2-(4-BroMo-2-Methylphenyl)acetonitrile
- Product Name
- 2-(4-BroMo-2-Methylphenyl)acetonitrile
- CAS No.
- 215800-05-8
- Chemical Name
- 2-(4-BroMo-2-Methylphenyl)acetonitrile
- Synonyms
- 4-Bromo-2-methylbenzyl cyanide;4-broMo-2-Methylphenylacetonitrile;Benzeneacetonitrile, 4-bromo-2-methyl-;2-(4-BroMo-2-Methylphenyl)acetonitrile
- CBNumber
- CB82665452
- Molecular Formula
- C9H8BrN
- Formula Weight
- 210.07
- MOL File
- 215800-05-8.mol
2-(4-BroMo-2-Methylphenyl)acetonitrile Property
- Boiling point:
- 305.7±27.0 °C(Predicted)
- Density
- 1.418±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B614330
- Product name
- 2-(4-Bromo-2-methylphenyl)acetonitrile
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B614330
- Product name
- 2-(4-Bromo-2-methylphenyl)acetonitrile
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 126529
- Product name
- 2-(4-Bromo-2-methylphenyl)acetonitrile
- Purity
- >95%
- Packaging
- 1g
- Price
- $288
- Updated
- 2021/12/16
- Product number
- 0971AB
- Product name
- 2-(4-Bromo-2-methylphenyl)acetonitrile
- Packaging
- 10g
- Price
- $436
- Updated
- 2021/12/16
- Product number
- HCH0362632
- Product name
- 2-(4-BROMO-2-METHYLPHENYL)ACETONITRILE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $500.59
- Updated
- 2021/12/16
2-(4-BroMo-2-Methylphenyl)acetonitrile Chemical Properties,Usage,Production
Synthesis
143-33-9
156001-49-9
215800-05-8
Step c: Synthesis of intermediate 5,2-(4-bromo-2-methylphenyl)acetonitrile 1-Bromo-4-(bromomethyl)-3-methylbenzene (13.2 g, 50.1 mmol) was dissolved in DMF (65 mL). The reaction mixture was cooled to 0-5 °C, followed by addition of NaCN (3.66 g, 74.6 mmol) and water (8 mL). The reaction mixture was stirred at room temperature overnight. After completion of the reaction, water (170 mL) and saturated NaHCO3 solution (130 mL) were added, followed by hexane/Et2O (2:1, 150 mL) for extraction. The organic phase was separated and the aqueous phase was further extracted with hexane/Et2O (2:1, 3 x 150 mL). All organic phases were combined, washed with water (170 mL), dried over MgSO4, filtered and concentrated under reduced pressure to afford the target product 2-(4-bromo-2-methylphenyl)acetonitrile (9.76 g, 93% yield) as an orange oil. 1H NMR (300 MHz, chloroform-D) δ: 7.40-7.32 (2H, m), 7.23 (2H, d, J = 8.2 Hz), 3.61 (2H, s), 2.32 (3H, s).
References
[1] Patent: WO2008/18827, 2008, A1. Location in patent: Page/Page column 61-62
[2] Patent: WO2006/18725, 2006, A1. Location in patent: Page/Page column 164
2-(4-BroMo-2-Methylphenyl)acetonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
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