1,3,5-Trichloro-2,4,6-triiodobenzene

Product Name: 1,3,5-Trichloro-2,4,6-triiodobenzene
CAS No.: 151721-79-8
Chemical Name: 1,3,5-Trichloro-2,4,6-triiodobenzene
Synonyms: 1,3,5-Trichloro-2,4,6-triiodobenzene;Benzene, 1,3,5-trichloro-2,4,6-triiodo-
CBNumber: CB82693235
Molecular Formula: C6Cl3I3
Formula Weight: 559.14
MOL File: 151721-79-8.mol

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1,3,5-Trichloro-2,4,6-triiodobenzene Property

Melting point:: 276 °C
Boiling point:: 470.1±40.0 °C(Predicted)
Density: 2.919±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
form: powder to crystal
color: White to Light yellow

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Safety

HS Code: 2903.99.8001

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: T3584
Product name: 1,3,5-Trichloro-2,4,6-triiodobenzene
Packaging: 1G
Price: $179
Updated: 2025/07/31

AK Scientific

Product number: 7609AA
Product name: 1,3,5-Trichloro-2,4,6-triiodobenzene
Packaging: 1g
Price: $843
Updated: 2021/12/16

Matrix Scientific

Product number: 095857
Product name: 1,3,5-Trichloro-2,4,6-triiodobenzene
Purity: 95+%
Packaging: 250mg
Price: $265
Updated: 2021/12/16

AK Scientific

Product number: 7609AA
Product name: 1,3,5-Trichloro-2,4,6-triiodobenzene
Packaging: 250mg
Price: $407
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0361836
Product name: 1,3,5-TRICHLORO-2,4,6-TRIIODOBENZENE
Purity: 95.00%
Packaging: 5MG
Price: $505.67
Updated: 2021/12/16

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1,3,5-Trichloro-2,4,6-triiodobenzene Chemical Properties,Usage,Production

Synthesis

108-70-3

151721-79-8

Synthesis Example 1 Synthesis of 1,3,5-trichloro-2,4,6-triiodobenzene (Scheme 3-(7)) [show image] In a 100 mL three-necked flask, 1,3,5-trichlorobenzene (5.0 g, 27.6 mmol), iodine (40.3 g, 31.8 mmol), and 98% concentrated sulfuric acid (75 mL) were added, and heated and refluxed for 72 hours at 140 °C. Upon completion of the reaction, the reaction mixture was washed sequentially with aqueous sodium bisulfite, saturated aqueous sodium bicarbonate and deionized water, followed by drying. The crude product was dissolved in tetrahydrofuran (THF) and purified by recrystallization to give colorless needle-like crystals (14.3 g, 93% yield). Mass spectrum (70 eV, EI) m/z = 558 (M+); melting point > 300°C (determined in a sealed tube).

References

[1] Angewandte Chemie - International Edition, 2016, vol. 55, # 21, p. 6270 - 6274
[2] Angew. Chem., 2016, vol. 128, # 21, p. 6378 - 6382,5
[3] Patent: WO2017/98455, 2017, A1. Location in patent: Page/Page column 6
[4] Organic Letters, 2001, vol. 3, # 15, p. 2419 - 2421
[5] Patent: EP2361915, 2011, A1. Location in patent: Page/Page column 35

1,3,5-Trichloro-2,4,6-triiodobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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1,3,5-Trichloro-2,4,6-triiodobenzene Suppliers

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151721-79-8, 1,3,5-Trichloro-2,4,6-triiodobenzeneRelated Search:

Chromium(VI) oxide

1,3,5-Trichloro-2,4,6-triiodobenzene

Benzene, 1,3,5-trichloro-2,4,6-triiodo-

151721-79-8

C6Cl3I3

intermediate