9-(4-phenylphenyl)carbazole
- Product Name
- 9-(4-phenylphenyl)carbazole
- CAS No.
- 6299-16-7
- Chemical Name
- 9-(4-phenylphenyl)carbazole
- Synonyms
- NSC 42475;N-Biphenylcarbazole;9-(4-biphenyl)carbazole;N-(4-biphenylyl)carbazole;9-(4-biphenylyl)carbazole;9-(4-Phenylphenyl)carbazol;9-(Biphenyl-4-yl)carbazole;9-(4-phenylphenyl)carbazole;9-(4-Biphenylyl)-9H-carbazole;9-[1,1'-Biphenyl]-4-yl-carbazole
- CBNumber
- CB82707356
- Molecular Formula
- C24H17N
- Formula Weight
- 319.4
- MOL File
- 6299-16-7.mol
9-(4-phenylphenyl)carbazole Property
- Melting point:
- 224-226℃
- Boiling point:
- 512.0±33.0 °C(Predicted)
- Density
- 1.11±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- color
- White to Light yellow
Safety
- HS Code
- 2933.99.8290
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- B5128
- Product name
- 9-(4-Biphenylyl)carbazole
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $33
- Updated
- 2025/07/31
- Product number
- B5128
- Product name
- 9-(4-Biphenylyl)carbazole
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $77
- Updated
- 2025/07/31
- Product number
- 9568AL
- Product name
- 9-(4-Biphenylyl)carbazole
- Packaging
- 25g
- Price
- $90
- Updated
- 2021/12/16
- Product number
- AS024435
- Product name
- 9-(4-Biphenylyl)carbazole
- Purity
- 97%
- Packaging
- 25g
- Price
- $93
- Updated
- 2021/12/16
- Product number
- A128729
- Product name
- 9-(4-Biphenylyl)carbazole
- Purity
- 97%
- Packaging
- 25g
- Price
- $94
- Updated
- 2021/12/16
9-(4-phenylphenyl)carbazole Chemical Properties,Usage,Production
Synthesis
92-66-0
86-74-8
6299-16-7
General procedure for the synthesis of 9-(4-biphenylyl)carbazole from 4-bromobiphenyl and carbazole: To a three-necked flask under nitrogen protection were added 12 g (50 mmol) of 4-bromobiphenyl, 8.4 g (50 mmol) of carbazole, 230 mg (1 mmol) of palladium acetate, 1.8 g (3.0 mmol) of 1,1-bis(diphenylphosphino)ferrocene and 13 g ( 180 mmol) sodium tert-butoxide. After displacing the atmosphere in the flask with nitrogen, 80 mL of dehydroxylene was added and degassed. The reaction mixture was stirred at 120°C for 7.5 hours under nitrogen atmosphere. Upon completion of the reaction, about 600 mL of preheated toluene was added to the suspension, which was sequentially filtered twice through florid silica, alumina and diatomaceous earth. The resulting filtrate was concentrated and recrystallized by adding hexane. The solid product was collected by filtration and dried to give 14 g (yield: 87%) of 9-(4-biphenyl)carbazole as a cream colored powder.
References
[1] Patent: JP2017/128519, 2017, A. Location in patent: Paragraph 0029
[2] Patent: WO2006/70912, 2006, A1. Location in patent: Page/Page column 70; 71
[3] Journal of Organic Chemistry, 1957, vol. 22, p. 226
[4] Patent: EP2085382, 2009, A1. Location in patent: Page/Page column 41
[5] Inorganica Chimica Acta, 2012, vol. 390, p. 119 - 122
9-(4-phenylphenyl)carbazole Preparation Products And Raw materials
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View Lastest Price from 9-(4-phenylphenyl)carbazole manufacturers
- Product
- 9-([1,1'-biphenyl]-4-yl)-9H-carbazole 6299-16-7
- Price
- US $10.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 ton
- Release date
- 2024-12-06
- Product
- N-Biphenylcarbazole 6299-16-7
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.00%
- Supply Ability
- 150KG /month
- Release date
- 2021-11-12
- Product
- 9-([1,1'-biphenyl]-4-yl)-9H-carbazole 6299-16-7
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-31