3-(BroMoMethyl)-2-Methoxypyridine
- Product Name
- 3-(BroMoMethyl)-2-Methoxypyridine
- CAS No.
- 942060-13-1
- Chemical Name
- 3-(BroMoMethyl)-2-Methoxypyridine
- Synonyms
- 3-(BroMoMethyl)-2-Methoxypyridine;Pyridine, 3-(bromomethyl)-2-methoxy-
- CBNumber
- CB82666378
- Molecular Formula
- C7H8BrNO
- Formula Weight
- 202.05
- MOL File
- 942060-13-1.mol
3-(BroMoMethyl)-2-Methoxypyridine Property
- Boiling point:
- 235.0±25.0 °C(Predicted)
- Density
- 1.484±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 2.49±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
N-Bromosuccinimide Price
- Product number
- B847145
- Product name
- 3-(Bromomethyl)-2-methoxypyridine
- Packaging
- 100mg
- Price
- $265
- Updated
- 2021/12/16
- Product number
- HCH0364683
- Product name
- 3-(BROMOMETHYL)-2-METHOXYPYRIDINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.66
- Updated
- 2021/12/16
- Product number
- 6069AC
- Product name
- 3-(Bromomethyl)-2-methoxypyridine
- Packaging
- 1g
- Price
- $531
- Updated
- 2021/12/16
- Product number
- CM129999
- Product name
- 3-(bromomethyl)-2-methoxypyridine
- Purity
- 95%
- Packaging
- 1g
- Price
- $720
- Updated
- 2021/12/16
- Product number
- A319455
- Product name
- 3-(Bromomethyl)-2-methoxypyridine
- Purity
- 95%
- Packaging
- 1g
- Price
- $351
- Updated
- 2021/12/16
3-(BroMoMethyl)-2-Methoxypyridine Chemical Properties,Usage,Production
Synthesis
112197-16-7
942060-13-1
Step 2: Synthesis of 3-(bromomethyl)-2-methoxypyridine (Int-37) To a dichloromethane solution (10 mL) of (2-methoxypyridin-3-yl)methanol (811 mg, 5.8 mmol) and N-bromosuccinimide (1.24 g, 7.0 mmol), triphenylphosphine (1.8 g, 7.0 mmol) was added at room temperature and the mixture was stirred for 2 hours. Upon completion of the reaction, the reaction was quenched with deionized water and extracted with ethyl acetate. The organic layers were combined, washed with saturated brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography to afford 3-(bromomethyl)-2-methoxypyridine (829 mg, 70%) as a colorless oil. 1H NMR (CDCl3) δ: 8.14 (dd, J = 5.0, 1.9 Hz, 1H), 7.63 (dd, J = 7.3, 1.9 Hz, 1H), 6.89 (dd, J = 7.3, 5.0 Hz, 1H), 4.51 (s, 2H), 4.04 (s, 3H).
References
[1] Patent: WO2015/2994, 2015, A2. Location in patent: Paragraph 00195
[2] Patent: WO2007/71900, 2007, A1. Location in patent: Page/Page column 95
[3] Patent: WO2012/27261, 2012, A1. Location in patent: Page/Page column 571; 572
3-(BroMoMethyl)-2-Methoxypyridine Preparation Products And Raw materials
Raw materials
Preparation Products
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