124-63-0

73874-95-0

287953-38-2

General procedure for the synthesis of 1-methanesulfonyl-4-tert-butoxycarbonylaminopiperidine from methanesulfonyl chloride and 4-tert-butoxycarbonylaminopiperidine: 5.00 g (25.0 mmol) of Boc-4-aminopiperidine was dissolved in 19.8 mL of pyridine and cooled in an ice bath. 2.13 mL (27.5 mmol) of methanesulfonyl chloride was added slowly and dropwise. The reaction mixture was stirred at room temperature for 16 hours. After completion of the reaction, the reaction mixture was diluted with water and then extracted with dichloromethane (DCM). The organic layer was washed with water, dried over anhydrous magnesium sulfate (MgSO4) and filtered. The solvent was removed by concentration under reduced pressure to give 6.30 g of tert-butyl 1-methanesulfonyl-piperidin-4-yl-carbamate. The yield was 91%; ESI-MS: 279 [M + H]+.

References

[1] Patent: WO2014/184327, 2014, A1. Location in patent: Page/Page column 27
[2] Patent: WO2006/77414, 2006, A1. Location in patent: Page/Page column 163-164
[3] Bioorganic Chemistry, 2015, vol. 61, p. 21 - 27
[4] Journal of Medicinal Chemistry, 2006, vol. 49, # 22, p. 6549 - 6560
[5] Patent: US2006/14708, 2006, A1. Location in patent: Page/Page column 13

tert-Butyl (1-(Methylsulfonyl)piperidin-4-yl)carbaMate Preparation Products And Raw materials

Raw materials

Preparation Products

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tert-Butyl (1-(Methylsulfonyl)piperidin-4-yl)carbaMate Suppliers

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