ChemicalBook > CAS DataBase List > 1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE

1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE

Product Name: 1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE
CAS No.: 84478-76-2
Chemical Name: 1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE
Synonyms: uoro-2-methoxy-4-nitrobenzene;2-CHLORO-4-FLUORO-5-NITROANISOLE;4-Chloro-2-fluoro-5-methoxy-1-nitrobenzene;1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE;Benzene, 1-chloro-5-fluoro-2-methoxy-4-nitro-;1-Chloro-5-fluoro-2-methoxy-4-nitrobenzene, 2-Chloro-4-fluoro-5-nitrophenyl methyl ether
CBNumber: CB8267243
Molecular Formula: C7H5ClFNO3
Formula Weight: 205.57
MOL File: 84478-76-2.mol

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1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE Property

Melting point:: 72-75°C
Boiling point:: 307.9±37.0 °C(Predicted)
Density: 1.453
storage temp.: Sealed in dry,Room Temperature
form: Solid
Appearance: White to off-white Solid
CAS DataBase Reference: 84478-76-2(CAS DataBase Reference)

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Safety

Hazard Codes: Xi,C
Risk Statements: 34
Safety Statements: 26-36/37/39-45
HazardClass: IRRITANT
HS Code: 2909309090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: C584995
Product name: 1-Chloro-5-fluoro-2-methoxy-4-nitrobenzene
Packaging: 250mg
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC103325
Product name: 2-Chloro-4-fluoro-5-nitroanisole
Packaging: 1g
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC103325
Product name: 2-Chloro-4-fluoro-5-nitroanisole
Packaging: 2g
Price: $110
Updated: 2021/12/16

Matrix Scientific

Product number: 045411
Product name: 1-Chloro-5-fluoro-2-methoxy-4-nitrobenzene
Purity: >95%
Packaging: 1g
Price: $29
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-7-01
Product name: 2-Chloro-4-fluoro-5-nitroanisole
Packaging: 1g
Price: $32
Updated: 2021/12/16

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1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE Chemical Properties,Usage,Production

Synthesis

84478-75-1

74-88-4

84478-76-2

Potassium carbonate (18 g, 131 mmol) and iodomethane (8.0 mL, 131 mmol) were added to a solution of 2-chloro-4-fluoro-5-nitrophenol (5.0 g, 26.1 mmol) in acetone (100 mL) and stirred at room temperature. The reaction mixture was stirred at room temperature for 2 h. The progress of the reaction was monitored by thin layer chromatography (TLC). After completion of the reaction, the solvent was removed by evaporation under reduced pressure. The residue was diluted with distilled water (100 mL) and extracted with ethyl acetate (3 x 100 mL). The organic layers were combined, washed sequentially with distilled water (100 mL) and saturated saline (100 mL), dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 2-chloro-4-fluoro-5-nitroanisole as a yellow solid. Yield: 5.0 g (93%). 1H NMR (400 MHz, DMSO-d6): δ 7.94-7.97 (m, 1H), 7.81-7.83 (m, 1H), 3.95 (s, 3H).

References

[1] Patent: WO2018/37223, 2018, A1. Location in patent: Page/Page column 206; 207
[2] Patent: US5136868, 1992, A
[3] Patent: US4427438, 1984, A
[4] Patent: US2004/162282, 2004, A1
[5] Patent: US2009/143367, 2009, A1. Location in patent: Page/Page column 37-38

1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE manufacturers

Career Henan Chemical Co

Product: 1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE 84478-76-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-12

84478-76-2, 1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENERelated Search:

2-CHLORO-4-FLUORO-5-NITROANISOLE

1-CHLORO-5-FLUORO-2-METHOXY-4-NITROBENZENE

4-Chloro-2-fluoro-5-methoxy-1-nitrobenzene

1-Chloro-5-fluoro-2-methoxy-4-nitrobenzene, 2-Chloro-4-fluoro-5-nitrophenyl methyl ether

uoro-2-methoxy-4-nitrobenzene

Benzene, 1-chloro-5-fluoro-2-methoxy-4-nitro-

84478-76-2

C7H5ClFNO3