1,3,5-Trichloro-2,4,6-triiodobenzene
- Product Name
- 1,3,5-Trichloro-2,4,6-triiodobenzene
- CAS No.
- 151721-79-8
- Chemical Name
- 1,3,5-Trichloro-2,4,6-triiodobenzene
- Synonyms
- 1,3,5-Trichloro-2,4,6-triiodobenzene;Benzene, 1,3,5-trichloro-2,4,6-triiodo-
- CBNumber
- CB82693235
- Molecular Formula
- C6Cl3I3
- Formula Weight
- 559.14
- MOL File
- 151721-79-8.mol
1,3,5-Trichloro-2,4,6-triiodobenzene Property
- Melting point:
- 276 °C
- Boiling point:
- 470.1±40.0 °C(Predicted)
- Density
- 2.919±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- form
- powder to crystal
- color
- White to Light yellow
Safety
- HS Code
- 2903.99.8001
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- T3584
- Product name
- 1,3,5-Trichloro-2,4,6-triiodobenzene
- Packaging
- 1G
- Price
- $179
- Updated
- 2025/07/31
- Product number
- 095857
- Product name
- 1,3,5-Trichloro-2,4,6-triiodobenzene
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $265
- Updated
- 2021/12/16
- Product number
- 7609AA
- Product name
- 1,3,5-Trichloro-2,4,6-triiodobenzene
- Packaging
- 250mg
- Price
- $407
- Updated
- 2021/12/16
- Product number
- HCH0361836
- Product name
- 1,3,5-TRICHLORO-2,4,6-TRIIODOBENZENE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $505.67
- Updated
- 2021/12/16
- Product number
- 095857
- Product name
- 1,3,5-Trichloro-2,4,6-triiodobenzene
- Purity
- 95+%
- Packaging
- 1g
- Price
- $588
- Updated
- 2021/12/16
1,3,5-Trichloro-2,4,6-triiodobenzene Chemical Properties,Usage,Production
Synthesis
108-70-3
151721-79-8
Synthesis Example 1 Synthesis of 1,3,5-trichloro-2,4,6-triiodobenzene (Scheme 3-(7)) [show image] In a 100 mL three-necked flask, 1,3,5-trichlorobenzene (5.0 g, 27.6 mmol), iodine (40.3 g, 31.8 mmol), and 98% concentrated sulfuric acid (75 mL) were added, and heated and refluxed for 72 hours at 140 °C. Upon completion of the reaction, the reaction mixture was washed sequentially with aqueous sodium bisulfite, saturated aqueous sodium bicarbonate and deionized water, followed by drying. The crude product was dissolved in tetrahydrofuran (THF) and purified by recrystallization to give colorless needle-like crystals (14.3 g, 93% yield). Mass spectrum (70 eV, EI) m/z = 558 (M+); melting point > 300°C (determined in a sealed tube).
References
[1] Angewandte Chemie - International Edition, 2016, vol. 55, # 21, p. 6270 - 6274
[2] Angew. Chem., 2016, vol. 128, # 21, p. 6378 - 6382,5
[3] Patent: WO2017/98455, 2017, A1. Location in patent: Page/Page column 6
[4] Organic Letters, 2001, vol. 3, # 15, p. 2419 - 2421
[5] Patent: EP2361915, 2011, A1. Location in patent: Page/Page column 35
1,3,5-Trichloro-2,4,6-triiodobenzene Preparation Products And Raw materials
Raw materials
Preparation Products
1,3,5-Trichloro-2,4,6-triiodobenzene Suppliers
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