N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE

Product Name: N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE
CAS No.: 58161-35-6
Chemical Name: N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE
Synonyms: SKL862;5-Acetamido-1-indanone;5-Acetylamino-1-indanone;N-(1-Oxo-indan-5-yl)-acetamide;N-(1-Oxo-2,3-dihydro-1H-inden-5-yl);5-Acetamido-2,3-dihydro-1-oxo-1H-indene;N-(1-oxo-2,3-dihydroinden-5-yl)acetamide;N-(2,3-dihydro-1-oxo-1H-inden-5-yl)acetamide;N-(1-Oxo-2,3-dihydro-1H-inden-5-yl)acetamide;N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE
CBNumber: CB8268194
Molecular Formula: C11H11NO2
Formula Weight: 189.21
MOL File: 58161-35-6.mol

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N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE Property

Melting point:: 172 °C
Boiling point:: 427.4±34.0 °C(Predicted)
Density: 1.277±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.53±0.20(Predicted)
form: powder
color: Yellow
InChI: InChI=1S/C11H11NO2/c1-7(13)12-9-3-4-10-8(6-9)2-5-11(10)14/h3-4,6H,2,5H2,1H3,(H,12,13)
InChIKey: GHUPGGYDRVSZSW-UHFFFAOYSA-N
SMILES: C(NC1C=CC2=C(C=1)CCC2=O)(=O)C

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Safety

Hazard Note: Harmful
HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H332Harmful if inhaled

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: N887310
Product name: N1-(1-Oxo-2,3-dihydro-1H-inden-5-yl)acetamide
Packaging: 500mg
Price: $90
Updated: 2021/12/16

Apolloscientific

Product number: OR30266
Product name: N-(1-Oxoindan-5-yl)acetamide
Purity: 97%
Packaging: 1g
Price: $70
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4648-1-Y0
Product name: N-(1-Oxoindan-5-yl)acetamide
Purity: 97%
Packaging: 1g
Price: $77
Updated: 2021/12/16

AK Scientific

Product number: W7136
Product name: N-(1-Oxo-2,3-dihydro-1H-inden-5-yl)acetamide
Packaging: 100mg
Price: $81
Updated: 2021/12/16

AK Scientific

Product number: W7136
Product name: N-(1-Oxo-2,3-dihydro-1H-inden-5-yl)acetamide
Packaging: 250mg
Price: $91
Updated: 2021/12/16

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N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE Chemical Properties,Usage,Production

Definition

ChEBI: N1-(1-oxo-2,3-dihydro-1H-inden-5-yl)acetamide is a member of indanones.

Synthesis

59856-06-3

58161-35-6

General procedure for the synthesis of 5-acetamido-1-indanone from N-(2,3-dihydro-1H-inden-5-yl)acetamide: To a stirred solution of N-(2,3-dihydro-1H-inden-5-yl)acetamide (11.5 g, 65.7 mmol) in acetic acid: ethyl acetate (1:1, 200 ml) was slowly added dropwise to a solution of chromium trioxide (15 g) dissolved in water at 0 °C 151.11 mmol) dissolved in water. The reaction mixture was continued to be stirred at room temperature for 3 hours. After completion of the reaction, the mixture was diluted with water and extracted with ethyl acetate. The organic phases were combined, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography with methanol/dichloromethane as eluent to afford the target product 5-acetamido-1-indanone (9 g, 85% yield) as a yellow solid. m/z = 190 [M + H]+ by LC-MS.

References

[1] Patent: WO2016/44770, 2016, A1. Location in patent: Page/Page column 548
[2] Journal of Chemical Research, 2013, vol. 37, # 4, p. 232 - 235
[3] Journal of Organic Chemistry, 1962, vol. 27, p. 70 - 76
[4] Physical Chemistry Chemical Physics, 2001, vol. 3, # 17, p. 3555 - 3561
[5] Patent: WO2013/62892, 2013, A1. Location in patent: Page/Page column 45

N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE Suppliers

Belgium 1 China 62 Germany 1 India 1 United Kingdom 4 United States 15 Global 84

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Thermo Fisher Scientific

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View Lastest Price from N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE manufacturers

Career Henan Chemical Co

Product: N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE 58161-35-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-12-18

58161-35-6, N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDERelated Search:

4-ACETAMIDO-2-METHYLACETOPHENONE 5-Aminoindan-1-one Indene N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE 5-Aminoindan 4'-ETHYL-3'-METHYLACETANILIDE 4'-AMINOPROPIOPHENONE 4'-ACETAMIDOACETOPHENONE N1-(4-PROPYLPHENYL)ACETAMIDE N-(6-BROMO-2,3-DIHYDRO-1-OXO-1H-INDEN-5-YL)ACETAMIDE Ethanone, 1-(4-amino-2-methylphenyl)- (9CI) N1-(2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE 4-BROMO-5-ACETAMIDOINDANONE INDAN-5-YL-METHYL-AMINE 2,2,2-trifluoro-N-(4-methoxy-3-oxo-2,3-dihydro-1H-inden-1-yl)acetamide N1-[2-(2-furylmethylidene)-1-oxo-2,3-dihydro-1H-inden-5-yl]acetamide 2,2,2-TRIFLUORO-N-(6-METHOXY-3-OXO-2,3-DIHYDRO-1H-INDEN-1-YL)ACETAMIDE 2-CHLORO-N-(5,6-DIMETHOXY-3-OXO-2,3-DIHYDRO-1H-INDEN-1-YL)ACETAMIDE

N1-(1-OXO-2,3-DIHYDRO-1H-INDEN-5-YL)ACETAMIDE

5-Acetamido-1-indanone

5-Acetylamino-1-indanone

N-(1-Oxo-2,3-dihydro-1H-inden-5-yl)acetamide

5-Acetamido-2,3-dihydro-1-oxo-1H-indene

N-(1-Oxo-2,3-dihydro-1H-inden-5-yl)

N-(2,3-dihydro-1-oxo-1H-inden-5-yl)acetamide

N-(1-Oxo-indan-5-yl)-acetamide

N-(2,3-Dihydro-1-oxo-1H-inden-5-yl)acetamide, 5-(Acetylamino)-2,3-dihydro-1-oxo-1H-indene, 5-Acetamido-2,3-dihydro-1-oxo-1H-indene

N-(1-oxo-2,3-dihydroinden-5-yl)acetamide

Acetamide, N-(2,3-dihydro-1-oxo-1H-inden-5-yl)-

SKL862

58161-35-6

KETONE

API intermediates